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BIOSORPTION OF Pb2+, Cd2+, & Ni2+ FROM WATERS BY ...

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Table 3.2. Elemental composition of biosorbents in terms of C, H, N, and S<br />

Biosorbents % C % H % N % S<br />

Dunaliella salina 40.19 5.79 9.19 0.76<br />

Oocystis sp. 47.66 7.18 5.49 0.57<br />

Porphyridium cruentum 14.45 3.11 1.30 1.57<br />

Scenedesmus protuberans 47.52 7.02 7.18 0.66<br />

3.1.4. Thermo Gravimetric Analysis (TGA)<br />

Thermal stability of the algae was investigated using TGA in which the mass<br />

loss of the sample is monitored as a function of temperature. The solid samples were<br />

heated from 25ºC to 750ºC in 10 minute intervals in N2 atmosphere. The plots are given<br />

in Figure 3.3–3.6.<br />

In Figure 3.3, the first mass loss of Dunaliella salina which is less than 10% in<br />

the temperature range of 25ºC-100ºC is due to the release of bound water molecules.<br />

The largest loss can be seen in 240ºC-560ºC, and then in 560ºC-630ºC which can be<br />

attributed to the decomposition of the organic part of the sample.<br />

Figure 3.3. TGA decomposition curve of Dunaliella salina<br />

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