Ph. D. THESIS 2009

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Selected references 1. (a) K. Frische, M. Greenwald, E. Ashkenasi, N.G. Lemcoff, S. Abramson, I. Golender, B. Fuchs, Tetrahedron Lett. 1995, 36, 9193-9196; (b) A. Merz, L. Gromann, A. Karl, T. Burgemeister, K. Kastner, Liebigs Ann. 1996, 10, 1635- 1640, (c) D. Ranganathan, V. Haridas, I. L. Karle, , Tetrahedron 1999, 55, 6643- 6656 ; (d) B. J. Bridson, R. England, M. F. Mahon, K. Reza, M. Sainsbury, , J. Chem. Soc. Perkin Trans. 2 1995, 10, 1909-1039. 1 2. P. Yates, E. S. Hand, G. B. French, , J. Am. Chem. Soc. 1960, 82, 6347- 6353. 3. H. Stetter, H. Held, A. Schulte-Oestrich, , Chem. Ber. 1962, 95,1687-1691. 4. L. M. Jackman, S. Sternhell, “ Applications of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry”, 2 nd ed., Pergamon Press: Oxford, 1969, 334-335. 5. S. H Bertz, G. Dabbagh, Angew. Chem, Int. Ed. Engl. 1983, 21, 303; (b) R. D Sands, J. Org. Chem. 1983, 48, 3362-3363. 6.(a) M. M. Folkendt, B. E. Weiss-Lopez, J. P. Chauvel Jr, N. S. True, , J. Phys. Chem. 1985, 89, 3347-3352; (b) T. Ishida, F. Hirata and S. Kato, J. Chem. Phys. 1999, 110, 3938-3945; (c) Y. Park and C. H. Turner, , J. Supercrit. Fluids 2006, 37, 201-208. 7. N. Tosa, A. Bende, S. Cîntă Pînzaru, I. Grosu, and E. Surducan, Studia Univ. Babes-Bolyai, Physica , 2004, 44, 289-292. 8. E. Mesaros, I. Grosu, S. Mager, G. Plé, I. Farcas, , Monatsh. Chem. 1998, 129, 723-733. 9. F. Matloubi Moghaddam, A. Sharifi, , Synth. Commun. 1995, 25, 2457-2461 11. I. Fenesan, R. Popescu, C. T. Supuran, S. Nicoara, M. Culea, N. Palibroda, Z. Moldovan, O. Cozar, Rapid Commun Mass Spectrom., 2001, 15, 721-729. 11. S. Mager, N. Palibroda, I. Grosu, M. Horn, Studia Univ. Babes-Bolyai, Chemia, 1983, XXVIII, 14-19. 12. M. Culea, N. Palibroda, S. Nicoara, O. Cozar, I. Oprean, I. Fenesan, Studia Univ Babes-Bolyai, Physica, 1991, XXXVIII, 11-21. 13. A. Mitra and M. Dutta Gupta, Tetrahedron 1976, 32, 2731-2733. 14. B. D. Gupta, R. Yamuna, and D. Mandal, Organometallics 2006, 25, 706- 714. 15. I. Grosu, E. Bogdan, G. Plé, L. Toupet, Y. Ramondenc, E. Condamine, V. Peulon-Agasse, M. Balog, Eur. J. Org. Chem. 2003, 16, 3153-3161. 16. N. Toşa, A. Bende, R. A. Varga, A. Terec, I. Bratu and I. Grosu, J. Org. Chem. 2009, 74, 3944-3947. 17. A. Strenger, P. Rademacher, Eur. J. Org. Chem. 1999, 7, 1611-1617. 18. I. Grosu, M. Balog, S. Mager, Rev. Roum. Chim. 2005, 50, 333-339. 19. (a) J. W. Fraser, G. R. Hedwig, M. M. Morgan, H. K. Powell,. J. Aust. J. Chem. 1970, 23, 1847-1852; (b) H. K. J Powell, J. M. Russell Aust. J. Chem. 1977, 30, 1467-1473. 45
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Page 1 and 2: “BABES-BOLYAI” UNIVERSITY CLUJ-
Page 3 and 4: General Introduction OUTLINE Part A
Page 5 and 6: 3.6.1. Dots 188 3.6.2. 3D structure
Page 7 and 8: Part A: Synthesis and Structural An
Page 9 and 10: H 3C H 3C O O O C C O O 1a O O C C
Page 11 and 12: The two forms are in equilibrium an
Page 13 and 14: Figu re 4 . Th e 13 C-NMR APT (CDCl
Page 15 and 16: set used , the anarmonicities that
Page 17 and 18: Figure 9. ORTEP diagram for the bic
Page 19 and 20: 1.5.1. Tetramethyl 3,7-dihydroxybic
Page 21 and 22: Table 7. The selected molecular par
Page 23 and 24: a b Figure 14. 1 H NMR spectrum (CD
Page 25 and 26: Figure 16. 13 C NMR spectrum APT (C
Page 27 and 28: Absorbance (a. u.) Absorbance (a.u.
Page 29 and 30: icyclo[3.3.1]nonane-3,7-dione solut
Page 31 and 32: m u lt ip let a t a t δ ==1 .7 6 p
Page 33 and 34: Figure 22. 13 C NMR APT spectrum of
Page 35 and 36: Figure 24. NMR investigation of the
Page 37 and 38: (mol·l -1 ) syn 8.8 x10 -3 1.4373
Page 39 and 40: a b Figure 29. 3D FTIR spectra in s
Page 41 and 42: Figure 32. ORTEP diagram for the cy
Page 43 and 44: H2 … N3 = 1.839 Å H5 … N6 = 1.
Page 45: 2. Conclusions of the part A Differ
Page 50 and 51: 2. Experimental part: fabrication a
Page 52 and 53: 3 m 30 m a b Figure 4. Optical imag
Page 54 and 55: (NA 1.25) in phase-contrast (a) and
Page 56 and 57: was chosen instead of an aqueous on
Page 58 and 59: Our goal is to develope a lasser as
Page 60 and 61: Figure 15. a Optical image of gold
Page 62 and 63: the power as parameter exhibits a m
Page 64 and 65: a b Figure 21 a) Optical image of g
Page 66: 4.5.3. 3D structures The 3D structu
Page 69 and 70: Selected References 1. E. S. Wu, J.
Page 71: VIII. J. Bosson-Ehoomann, A. Mihut,

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