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SEDIMENT SIZE ANALYSIS - Nutrient Analytical Services Laboratory

SEDIMENT SIZE ANALYSIS - Nutrient Analytical Services Laboratory

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8. Repeat steps 4-6 until the fluid is clear. This may take up to several liters of<br />

SHMP solution depending on the type of sediment.<br />

9. Rinse what remains in the beaker thoroughly with deionized water.<br />

10. Remove contents in the beaker to the pre-weighed aluminum foil dish and dry<br />

at 80 degrees C.<br />

To Determine The Amount of Fines<br />

Measure the amount of SHMP used for a specific sample and<br />

record on the bench sheet.<br />

Filter at least two replicate aliquots for TSS measurements/sample<br />

on a pre weighed 47 mm GF/F filter. Dry and weigh as per a normal TSS<br />

measurement. Record on bench sheet.<br />

Based on the TSS result (number of grams material for a given<br />

volume), determine the amount of fine material for the entire sample.<br />

Enter your work on the bench sheet.<br />

Ro-tap Sieve Method<br />

1. Record the dry weight of the sample.<br />

2. Place the entire sample onto the first (most coarse) sieve.<br />

3. Ro-tap for 15 minutes. Sieve sizes routinely used are 2.0 mm, 0.5 mm,<br />

0.25 mm, 125 micron and 60 micron and the method allows for the<br />

flexibility to add or subtract sieves depending on the project requirements.<br />

4. Transfer material that is retained on each sieve to a pre-weighed large<br />

plastic weighing dish. Use a tooth brush to loosen as much material as<br />

possible. Record the sample+weighing dish weight on the bench sheet.<br />

Calculation<br />

Subtract the weigh dish weight from the total amount weighed for that sieved<br />

fraction.<br />

Add the amount determined from the SHMP procedure to the last fraction<br />

(

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