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Processing kodak motion picture films, module 3 analytical procedures

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Titration<br />

1. Titrate the sample potentiometrically according to<br />

Method ULM-0003-01, with standardized 0.05 N<br />

silver nitrate using a 25-mL buret.<br />

Note: The titration may be performed most rapidly in<br />

the beginning where the potential change is the<br />

smallest. Refer to Figures 1 and 2, to determine the<br />

increment size to use in the region of the end point and<br />

the expected potential change in millivolts.<br />

2. Determine the end point using the concentric arcs from<br />

Method ULM-0003-01, Potentiometric Titrations for<br />

Photoprocessing Solutions.<br />

Calculations<br />

NaBr, g/L =<br />

(N AgNO3 )(mL AgNO3 ) x (eq. wt. NaBr) x (1000)<br />

=<br />

(mL sample) x (1000)<br />

(N AgNO 3 )(mL AgNO 3 ) x (102.91) x (1000)<br />

(50) x (1000)<br />

2.058(mL AgNO 3)(N AgNO 3)<br />

=<br />

4 <strong>Processing</strong> KODAK Motion Picture Films, Module 3, Analytical Procedures H24.03

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