Processing kodak motion picture films, module 3 analytical procedures

Table 1 Required Tolerance for Volumetric
Glassware
Capacity,
mL
Delivery
Time *
Pipets
Class A
or Equiv.
TD †
Tolerance of Glassware, mL
Graduated
Cylinder
TD †
Burets
(Class A)
TD †
* Minimum delivery time for Class A serialized and non-serialized (maximum
delivery time 60 sec).
† Calibrated to deliver.
‡ Calibrated to contain.
Table 2 Effect of Temperature on Solution Volume
Volumetric
Flasks
(Class A)
TC ‡
1 10 ± 0.006 ± 0.1 ± 0.01
2 10 0.006 0.015
3 10 0.01 0.015
4 10 0.01
5 15 0.01 0.02
10 15 0.02 0.1 ± 0.02 0.02
15 15 0.03
20 25 0.03
25 25 0.03 0.3 0.03 0.03
50 30 0.05 0.4 0.05 0.05
100 40 0.08 0.6 0.10 0.08
200 50 0.10 1.4 0.10
250 1.4 0.12
500 2.6 0.15
1000 5.0 0.3
2000 10.0 0.5
4000 50.0
Solution
Composition
Volumes (mL) Occupied at *
59°F 68°F 77°F 86°F 95°F
15°C 20°C 25°C 30°C 35°C
1.0 N HCl 996.7 1000.0 1001.3 1002.8 1004.7
0.1 N HCl 997.1 1000.0 1001.2 1002.6 1003.8
Water 999.1 1000.0 1001.1 1002.5 1004.2
* References: Fales and Kenney, Inorganic Quantitative Analysis (1940).
Processing KODAK Motion Picture Films, Module 3, Analytical Procedures H24.03 9