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CASE NARRATIVE 

LABORATORY TMA/ARLI } 10 

CASE : 12-047 

CONTRACT ID : WESTINGHOUSE HANFORD COMPANY 11 

SDG RECEIPT DATE : December 14, 1992 

1.0 DESCRIPTION OF CASE : 

,e0? Q 93-•'7"m A -3 9.5- 

0046301 00000' 

Thirteen soil samples were analyzed for TCL Organics- 

Volatiles and Semivolatiles and Pesticide/PCBs according to 

the USEPA Contract Laboratory Program (CLP) Statement of 

Work for Organic Analysis, Revision OLM01.8. 

2.0 SAMPLE LIST : 

ANALYSIS 

WESTINGHOUSE ID LAB ID MATRIX 

B07093 A2-12-047-01A V SOIL 

807093 A2-12-047-018 SV & P SOIL 

B07093 MS A2-12-047-01C SV SOIL 

807093 MSD A2-12-047-011) SV SOIL 

B07094 A2-12-047-02A V SOIL 

807094 A2-12-047-02B SV & P SOIL 

B07094 MS A2-12-047-02C P SOIL 

807094 MSD A2-12-047-02D P SOIL 

B070BO A2-12-047-03A V SOIL 

B07090 MS A2-12-047-038 V SOIL 

807080 MSD A2-12-047-03C V SOIL 

B07081 A2-12-047-04A V SOIL 

B07QB1 A2-12-047-048 SV & P SOIL 

807095 A2-12-047-05A V SOIL 

807095 A2-12-047-05B SV & P SOIL 

807096 A2-12-047-06A V SOIL 

B07096 A2-12-047-068 SV & P SOIL 

B07099 A2-12-047-07A V SOIL 

807099 A2-12-047-07B SV & P SOIL 

807082 A2-12-047-08A V SOIL 

B07082 A2-12-047-08B SV & P SOIL 

B07QB3 A2-12-047-09A V SOIL 

B07QB3 A2-12-047-099 SV & P SOIL 

B070SS A2-12-047-10A V SOIL 

B070B8 A2-12-047-109 SV & P SOIL 

B07QB9 A2-12-047-11A V SOIL 

8070B9 A2-12-047-11B SV & P SOIL 

B07000 A2-12-047-12A V SOIL 

B07000 A2-12-047-128 SV & P SOIL 

907098 A2-12-047-13A V SOIL 

807098 A2-12-047-138 SV & P SOIL 

'k•

3.0 COMMENTS : 

3.1 SHIPPING AND DOCUMENTATION 

000 

All of the samples were received and properly 

documented. The VOA aliquot for sample B07QB3 was 

received from Skinner & Sherman on 12/17/92. 

3.2 ANALYSIS 

3.2.1 VOLATILE ANALYSIS COMMENTS : 

LOW LEVEL SOIL 

The samples were analyzed by heated purge within 

the CLP SOW holding times. 

All of the QC results were within the limits 

specified by the EPA CLP SOW. 

TUNES : 

All of the BPB tunes are injected directly into 

the GC/MS instrument. 

3.2.2 SEMIVOLATILE ANALYSIS COMMENTS : 

LOW LEVEL SOIL : 

The samples were extracted and analyzed within the 

CLP SOW holding times. 

All of the OC results were within the limits 


3.2.3 PESTICIDE/PCB ANALYSIS COMMENTS : 

SEQUENCE NOTES : 

The sequence was started on 01/05/93 and analyzed 

in accordance with the EPA CLP SOW. The sequence 

was analyzed by single injection into a dual 

column system. The sequence met all the QC 

criteria specified in the CLP SOW. 

The Chromatograms are presented in the manner 

consistent with the capabilities of the Nelson 

2700 Turbochrome Data System which normalizes the 

largest peak to scale.

SAMPLE NOTES: 

LOW LEVEL SOIL 

The samples were extracted and analyzed within the 

CLP SOW holding times. Samples 807093 and B07099 

had TCX surrogate recoveries slightly below the QC 

limits for both GC columns. Sample 8070BS had TCX 

surrogate recoveries slightly below the QC limits 

for the DB-608 column. Sample B07098 had TCX 

surrogate recoveries slightly below the QC limits 

on the DB-1701 column. Sample PBLK1221S had TCX 

and DCB surrogate recoveries slightly below the QC 

limits for both GC columns. In accordance with 

protocol, no further action was required. 

All of the other QC results were within the limits 


We certify that this data package is in compliance with the 

terms and conditions of the contract, both technically and 

for completeness, for other than the conditions detailed 

above. Release of the data in this hardcopy data package 

and in the computer-readable data submitted on diskette is 

authorized by the Laboratory Manager or his designee, as 

verified by the following signatures. 

Nicole Roth Wida Ang 

CLP Program Manager Organics Supervisor 

111l1^,

IA 

VOLATILE ORGANICS ANALYSIS DATA SHEET 

Lab Name: TMA/ARLI Contract: WHC 1 

000005 

EPA SAMPLE NO. 

I B07Q93 

Lab Code: TMALA Case No.: 12047 SAS No.: KA SDG No.: gam_ 

Matrix: (soil/water) SOIL Lab Sample ID: A212047-01A 

Sample wt/Vol: 5.0 (g/mL) G Lab File ID: 21221R03_ 

Level: (low/mad) I&N— Date Received: 12/14/92 

% Moisture: not doe. 6 Date Analyzed: 12/21/92 

GC Column: BACK ID: 2.00 (mm) Dilution Factor: 1.0 

Soil Extract Volume: (uL) Soil Aliquot Volume: (UL) 

:ONCENTRATION UNITS: 

CAS NO. COMPOUND (ug/L or ug/Rg) UG/KQ Q 

74-87- 3 --------- Chloromethane li I V1 

74-83-9 --------- Bromomethane j 11 I U 1 

75-01-4---------Vinyl Chloride 1 li IV 1 

75-00-3 --------- Chloroethane 1 11 III 1 

75-09-2---------Methylene Chloride I 10 I J 1 

67-64-1---------Acetone 1 42 I B 1 

75-15-0---------Carbon Disulfide I 11 IV 1 

75-35-4 --------- 1,1-Dichloroethens I 11 IU 1 

75-34-3 --------- 1,1-Dichloroethans 1 11 III 1 

540-59-0 -------- 1,2-Dichloroethene (total) _I 11 I U1 

67-66-3---------Chloroform 1 it III 1 

107-06-2 -------- 1,2-Dichloroethane 1 11 III 1 

78-93-3 --------- 2-Butanone 1 11 I U 1 

71-55-6 --------- 1,1,1-Trichloroethane 1 it I U I 

56-23-5---------Carbon Tetrachloride 1 11 I U 1 

75-27-4 --------- Bromodichloromethane I li I U1 

78-87-5 --------- 1,2-Dichloropropane I 11 I II 1 

10061-01-5 ------ cis-1,3-Dichloropropane I 11 I U 1 

79-01-6 --------- Trichloroethene 1 11 I U 1 

124-48-1 -------- Dibromochloromethane 1 11 I UI 

79-00-5 --------- 1,1,2-Trichloroethans 1 it I II j 

71-43-2---------Benzene I 11 I U1 

10061-02-6 ------ trans-1,3-D chloropropene I 11 I U1 

75-25-2 --------- Bromoform 1 li III I 

108-10-1 -------- 4-Methyl-2-Pentanons I 11 I U1 

591-78-6 -------- 2-Hexanone I 11 I U1 

127-18-4 -------- Tetrachloroethene I 11 I U1 

79-34-5 --------- 1,1,2,2-Tetrachloroethene 1 11 I V_ I 

108-88-3--------Toluene 1 it I UI 

108-90-7 -------- Chlorobenzene 1 11 I UI 

100-41-4 -------- Ethylbenzene 1 11 I UI 

100-42-5--------Styrene I 11 I VI 

1330-20-7 ------- 8ylene (total) j it 

I 

I UI 

I I 

FORM I VOA 3/90

is 

EPA SAM12M 


TENTATIVELY IDENTIFIED COMPOUNDS I 

I B07Q93 I 

Lab Name: TMA/ARLI Contract: WHC I i 

Lab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 5.0 (q/mL) G Lab File ID: 21221R03 

Level: (low/mad) LOW Date Received: 12/14/92 

% Moisture: not dec. _ 6 Date Analyzed: 12/21/92 

GC Column: PACK ID: 2.00 (mm) Dilution Factor: 1.0 

Soil Extract Volume: (UL) Soil Aliquot Volume: (uL) 

CONCENTRATION UNITS: 

Number TICS found: _1 (ug/L or ug/Kg) UG/KG 

I CAS NUMBER I COMPOUND NAME RT EST. CONC. I Q 

I 1. (UNKNOWN ALKANE 16.53 6 IJ 

FORM I VOA-TIC 3/90

IA EPA Qa. 


I B07Q94 

Lab Name: TMA/ARLI Contract: WHC I 

Lab Code: MJ&LA Case No.: 12047 SAS No.: NA SDG No.: Kh 

Matrix: ( soil/water) SOIL 

d 

Lab Sample ID: A212047-02A 

Sample wt/vol: 5.0 (VML) G File ID: 21221804 

Level: (low/mad) LOW Date Received: 12 /14/92 

t Moisture: not dec. 4 Date Analyzed: 12/21/92 


Soil Extract Volume: (uL) Soil Aliquot Volume: (uL) 

^ 

CAS NO. COMPOUND 


(ug/L or ug/Kg) UG/KG Q 

74-87-3 --------- Chloromethane 

74-83-9 --------- Bromomethane 

75-01-4---------Vinyl Chloride 

75-00 - 3 --------- Chloroethane 

I 

1 

I 

I 

I 

10 

10 

10 

10 

I 

IU 

III 

III 

III 

75-09 -2---------Methylene Chlor de I 

9 IJ 

67-64-1-------- -Acetone 1 41 IB 

75-15- 0---------Carbon Disulfide 1 10 III 

75-35-4 --------- 1, 1-Dichloroethene I 10 III 

75-34-3 --------- 1,1-Dichloroethane 1 10 III 

540-59-0 -------- 1,2-Dichloroethens (total)_I 10 III 

67-66-3---------Chloroform I 10 III 

107-06-2 -------- 1,2-Dichloroethane 1 10 III 

78-93 -3 --------- 2-Butanone 1 10 III 

71-55 - 6 --------- 1,1,1 -Trichloroethane 1 10 III 

56-23 -5---------Carbon Tetrachloride I 10 III 

75-27-4 --------- Bromodichloromethane I 10 I V 

78-87-5 --------- 1,2-Dichloropropane 1 10 III 

10061-01-5 ------ cis-1,3 -Dichloropropane 1 10 III 

79-01-6 --------- Trichloroethene I 10 1 U 

124-48-1 -------- Dibromochloromethane I 10 I V 

79-00 - 5 --------- 1,1,2-Trichloroethane I 10 III 

71-43-2---------Benzene I 10 III 

10061 -02-6 ------ trans -1,3-D chloropropena I 10 IU 

75-25-2 --------- Bromoform 1 10 III 

108-10-1 -------- 4-Methyl-2 -Pentanone I 10 III 

591-78-6 -------- 2-Hexanone 1 10 III 

127-18 -4 -------- Tetrachloroethene 1 10 Iv 

79-34-5 --------- 1,1,2,2-Tetrachloroethana I 10 IU 

108-88-3------- -Toluene 1 10 IU 

108-90 -7 -------- Chlorobenzene 1 10 III 

100-41-4 -------- Ethylbenzene 1 10 III 

100-42-5--------Styrene 1 10 IU 

1330-20-7 ----- --Xylene ( total) 

1 

10 III 

FORM I VOA 

I 

I- 

3/90

is EPX ^saelT^MO 


TENTATIVELY IDENTIFIED COMPOUNDS 

Lab Name: TMA/ARLI Contract: NBC 

I 807Q94 

Lab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: Imo_ 

Matrix: ( soil/water) SOIL Lab Sample ID: A212047-02A 

Sample wt/vol: 5.0 (g/mL) G Lab File ID: 2122IR04 

Level: (low/med) LO _ Date Received: 12/14/92 

3 Moisture: not dec. _4 Date Analyzed: 12/21/92 


Soil Extract Volume: (uL) Soil Aliquot Volume: _(UL) 


Number TICS found: _ 1 (ug/L or ug/Kg) UG/KG 

I 

I I 

I I I 

CAS NUMBER 

I COMPOUND NAME I RT 

I EST. CONC. I Q 

Is:saaaas=aaasasa I sasaaaams:siss¢s:vss:s:::seas l a:::s:ss I asaasam:sssm I maa I 

1. 

(UNKNOWN ALKANE I 16.58 I 5 IJ I 

I 

i I 

I I I 

FORM I VOA-TIC 3/90 

I

2A 


000009 


I I 

I B07Q95 

Lab Name: TMA/ARLI Contract: WHC I I 

Lab Code: TMhLA _ Case No.: 12047 SAS No.: NA SDG No.: KA 

Matrix: (soil/water) SOIL 

Sample wt/vol: 5.0 (g/mL) G 

Level: (low/mad) LOW 

4 Moisture: not dec. 5 

GC Column: PACK ID: 2.00 (mm) 

Soil Extract Volume: (uL) 


Lab Sample ID: 

Lab File ID: 

Date Received: 

Date Analyzed: 

Dilution Factor: 1.0 

Soil Aliquot Volume: (uL) 


(ug/L or ug/Kg) QCs (t 

I I 

74-87-3 --------- Chloromethane I 

li IU 

74-83-9 --------- Bromomethane I 11 III 

75-01-4---------Vinyl Chloride I 11 1U 

75-00-3 --------- Chlorcethane I 11 IV 

75-09-2---------Methylene Chloride I 3 IJ 

67-64-1---------Acetone I 24 IB 

75-15-0---------Carbon Disulfide I 11 III 

75-35-4 --------- 1,1-Dichloroethens I li IU 

75-34-3 --------- 1,1-Dichloroethane I 11 III 

540-59-0 -------- 1,2-Dichloroethene (total) _I li IV 

67-66-3---------Chloroform I 11 IU 

107-06-2 -------- 1,2-Dichloroethane i 11 IV 

78-93-3 --------- 2-Butanone I 11 III 

71-55-6 --------- 1, 1, 1-Trichloroethane I 11 1 

56-23-5---------Carbon Tetrachloride I 11 IU 

75-27-4 --------- Bromodichloromethane I 11 IU 

78-87-5 --------- 1,2-Dichloropropane i it III 

10061-01-5 ------ cis-1,3-Dichloropropens I 11 IU 

79-01-6 --------- Trichloroethene I 11 IU 

124-48- 1 -------- Dibromochloromethane I li IV 

79-00-5 --------- 1,1,2-Trichloroethane I 11 IU 

71-43-2---------Benzene I it IV 

10061-02-6 ------ trans-1,3-D chloropropene I it IU 

75-25-2 --------- Bromoform I 11 IV 

108-10-1 -------- 4-Methyl-2-Pentanone I 11 IU 

591-78-6 -------- 2-Hexanone I 11 IU 

127-18-4 -------- Tetrachlorcethene I 11 I 

79-34-5 --------- 1,1,2,2-Tetrachloroethans I 11 IU 

108-88-3--------Toluene I 11 IV 

108-90-7 -------- Chlorobenzens I li IV 

100-41-4 -------- Ethylbenzene 1 11 IV 

100-42-5--------Styrene I 11 IU 

1330-20-7 ------- Xvlene (total) 1 11 IV 

FORM I VOA 

3/90

Lab Name: TMA/ARLI 

Lab Code: THAj A _ Case No.: 12047 



Level: (low/med) LOW_ 

t Moisture % not dec. r5 

GC Column: pACR ID: 2.00 (mm) 


I 

I 

1E 



Number TICS found: _0 

Contract: WHC I 

000010 


B07Q9S 

SAS No.: NA SDG No.: NA - 


Lab File ID: 2122IR09 

Date Received: 12/14/92 

Date Analyzed: 12/21/92 

Dilution Factor: 

1.0 

Soil Aliquot Volume: (UL) 


(ug/L or ug/Kg) UG/KG 

CAS NUMBER COMPOUND NAME 

EST. CONC. I Q I 

a^ssssaaamssa:â RT ai8ial i t I 

FORM I VOA-TIC 

I I 

3/90

IA 

VOLhTILE ORGANICS ANALYSIS DATA SHEET 

EPA`" ;. 

I 

I 

I B07Q96 I 


Lab Code: THMA_ Case No.: 12047 SAS No.: NA SDG No.: Imo_ 

Matrix: (soil/eater) SOIL Lab Sample ID: A212047-06A 

Sample wt/vol: 5.0 (g/mL) Q— Lab File ID: 21221810 

Level: (low/coed) jet_ Date Received: 12/14/92 

3 Moisture: not dec. _ 4 Date Analyzed: 12/21/92 




CAS NO. COMPOUND (ug/L or ug/Kg) JZG/KG Q 

74-87-3 --------- Chlor 

74-83-9 --------- Bromo: 

75-01-4---------Vinyl 

75-09-2---------Methylene Chloride 

67-64-1---------Acetone 

75-15-0---------Carbon Disulfide 

75-35-4 --------- 1,1-Dichloroethene 

75-34-3 --------- 1,1-Dichloroethane 

540-59-0 -------- 1,2-Dichloroethene (total) 

67-66-3---------Chloroform 

107-06-2 -------- 1,2-Dichloroethane 

78-93-3 --------- 2-Butanone 

71-55-6 --------- 1,1,1-Trichloroethane 

56-23-5---------Carbon Tetrachloride 

75-27-4 --------- Bromodichloromethans 

78-87-5 --------- 1,2-Dichloropropane 

10061-01-5 ------ cis-1,3-Dichloropropene 

124-48-1 -------- Dibromochloromethane 


71-43-2---------Benzene 

10061-02-6 ------ trans-1,3-D chloropropene 

75-25-2 --------- Bromoform 

108-10-1 -------- 4-Methyl-2-Pentanons 

591-78-6 -------- 2-Hexanone 

127-18-4 -------- Tetrachloroethene 

79-34-5 --------- 1,1,2,2-Tetrachloroethane 

108-88-3--------Toluene 

108-90-7 -------- Chlorobenzene 

100-41-4 -------- Ethylbenzens 

100-42-5--------Styrene 

1330-20-7 ------- Xylene (total) 

FORM I VOA 

I 

10 III 

10 III 

10 III 

10 IV 

3 IJ 

19 IS 

10 IU 

10 IU 

10 IV 

10 III 

10 IV 

10 III 

10 III 

10 IV 

10 III_ IU 

10 IU 

10 IU 

10 IV 

10 IU 

10 IU 

10 IV 

10 III 

10 III 

10 IU 

10 IV 

10 IU 

10 III 

10 IV 

10 IU 

10 IV 

10 IU 

10 IV 

I- 

3/90


000012 

is EPA SAMPLE NO. 


TENTATIVELY IDENTIFIED COMPOUNDS i i 

Lab Code: TRAL_ Case NO.: 12047 

Matrix: (soil/water) ,SOIL 


Level: ( low/med) LO 

% Moisture: not dec. _ 4 

GC Column: PACK ID: 2400 (mm) 


Number TICS found: 0 

I I 

CAS NUMBER I COMPOUND NAME 

Isssaszsassaaasssl sss^sssssssasasssassss 

I I 

I B07Q96 


SAS No.: NA SDG NO.: Imo_ 


Lab File ID: 21221RIO 




Soil Aliquot Volume: —(UL) 



I 

I RT 

I 

I EST. CONC. 

I I 

I Q 

I ssssasssl ssssaassssaas I asses I 

I 

I I 


I

lA 


Lab File ID: 21221R17 



Dilution Factor! 1.0 




000023 


907498 

Lab Name: TMA/ARLI Contract: WHC 

Lab Code: TMALA Case No.: 12047 SAS No.: NA SDO No.: N_ 

_ 




Level: (low/mod) LOW 

t Moisture: not dec. _ 4 


Soil Extract Volume: (UL) 



I 

I 

10 JU 

74-83-9 --------- Bromomethane 10 IV 

75-01-4---------Vinyl Chloride 10 III 

75-00-3 --------- Chloroethane 10 IV 

75-09-2---------Methylene Chloride 2. IJ 

67-64-1---------Acetone 17 IB 

75-15-0---------Carbon D sulf de 10 IV 

75-35-4 --------- 1,1-Dichloroethene 10 IU 

75-34-3 --------- 1,1-Dichloroethane 10 IU 

540-59-0 -------- 1,2-Dichloroethene (total)_) 10 JU 

67-66-3---------Chloroform 10 JU 

107-06-2 -------- 1,2-Dichloroethane 10 JU 

78-93-3 --------- 2-Butanone 10 IU 

71-55-6 --------- 1,1,1-Trichloroethane 10 IU 

56-23-5---------Carbon Tetrachloride 10 IU 

75-27-4 --------- Bromodichloromethane I 10 JU 

78-87-5 --------- 1,2-Dichloropropane 1 10 JU 

10061-01-5 ------ cis-1,3-Dichloropropene 1 10 JU 

79-01-6 --------- Trichloroethene I 10 IU 

124-48-1 -------- Dibromochloromethane 1 10 IU 

79-00-5 --------- 1,1,2-Trichloroethans 1. 10 IV 

71-43-2---------Benzene 1 10 JU 

10061-02-6 ------ trans-1,3-D chloropropene 10 JU 

75-25-2 --------- Bromoform 1 10 IU 

108-10-1 -------- 4-Methyl-2-Pentanone 1 10 IV - 

591-78-6 -------- 2-Hexanone 10 JU 

127-18-4 -------- Tetrachloroethene 10 JU 

79-34-5 --------- 1,1,2,2-Tetrachloroothane I 10 JU 

108-88-3--------Toluene 1 10 JU 

108-90-7 -------- Chlorobenzene 1 10 IU 

100-41-4 -------- Ethylbenzene 1 10 JU 

100-42-5--------Styrene 10 JU 

1330-20-7 ------ -XViene (total) 1 10 IV 

FORM I VOA 

3/90


lE 



Lab Code: TMALA Case No.: 12047 


Sample wt/vol: 5.0 (g/mL) Q 

Level: ( low/mad) IAw_ 




I 


Contract: WHC 

000014 


B07Q9$ 

SAS No.: NA SDG No.: NA 







2ONCENTRATION UNITS: 

(ug/L or ug/Rg) UG/XG 

I I 

I 

I 

CAS NUMBER 

COMPOUND NAME 

RT EST. CONC. I Q 

Ias+aââaass:s:s' ^^^âssâas^ss^s^s^^sa^^:was I ssats^^sa I saasaâ^sssss I ^^â^ 

FORM I VOA-TIC 3/90

000015 

IA EPA SA PLE NO. 


Lab Name: TWA= Contract: WHC 

B07Q99 

Lab Code: TMALA,_ Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 5.0 (g/mL) Q_ 

Level: (low/zed) LOW 

i Moisture: not dec. _4. 



Lab File ID: 21221811 






CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 

74-87-3 --------- Chloromethane 1 

1 

1 

10 III 

74-83-9 --------- Bromomethane 1 10 1II 

75-01-4---------Vinyl Chloride 1 10 III 

75-00-3 --------- Chloroethane 1 10 1II 

75-09-2---------Methylene Chloride 1 3 IJ 

67- 64- 1---------Acetone 1 27 IB 

75-15-0---------Carbon D sulf de I 10 IU 

75-35-4 --------- 1,1-Dichloroethane i 10 III 

75-34-3 --------- 1,1-Dichloroethane ( 10 1II 

540-59-0 -------- 1,2-Dichloroethane (total)_1 10 1U 

67-66-3---------Chloroform 1 10 III 

107-06-2 -------- 1,2-Dichloroethane 1 10 IV 

78-93-3 --------- 2-Butanone 1 10 1D 

71-55-6 --------- 1,1,1-Trichloroethans 1 10 1U 

1 56-23-5---------Carbon Tetrachloride I 10 IV 

1 75-27-4 --------- Bromodichloromethane 1 10 1 t 

1 78-87-5 --------- 1,2-Dichloropropans 1 10 1Q 

1 10061-01-5 ------ cis-1,3-Dichloropropene 1 10 III 

179-01-6 --------- Trichloroethene 1 10 1II 

1 124-48-1 -------- Dibromochloromethane I 10 IV 

1 79-00-5 --------- 1,1,2-Trichloroethane 1 10 III 

1 71-43-2---------Benzene 1 10 1U 

1 10061-02-6 ------ trans-1,3-D chloropropene I 10 III 

175-25-2 --------- Bromoform 1 10 III 

1 108-10-1 -------- 4-Methyl-2-Pentanone 1 10 IV 

1 591-78-6 -------- 2-Hexanone 1 10 IV 

1 127-18- 4 -------- Tetrachloroethene I 10 IV 

1 79-34-5 --------- 1,1,2,2-Tetrachloroethane I 10 1U 

1 108-88-3--------Toluene 1 10 1U 

1 108-90-7 -------- Chlorobenzene 1 10 IU 

1 100-41-4 -------- Ethylbenzene 1 10 III 

1 100-42-5--------Styrene 1 10 IV 

1330-20-7 ------- Xylene (total) 1 10 1U 

FORM I VOA 3/90

000016 




I 807Q99 


Lab Code: THALA_ Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 5.0 (g/mL) G Lab File ID: 21221R11 

Level: (low/med) IQK_ Date Received: 12/14/92 

t Moisture: not dec. _4 Date Analyzed: 12/21/92 

GC Column: PACK ID: 2.00 (ma) Dilution Factor: 1.0 

Soil Extract Volumes (uL) Soil Aliquot Volume: (uL) 


Number TICS found: 0 (ug/L or ug/Kg) UG/KG 

I 

I CAS NUMBER COMPOUND NAME I RT I EST. CONC. I Q 

FORK I VOA-TIC 3/90 

I

1A 


00001 7 


I 

I 


I B07QBO 

I 

I 

I 

Lab Code: TMALN Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 5.0 (q/mL) G_ 

Level: (low/med) LOW 

t Moisture: not dec. _3 







Soil Extract Volume% (uL) Soil Aliquot Volume: (UL) 


CAS NO. COMPOUND (uq/L or uq/Kq) UG/KG Q 


I 

I 

10 IU 


75-01-4---------Vinyl Chloride I 10 III 

75-00-3 --------- Chloroethane 1 10 III 

75-09-2---------Methylene Chloride 1 9 11 

67-64-1---------Acetone I 35 IS 

75-15-0---------Carbon Disulfide I 10 1 L 

75-35-4 --------- 1,1-Dichloroethens 1 10 III 

75-34-3 --------- 1,1-Dichloroethane I 10 IU 

540-59-0 -------- 1,2-Dichloroethene (total)_1 10 III 


107-06-2 -------- 1,2-Dichloroethane I 10 III 

78-93-3 --------- 2-Butanone I 10 ID 

71-55-6 --------- 1,1,1-Trichloroethens 1 10 IU 

56-23-5---------Carbon Tetrachloride 1 10 1U 

75-27- 4 --------- Bromodichloromethane 1 10 III 

78-87-5 --------- 1,2-Dichloropropene 1 10 III 

10061-01-5 ------ cis-1,3-Dichloropropene 1 10 IU 

79-01-6 --------- Trichloroethene I 10 ID 

124-48-1 -------- Dibromochloromethane 1 10 III 


71-43-2---------Benzene I 10 III 

10061-02-6 ------ trans-1,3-D chloropropene I 10 IU 

75-25-2 --------- Bromoform I 10 III 

108-10-1 -------- 4-Methyl-2-Pentanone i 10 IU 

591-78-6 -------- 2-Hexanone 1 10 III 

127-18-4 -------- Tetrachloroethene 1 10 III 

79-34-5 --------- 1,1,2,2-Tetrachloroethene I 10 IV 

108-88-3--------Toluene I 10 In 

108-90-7 -------- Chlorobenzene I 10 III 

100-41-4 -------- Ethylbenzene I 10 IU 

100-42-5--------Styrene I 10 1U 

1330-20-7 ------- Xylene (total) I 10 III 

FORM I VOA 

3/90


lE 





Sample wt/vol: 5.0 (g/mL) Q— 


3 Moisture: not doe. 3 

GC Column: PACK ID: 2.00 (nn) 



I I 

I B07QBO I 

Contract: WHC I I 




Date Received: 12LIA/92 






CAS NUMBER I COMPOUND NAME I RT EST. CONC. I Q I 

1. (UNKNOWN ALKANE i 16.53 5 IJ I 

n 

I I I I 


I 

I

111 



EPA ^°°L° 1f0. 

B07QB1 

Lab Code: TMA1A Case No.: 12047 SAS No.: NA SDG No.: NA 

Matrix: ( soil/water) ;SOIL Lab Sample ID: A212047-04A 

Sample wt/vol: 5.0 ( q/mL) Q Lab File ID: 21221R0S 

Level: ( low/mad) LOW Date Received: 2/li/92 

t Moisture: not dec. 3 Date Analyzed: 12/21/92 


Soil Extract Volume: (UL) Soil Aliquot Volume: (uL) 

I 


CAS NO. COMPOUND ( uq/L or uq/Kq) UG/KG Q 

I 

I I 

74-87-3 --------- Chloromethane 1 10 IU_ 

1 

74-83 -9 --------- Bromomethane ( 10 IU 1 

75-01-4-------- -Vinyl Chloride j 10 1 U I 

75-00-3 --------- Chloroethane I 10 I U 1 

75-09-2-------- -Methylene Chloride 1 10 IJ 1 

67-64-1---------Acetone I 25 I S 1 

75-15-0---------Carbon Disulfide j 10 IU 1 

75-35-4 --------- 1,1-Dichloroethens 1 10 III 1 

75 -34 - 3 --------- 1,1 -Dichloroethane 1 10 IU 1 

540-59-0 -------- 1,2-Dichloroethens (total)— j 10 I II 1 

67-66-3---------Chloroform 1 10 jU 1 

107-06-2 -------- 1,2-Dichloroethane 1 10 jU 1 

78-93-3 --------- 2-Butanone 1 10 jU 1 

71-55-6 --------- 1,1,1-Trichloroethane 1 10 jU 1 

56-23 - 5---------Carbon Tetrachloride I 10 jU 1 

75-27-4 --------- Bromodichloromethane 1 10 IU 1 

78-87-5 --------- 1,2-Dichloropropane 1 10 jU 1 

10061 -01 -5 ------ cis-1,3 -Dichloropropene 1 10 jU 1 

79 -01-6 --------- Trichloroethene 1 10 jU 1 

124 -48 - 1 -------- Dibromochloromethane 1 10 jU 1 

79-00-5 --------- 1,1,2-Trichloroethane j 10 jU 1 

71-43-2-------- -Benzene 1 10 IU 1 

10061- 02 -6 ------trans -1,3 -D chloropropene 1 10 jU j 

75-25-2 --------- Bromoform 1 10 I U I 

108-10-1 -------- 4-Methyl-2 -Pentanone 1 10 jU I 

591-78-6 -------- 2-Hexanone 1 10 jU 1 

127-18-4 -------- Tetrachloroethene 1 10 jU 1 

79-34-5 --------- 1,1,2,2-Tetrachloroethana 1 10 jU I 

108-88-3------- -Toluene 1 10 jU I 

108-90-7 -------- Chlorobenzene I 10 jU I 

100-41-4 -------- Ethylbenzene 1 10 j U I 

100-42-5--------Styrene j 10 III I 

1330-20 -7 ------- Xylene ( total) 

FORM I VOA 

j 

I 

10 

1U I 

I i 

3/90

Lab Name: 

1E 

VOLATILE ORGANICS ANALYSIS 

TENTATIVELY IDENTIFIED 

Lab Code: TMAL8_ Case No.: 12047 


Sample wt/vol: 5.0 ( g/mL) 

Level: (low/med) IDJL_ 

% Moisture: not dec. _3 




DATA SHEET 

000020 


COMPOUNDS I I 

B07QB1 i 

Contract: WHC _- I I 


Lab Sample ID: x212047-04A 

s^ Lab File ID: 2122IR08 







I I I 

CAS NUMBER I COMPOUND NAMEI RT 

Issss:ss:aassssss I a:mss::ss:ssss:::asssasssasss I sssss:ss 

I 1. (UNKNOWN ALKANE I 16.58 

I I 


6- IJ i 

I I 

FORM I VOA-TIC 3/90

1A 


Lab Name: TMA/ARLI Contract: jHQ__ I 

000021 


I B07QB2 

Lab Code: TMALA _ Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 5.0 (VRL) G 





Lab File ID: 






CAS NO. COMPOUND (ug/L or ug/Kg) UG1KG Q 


I 

i 

10 IU 

74-83-9 --------- Bromomethane I 10 IU 

75-01-4---------Vinyl Chloride I 10 IU 

75-00-3 --------- Chloroethane I 10 IU 

75-09-2---------Methylene Chloride I 4 IJ 

67-64-1---------Acetone I 27 IB 

75-15-0---------Carbon Disulfide I 10 IV 

75-35-4 --------- 1,1-Dichloroethene i 10 IV 

75- 34-3 --------- 1,1-Dichloroethene I 10 IU 

540-59-0 -------- 1,2-Dichloroethene (total) _I 10 III 


107-06-2 -------- 1,2-Dichloroethene I 10 IV 

78-93-3 --------- 2-BUtanone I 10 IU 


56-23-5---------Carbon Tetrachloride I 10 IU 

75-27-4 --------- Bromodichloromethane I 10 IU 

78-87-5 --------- 1,2-Dichloropropane I 10 IU 

10061-01-5 ------ cis-1,3-Dichloropropene I 10 III 

79-01-6 --------- Trichloroethane I 10 IU 

124-48-1 -------- Dibromochloromethane I 10 IU 


71-43-2---------Benzene I 10 IV 

10061-02-6 ------ trans-1,3-D chloropropene i 10 III 

75-25-2 --------- Bromoform I 10 IU 

108-10-1 -------- 4-Methyl-2-Pentanone I 10 IU 

591-78-6 -------- 2-Hexanone I 10 IU 

127-18-4 -------- Tetrachloroethene I 10 IU 

79-34-5 --------- 1,1,2,2-Tetrachloroethane I 10 IU 

108-88-3--------Toluene I 10 IV 

108-90-7 -------- Chlorobenzene I 10 IU 

100-41-4 -------- Ethylbenzene I 10 IU 

100-42-5--------Styrene I 10 IU 

1330-20-7 ------ -Xylene (total) I 10 IU 

FORM I VOA 

3/90 

•

000022 

1E EPA SAMPLE No. 



B074B2 

Lab Name: Contract: WHC 



Sample wt/vol: 5.0 (q/ML) G_ 

Level: ( low/mod) LOW 

i Moisture: not dec. _4 

GC Column: PACK ID: --Z.L.0 (mm) 



SAS No.: H SDG No.: jib_ 








( ug/L or uq/Kq) UG/KG 

I 

CAS NUMBER I COMPOUND NAME I RT I EST. CONC. R I 

:::^:s::ms:asas: I =asssaâ:a:sas:::::s:aa^::: I ^^sssaâ i ^âs^â ssa::I 


I

000023 

1A EPA SAMPLE NO. 


I ( 

B07QB3 I 


Lab Code: THALA_ Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 5.0 (q/mL) G 


% Moisture: not doe. _ 7 



Lab File ID: 




Soil Extract Volume: (uL) Soil Aliquot Volume: —(UL) 


CAS No. COMPOUND (uq/L or uq/Kq) UG/KG 

I 

74-87-3 --------- Chloromethane I 12 

74-83-9 --------- Bromomethane 1 12 

75-01-4---------Vinyl Chloride 1 12 

75-00-3 --------- Chloroethane I 12 

75-09-2---------Methylene Chlor de I 9 

67-64-1---------Acetone I 44 

75-15-0---------Carbon D sulf de I 12 

75-35-4 --------- 1,1-Dichloroethens 1 12 

75-34-3 --------- 1,1-Dichloroethane I 12 

540-59-0 -------- 1,2-Dichloroethens (total)_I 12 

67-66-3---------Chloroform I 12 

107-06-2 -------- 1,2-Dichloroethane I 12 

78-93-3 --------- 2-Butanone 1 12 

71-55-6 --------- 1,1,1-Trichloroethane 1 12 

56-23-5---------Carbon Tetrachloride I 12 

75-27-4 --------- Bromodichloromethane I 12 

78-87-5 --------- 1,2-Dichloropropane I 12 

10061-01-5 ------ cis-1,3-Dichloropropane I 12 

79-01-6 --------- Trichloroethens I 12 

124-48-1 -------- Dibromochloromethane 1 12 

79-00-5 --------- 1,1,2-Trichloroathane I 12 

71-43-2---------Benzene 1 12 

10061-02-6 ------ trans-1,3-D chloropropene 1 12 

75-25-2 --------- Bromoform 1 12 

108-10-1 -------- 4-Methyl-2-Pentanone I 12 

591-78-6 -------- 2-Hexanone I 12 

127-18-4 -------- Tetrachloroethene I 12 

79-34-5 --------- 1,1,2,2-Tatrachloroethane 1 12 

108-88-3--------Toluene 1 12 

108-90-7 -------- Chlorobenzene I 12 

100-41-4 -------- Ethylbenzene 1 12 

100-42-5--------Styrene 1 12 

1 1330-20- 7 ------- Xylene (total) 1 12 

FORM I VOA 

6 

3/90

Lab Name: 

Lab Code: TMATA 

lE 




Case No.: 12047 

Sample wt/vol: 5.0 (g/mL) 

Level: (low/mad) LDS_ 




Number TICs found: _Q 

DATA SHEET 

COMPOUNDS I 

000024'0 


I B07QB3 

Contract: WHC I i 

SAS No.: IA 

SDG No.: NA— 


SL_ Lab File ID: 21221213 







CAS NUMBER COMPOUND NAME I RT I EST. CONC. I Q I 

Issass:zxssaaaaas I asmsssssassssasssssassasssss I sss^sss I assssssasssss 

I 

I 

I 


I 

I sasssl 

I f 

3/90

000025 

IA 



I I 

I B07QBB i 











74-83-9 --------- Bromomethans 


75-00-3 --------- Chloroethane 

75-09-2---------Methylene Chlor de 

67-64-1---------Acetone 

75-15-0---------Carbon D sulf ids 

175-35-4 --------- 1,1-Dichloroethens 

75-34-3 --------- 1,1-Dichloroethans 

1 540-59-0 -------- 1,2-Dichloroethene (total)! 

1 67-66-3---------Chloroform 


1 78-93-3 --------- 2-Butanons 

1 71-55-6 --------- 1,1,1-Trichloroethans 


1 75-27-4 --------- Bromodichloromethane 

1 78-87-5 --------- 1,2-Dichloropropane 

1 10061-01-5 ------ cis-1,3-Dichloropropene 

79-01-6 --------- Trichloroethene 

1 124-48-1 -------- Dibromochloromethane 

179-00-5 --------- 1,1,2-Trichloroethans 

1 71-43-2---------Benzene 

1 10061-02-6 ------ trans-1,3-D chloropropene 

1 75-25-2 --------- Bromoform 

1 108-10-1 -------- 4-Methyl-2-Pentanons 

1 591-78-6 -------- 2-Hexanone 

1 127-18-4 -------- Tetrachloroathene 

1 79-34-5 --------- 1,1,2,2-Tetrachloroethane 

1 108-88-3--------Toluene 

1 


1 100-41-4 -------- Ethylbenzene 

1 100-42-5--------Styrene 

1 1330-20-7 ------- Xylene (total) 

FORM I VOA 


Lab File ID: 

21221R14 




Soil Aliquot Volume: 


(ug/L or ug/Kg) UG/KG G 

I 

I 

11 1U 

11 III 

11 IU 

11 IU 

6 IJ 

23 IB 

it IU 

11 IU 

11 III 

11 IU 

11 IU 

11 IU 

11 IU 

it IU 

it IU 

it IU 

11 IU 

11 IU 

11• III 

11 III 

11 IU 

11 IU 

it IU 

11 lu - 

ll 1U 

11 III 

11 1U 

11 1U 

11 1U 

11 III 

11 1U 

11 1U 

11 1 

(UL) 

3/90

Lab Name: 

is 



000026 


► B07QBS 

► 

I 


Matrix: (soil/water) SOIL ~^ 


Level: (low/mod) L40W 




Number TICs found: 0 

I 

► CAS NUMBER 

I I 

► COMPOUND NAME ► 

Contract: WHC ► I 


Lab Sample ID: x212047-10A 

s'^ Lab File ID: 2122IR14 






(ug/L or ug/Kg) y_G/KG 

RT EST. CONC. Q I 

I 

I 

► iiiissisisisisiilsiasisiiiisasiiiisiiiiiaaii ► iiiiliii ► iiiiisssiivsliiiisl 


I 

I 

3/90

IA 


Lab Name: TNA/ARLI Contract: WHC_ 

Lab Code: TMALA_ Case No.: 12047 4s 







( 

I 

000027 


B07QB9 



Lab File ID: 21221 ,E 


Date Analyzed: 12/21/92 1/92 


soil Aliquot Volume: (UL) 


CAS NO. COMPOUND (ug/L or ug/Kg) UQ KG 


74-83-9 --------- Bromomethane I 10 

75-01-4---------Vinyl Chloride I 10 

75-00-3 --------- Chloroethane I 10 

75-09-2---------Methylene Chlor de I 6- 

67-64-1---------Acetone I 22 

75-15-0---------Carbon D Sulf de I 10 

75-35-4 --------- 1,1-Dichloroethene ( 10 

75-34- 3 --------- 1,1-Dichloroethane I 10 

540-59-0 -------- 1,2-Dichloroethene (total) _I 

10 

67-66-3---------Chloroform I 10 

107-06-2 -------- 1,2-Dichloroethane I 10 

78-93-3 --------- 2-Butanone I 10 

71-55-6 --------- 1,1,1-Trichloroethans I 10 

56-23-5---------Carbon Tetrachloride I 10 

75-27-4 --------- Bromodichloromethans I 10 

78-87-5 --------- 1,2-Dichloropropane I 10 

10061-01-5 ------ cis-1,3-Dichloropropane I 10 

79-01-6 --------- Trichloroethene i 10 

124-48-1 -------- Dibromochloromethane I 10 

79-00-5 --------- 1,1,2-Trichloroethane I 10 

71-43-2---------Benzene I 10 

10061-02-6 ------ trans-1,3-D chloropropene I 10 

75-25-2 --------- Bromoform I 10 

108-10-1 -------- 4-Methyl-2-Pentanone I 10 

591-78-6 -------- 2-Hexanone i 10 

127-18-4 -------- Tetrachloroethene I 10 

79-34-5 --------- 1,1,2,2-Tetrachloroethane I 10 

108-88-3--------Toluene I 2- 

108-90-7 -------- Chlorobenzene I 10 

100-41- 4 -------- Ethylbenzene I 10 

100-42-5--------Styrene I 10 

1330-20-7 ------- Xylene (total) I 10 

FORM I VOA 

I 

10 

'S' 

3/90

Lab Name: 

Lab Code: TIhLA 

is 



Matrix: (soil/water) $OIL 

Case No.: 12047 

Sample wt/vol: 5.0 (g/mL) Q._ 

Level: (low/mad) IDE 

4 Moisture: not dec. 4 



Number TICs found: 0 








EPA SAMOPLB NO: S 

I B07QB9 


SAS No.: NA SDG No.: N_ 

Lab Sample ID: A212047-IIA 

CAS NUMBER ( COMPOUND NAME RT I EST. CONC. 

I 

Q I 

aaa::I 


I

lA 



Lab Code: TMALA Cass No.: 12047 








74-87-3 --------- Chloromethans 1 

0000: 


B07QC0 




Date Received: ,]2,/14/92 





(ug/L or ug/Kg) UQ/RG Q 

I i 

it III 

74-83-9 --------- Bromomethane I 11 I U I 

75-01-4---------Vinyl Chloride 1 it IU I 

75-00-3 --------- Chloroethans 1 11 III 1 

75-09-2---------Methylene Chloride 1 5 IJ I 

67-64-1---------Acetone i 28 18 1 

75-15-0---------Carbon Disulfide 1 11 1U 

75-35-4 --------- 1,1-Dichloroethene 1 11 III I 

75-34-3 --------- 1,1-Dichloroethane 1 11 III I 

540-59-0 -------- 1,2-Dichloroethene (total)_l 11 III I 

67-66-3---------Chloroform 1 11 1U I 

107-06-2 -------- 1,2-Dichloroethane 1 11 IU 

1 78-93-3 --------- 2-Butanons 1 11 I U I 

71-55-6 --------- 1,1,1-Trichloroethane 1 11 IU I 

1 56-23-5---------Carbon Tetrachloride I 11 III I 

1 75-27-4 --------- Bromodichloromethans I 11 IU 

1 78-87-5 --------- 1,2-Dichloropropans 1 11 IU I 

179-01-6 --------- Trichloroethene 1 li IU 

i 124-48-1 -------- Dibromochloromethane 1 

it IU 

1 10061-01-5 ------ cis-1,3-Dichloropropene 1 it I U I 

1 79-00-5 --------- 1,1,2-Trichloroethane I li III I 

1 71-43-2---------Benzene i 11 1 UI 

1 10061-02-6 ------ trans-1,3-D chloropropene 1 

1 

1 

it I U I 

1 75-25-2 --------- Bromoform 1 11 III I 

1 108-10-1 -------- 4-Methyl-2-Pentanone 1 11 IU 

1 591-78-6 -------- 2-Hexanone I 11 IU I 

1 127-18-4 -------- Tetrachloroethene I 11 I II I 

1 79-34-5 --------- 1,1,2,2-Tetrachloroethene 1 11 I UI 

1108-88-3--------Toluene 1 li IU 

1 108-90-7 -------- Chlorobenzene I 11 1II 

1 100-41-4 -------- Ethylbenzene 1 

it I UI 

1 100-42-5--------Styrene 1 11 I U 1 

1330-20-7 ------- Xylene (total) i 11 iU 

FORM I VOA 3/90

00003( 

lE EPA SAMPLE N0. 



B07QC0 

Lab Name: TMA/ARLi Contract: WHC 

Lab Code: TMALK_ Casa No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 5.0 (q/mL) Q__ 


% Moisture: not dec. 5 










(ug/L or ug/Kq) UG RG 

I I I I 

CAS NUMBER COMPOUND NAME I RT I EST. CONC. I Q 

I I I I 

FORM I VOA-TIC 3/90

1B 

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET 

Lab Name: TMAIARLI Contract: WHC I 

000031 


I 

I B07Q93 

Lab Code: =Lh_ Case No.: 12047 SAS No.: NA SDG No.: NA 

Matrix: (soil/water) 

Sample wt/vol: 

Level: (low/mad) 

% Moisture: 6 

Concentrated Extract 

Injection Volume: 

GPC Cleanup: (YIN) 

CAS NO. 

_ 30:_1 (9/ML) G 

LO 

decanted: (Y/N) NI_ 

Volume: 500.0 (uL) 

Y'_ 

2.0(uL) 

COMPOUND 

pH: _.7 

Lab Sample ID: A212047-01B 


Date Received: 12/14192 

Date Extracted: 12/21/92 





I i 

1 108-95-2--------Phenol 1 350 

1 111-44- 4 -------- bis(2-Chloroethyl)Ether 1 350 

195-57-8 --------- 2-Chlorophenol 1 350 

1 541-73-1 -------- 1,3-Dichlorobenzene 1 350 

1 106-46- 7 -------- 1,4-Dichlorobenzene I 350 

195-50-1 --------- 1,2-Dichlorobenzene I 350 

1 95-48-7 --------- 2-Methylphenol 1 350 

1 108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_I 350 

1 106-44-5 -------- 4-Methylphenol 1 350 

1 621-64- 7 -------- N-Nitroso-Di-n-Propylam ne_I 350 

1 67-72-1 --------- Hexachloroethane 1 350 

198-95-3---------Nitrobenzene i 350 

1 78-59-1 --------- Isophorone 1 350 

1 88-75-5 --------- 2-Nitrophenol 1 350 

105-67-9 -------- 2,4-Dimethylphenol 1 350 

1 111-91- 1 -------- bis(2-Chloroethoxy)Methane_1 350 

1 120-83- 2 -------- 2,4-Dichlorophenol 1 350 

1 120-82-1 -------- 1,2,4-Trichlorobenzene 1 350 

191-20-3---------Naphthalene I 350 

1 106-47- 8 -------- 4-Chloroanil ne 1 350 

1 87-68-3 --------- Hexachlorobutad ene 1 350 

1 59-50-7 --------- 4-Chloro-3-Methylphenol 1 350 

191-57-6 --------- 2-Methylnaphthalene 1 350 

1 77-47-4---------Hexachlorocyclopentad e — I 350 

188-06-2 --------- 2,4,6-Trichlorophenol I 350 


1 91-58-7 --------- 2-Chloronaphthalene 1 350 

188-74-4 --------- 2-Nitroaniline 1 850 

1 131-11- 3 -------- Dimethylphthalate 1 350 

i 208-96-8 -------- Acenaphthylene I 350 

199-09-2 --------- 3-Nitroaniline 1 850 

1 83-32-9 --------- Acenaphthene 1 350 

151-28-5 --------- 2,4-Dinitrophenol 1 850 

I UI 

IU I 

IU I 

IU I 

IU I 

IU I 

IU I 

IU I 

IU I 

IU I 

I UI 

I UI 

I II I 

I U I 

I U I 

I U I 

I U I 

I U I 

I U I 

I U I 

I U I 

I U I 

I U I 

I U I 

I U I 

I U I 

I U- I 

I U I 

3/90

lC 



EPA SAAM OPLE NO. 

I 

I 807Q93 

Lab Code: TMALA Case No.: 1,2047 SAS No.: NA SDG No.: NA 

_ 

Matrix: (soil/water) BOIL 


Sample wt/vol: 30.1 (g/mL) G Lab File ID: 21230510 

Level: (low/zed) LOW Date Received: 12/14/92 

% Moisture: 6 decanted: (YIN) iN Date Extracted: 12/21/92 

Concentrated Extract Volume: 500.0 (UL) 

Injection Volume: 2.0 (uL) 

GPC Cleanup: (YIN) Y pH: 7.7 


100-02-7 -------- 4-Nitrophenol 

132-64-9 -------- Dibenzofuran 

121-14-2 -------- 2,4-Dinitrotoluene 


84-66-2 --------- Diethylphthalate 

7005-72-3 ------- 4-Chlorophenyl-phenylether_ 

86 -73-7 --------- Fluorene 

100-01-6 -------- 4-Nitroan 1 ne 

534- 52-1 -------- 4,6-Dinitro-2-methylphenol_ 

86-30-6 --------- N-Nitrosodiphenylamine (1)i 

101-55-3 -------- 4-Bromophenvl-ohenvlether 

87-86-5 --------- Pentachlorophenol i 

85-01-8 --------- Phenanthrene 1 

120-12-7 -------- Anthracene I 

86-74-8 --------- Carbazole I 

84-74-2 --------- Di-n-BUtylphthalate I 

206-44-0 -------- Fluoranthene I 

129-00-0 -------- Pyrene I 

85-68-7 --------- BUtylbenzylphthalate I 

91-94-1 --------- 3,3'-Dichlorobenzidine I 

56-55-3 --------- Benzo(a)Anthracens I 

117-81-7 -------- bis(2-Ethylhexyl)Phthalate_I 

218-01-9 -------- Chrysene 1 

117-84-0 -------- Di-n-Octyl Phthalate 1 

205-99-2 -------- Benzo(b)Fluoranthene I 

207-08-9 -------- Benzo(k)Fluoranthens I 

50-32-8 --------- Benzo(a)Pyrene I 

193-39-5 -------- Indeno(1,2,3-cd)Pyrene I 

53-70-3 --------- Dibenz(a,h)Anthracene 1 

191-24-2 -------- Benzo(g,h,i)Perylens 

FORM I SV-2 




(ug/L or ug/Kg) UG/RG Q 

850 1U 1 

350 III 1 

350 III I 

350 IU 1 

350 III I 

350 IU 1 

350 IU 1 

850 1U 1 

850 IU 1 

350 IU 1 

350 1U I 

850 III 1 

350 III I 

350 IU 1 

350 III 1 

350 1U 

350 1U I 

350 1U 1 

350 III 1 

350 III 1 

350 III I 

350 1U I 

350 IU 1 

350 IU i 

350 IU 1 

350 III 

350 1U I 

350 III i 

350 U 

350 III I 

—1-1 

3/90


iF 


TENTATIVELY IDENTIFIED COMPOUNDS I ^ 



Sample wt/vol: 30.1 (g/mL) Q__ 

Level: ( low/mad) LOW_ 

t Moisture: _ 6 decanted: (Y/N)tN 

Concentrated Extract Volume % 500.0 (uL) 

Injection Volume: 2.0(UL) 

GPC Cleanup: (YIN) Y_ pH: 7.7 


CAS NUMBER COMPOUND NAME RT 

I 1. (UNKNOWN HYDROCARBON 

2• (UNKNOWN HYDROCARBON 6.68 

I 3. (UNKNOWN HYDROCARBON I 

7.37 

4 . (UNKNOWN ALCOHOL I 8.72 

I B07Q93 


SAS No.: NA 

000033 


SDG No.: N_ 


Lab File ID: 2123OS10 







EST. CONC. 

Q I 

W I 

J I 

W I 

BJ I I 

FORM I SV-TIC 3/90

is 

SEHIVOLATILE ORGANICS ANALYSIS DATA SHEET 

Lab Name: TMh(ARLI Contract: WHC 

Lab Code: ALA Case No.: 12047 

Matrix: (soil/water) BOIL 


Level: (low/med) 

% Moisture: _4 

decanted: (YIN) TN 

Concentrated Extract Volume: 500.0 (uL) 


GPC Cleanup: (YIN) y _ pH: 6.9 

00003 


B07Q94 

SAS No.: NA SDG No.: NA^_ 


Lab File ID: 



Date Analyzed: 12 /30/92 



CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 0 

I I 

1 108-95-2--------Phenol 1 340 

1 111-44-4 -------- bis(2-Chloroethyl)Ether 1 340 

1 95-57-8 --------- 2-Chlorophenol 1 340 

1 541-73-1 -------- 1,3-Dichlorobenzene i 340 

1 106-46-7 -------- 1,4-Dichlorobenzene I 340 

1 95-50-1 --------- 1,2-Dichlorobenzene i 340 

1 95-48-7 --------- 2-Methylphenol 1 340 

1108-60-1 -------- 2,2' -oxybis ( 1-Chloropropane)_I 340 

1 106-44 - 5 -------- 4-Methylphenol 1 340 

1 621-64-7 -------- N-Nitroso-Di-n-Propylam ne_I 340 

1 67-72-1 --------- Hexachloroethane 1 340 

i 98-95-3-------- -Nitrobenzene 1 340 

1 78-59-1 --------- Isophorone ( 340 

1 88-75 -5 --------- 2-Nitrophenol 1 340 

1 105-67-9 -------- 2,4-Dimethylphenol ( 340 

1 111-91-1 -------- bis(2-Chloroethoxy)Methane 

1 340 

1 120-83-2 -------- 2,4-Dichlorophenol r i 340 

1 120-82-1 -------- 1,2,4-Trichlorobenzene 1 340 

1 91-20-3---------Naphthalene 340 

1 

1 106-47-8 -------- 4-Chloroanil ne 340 

1 

1 87-68-3 --------- Hexachlorobutad ene 340 

1 

1 59-50-7 --------- 4-Chloro-3-Methylphenol I 340 

1 91-57-6 --------- 2-Methylnaphthalens 1 340 

1 77-47-4 --------- Hexachlorocyclopentad —ad a 

I 340 

1 88-06-2--- ------ 2,4,6-Trichlorophenol 1 340 

i 95-95-4 --------- 2,4,5-Trichlorophenol 820 

1 

1 91-58-7 --------- 2-Chloronaphthalene 340 

1 

1 88-74-4 --------- 2-Nitroaniline 820 

1 

1 131-11-3 -------- Dimethylphthalate 340 

1 

1 208-96-8 -------- Acenaphthylene 1 340 

1 99-09-2 --------- 3-Nitroaniline 820 

1 

1 83-32-9 --------- Acenaphthens 1 340 

1 51-28-5 --------- 2,4-Dinitrophenol 1 820 

IU I 

I II I 

IU I 

I UI 

III I 

I UI 

JU I 

III I 

JU I 

III I 

JU I 

IU I 

JU I 

IQ I 

I II I 

IU I 

JU I 

IU I 

IU I 

IU I 

JU I 

Iu I 

JU I 

J UI 

Iv I 

IU I 

IU I 

J UI 

I UI 

JU I 

3/90

1C 

SENIVOLATILE ORGANICS ANALYSIS DATA SHEET 


1 

000035 


i 807Q94 

Lab Code: TMALh Case No.: 12047 SAS No.: NA SDG No.: KA 

Matrix: (soil/water) Lab Sample ID: 



i Moisture: _4 decanted: (Y/N) 


Injection Volume: 2.0(uL) 

GPC Cleanup: (Y/N) Y pH: 6.9 


Lab File ID: 






(ug/L or ug/Kg) UG/KG Q- 

100-02-7 -------- 4-Nitrophenol 1 820 

132-64-9 -------- DibenzoPuran 1 340 1U 

121-14-2 -------- 2,4-Dinitrotoluene 1 340 III 

606-20-2 -------- 2,6- Dinitrotoluene 1 340 1U 

84-66-2 --------- Diethylphthalate 1 340 III 

7005-72-3 ------- 4-Chlorophenyl-phenylether_1 340 IU 

86-73-7 --------- Fluorene I 340 I V 

100-01-6 -------- 4-Nitroan 1 ne I 820 III 

534-52-1 -------- 4,6-Dinitro-2-methylphenol_1 820 1U 

86-30-6 --------- N-Nitrosodiphenylamine (1)- 1 340 1U 

101-55 -3 -------- 4 -Bromophenyl-phenylether 1 340 IU 

118-74-1 -------- Hexachlorobenzene 1 340 III 

87-86-5 --------- Pentachlorophenol 1 820 1U 

85-01 -8 --------- Phenanthrene 1 340 1U 

120-12-7 -------- Anthracene 1 340 IU 

86-74-8 --------- Carbazole 1 340 1U 

84 -74-2 --------- Di -n-BUtylphthalate 1 340 IU 

206-44 -0 -------- Fluoranthene 1 340 1U 

129 -00-0 ------- -Pyrene 1 340 1U 

85-68-7 ---------Butylbenzylphthalate 1 340 1U 

91-94-1 --------- 3,3'-Dichlorobenzidine I 340 III 

56-55-3 --------- Benzo(a)Anthracene 1 340 IU 

117 -81-7 -------- bis(2 -Ethylhexyl)Phthalate— I 340 1U 

218 -01-9 ------ --Chrysens 1 340 1U 

117 -84 -0 ------ --Di -n-Octyl Phthalate 1 340 IU 

205 -99 -2 -------- Benzo(b)Fluoranthene 1 340 IU 

207-08-9 -------- Benzo(k)Fluoranthene I 340 III 

50-32-8 --------- Benzo(a)Pyrene 1 340 IU 

193-39-5 -------- Indeno(1,2,3-cd)Pyrene 1 340 JU 

53-70-3 --------- Dibenz(a,h)Anthracens 1 340 IU 

191-24-2 -------- Benzo(g,h,i)Perylene 1 340 IU 

"II - Cannot he separated from ninhenvlamine 

FORM I SV-2 

1 

1 

IV 

3/90 

^

IF EPA SWAOR i 


TENTATIVELY IDENTIFIED COMPOUNDS I I 

I B07Q94 

Lab Name: TMAIARLI Contract: WHC 1 I 


Matrix: (soil/water) SOIL Lab Sample ID: A212047-02B 

Sample wt/vol: 30.5 (q/mL) Q_ Lab File ID: 2123OS13 

Level: (low/mad) ID Date Received: 12/14/92 

% Moisture: 4 decanted: (Y/N)Imo_ Date Extracted: 12121/92 

Concentrated Extract Volume: 500.0 (UL) Date Analyzed: 12/30/92 

Injection Volume: _ 2,O(UL) Dilution Factor: 1.0 

GPC Cleanup: (YIN) Y_ PRO 6.9 


Number TICS found: _3 (ug/L or ug/Kg) UG/KG 

CAS NUMBER 

1. 

2. 

3. 

COMPOUND NAME I 

I I 

RT I EST. CONC. 

I I 

I Q I 

^âa::aaa::saa:sa:^^â^sa: I s::as:::Iva:a:aaass^K I a^^ss I 

SUBST. BENZENE 1 6.42 i 100 IJ 1 

UNKNOWN HYDROCARBON 1 7.37 1 1400 IBJ I 

UNKNOWN ALCOHOL 1 8.72 I 

240 1 BJ I 

1-1 

1-1 

FORM I SV-TIC 3/90

000037 

18 SPA SAMPLE NO. 



Lab Code: TMALA Case No.: 1 047 

Contract: WHC 

SAS No.: NA 

B07Q95 

SDG No.: N_ 


Sample wt/vol: 30.5 ( g/mL) Q_ Lab File ID: 

Level: (low/med) Date Received: 

t Moisture: _ 5 decanted: (YIN) N Date Extracted: 12/21/92 


Injection Volume: _ 2.0(uL) Dilution Factor: 1.0 



CAS NO. COMPOUND (ug/L or ug/Kg) 9Q/KG Q 

108-95-2--------Phenol 

111-44-4 -------- bis(2-Chloroathyl)Ether 

95-57-8 --------- 2-Chlorophenol 

541-73-1 -------- 1,3-Dichlorobenzene 


95-50-1---------1,2-Dichlorobenzene 

95-48-7---------2-Methylphenol 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_1 

106-44- 5 -------- 4-Methylphenol 1 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne_1 

67-72-1 --------- Hexachloroethane 

98-95-3---------Nitrobenzene 

78-59-1 --------- Isophorone 

88-75-5 --------- 2-Nitrophenol 

105-67-9 -------- 2,4-Dimethylphenol 

111-91-1 -------- bis(2-Chloroethoxy)Methane,l 

120-83-2 -------- 2,4-Dichlorophenol 

120-82-1 -------- 1,2,4-Trichlorobenzene 

91-20-3---------Naphthalene I 

87-68-3 --------- Hexachlorobutadiene 

59-50-7 --------- 4-Chloro-3-Methylphenol 

91-57-6 --------- 2-Methylnaphthalene 

77-47-4 --------- Hexachlorocyclopentad — ene 

88-06-2 --------- 2,4,6-Trichlorophenol 


91-58-7 --------- 2-Chloronaphthalene 

88-74-4 --------- 2-Nitroaniline 

131-11-3 -------- Dimethylphthalate 

208-96-8 -------- Acenaphthylene 

99-09-2 --------- 3-Nitroaniline 

83-32-9 --------- Acenaphthene 

51-28-5 --------- 2,4-Dinitrophenol 

FORM I SV-1 

340 III 

340 IU 

340 JU 

340 III 

340 JU 

340 JU 

340 JU 

340 IU 

340 JU 

340 JU 

340 JU 

340 JU 

340 IU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 IV 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 1 

340 JU 1 

830 IU 1 

340 JU 1 

830 JU 1 

340 J U 1 

340 J U 1 

830 JU 1 

340 III 1 

830 III I 

3/90

1C 


COMPOUND 


(ug/L or ug/Kg) yG/KG 

000038 


I B07Q95 



I-;_ 


Sample wt/vol: 30.5 (g/mL) Q_ Lab File ID: 

Level: (low/mod) Date Received: 12/14/92 

% Moisture: _r 5 decanted: (Y/N) N Date Extracted: 12/21/92 


Injection Volume: 2.0(UL) Dilution Factor: 1.0 

GPC Cleanup: ( YIN ) Y_ pH: 7.3 

100-02-7 -------- 4-Nitrophenol 1 

132-64-9 -------- Dibenzofuran 1 

121-14-2 -------- 2,4-Dinitrotoluene 1 


84-66-2---------Diethylphthalate I 

7005-72-3 ------- 4- Chlorophenyl-phenylether_1 

86-73-7 --------- Fluorene 1 

100-01-6 -------- 4-Nitroan 1 ne 1 

534-52-1 --------4,6-Dinitro-2-methylphenol_I 

86-30-6 --------- N-Nitrosodiphenylamine (1) _1 

101-55-3 -------- 4-Bromophenyl-phenylether I 

118-74-1 -------- Hexachlorobenzene 1 

87-86-5 --------- Pentachlorophenol I 

85-01-8 --------- Phonanthrene 1 

120-12-7 -------- Anthracene 1 

86-74-8 --------- Carbazole 1 

84-74-2 --------- Di-n-Butylphthalate I 

206-44-0 -------- Fluoranthene i 

129-00-0 ----- ---Pyrene 1 

85-68-7 ------ ---Butylbenzylphthalate I 

91-94-1 --------- 3,3'-Dichlorobenzidine 1 

56-55-3 --------- Benzo(a)Anthracens i 

117-81-7 -------- bis(2-Ethylhexyl)Phthalate_i 

218-01-9 ------- -Chrysene 1 

117-84-0 ------- -Di-n-Octyl Phthalate I 

205-99-2--------Benzo(b)Fluoranthene 1 

207-08-9 -------- Benzo(k)Fluoranthene 1 

50-32-8 --------- Benzo(a)Pyrene 1 

193-39-5 -------- Indeno(1,2,3-cd)Pyrene 1 

53-70-3 --------- Dibenz(a,h)Anthracens I 

191-24-2 -------- Benzo(g,h,i)Perylene I 

(1) - Cannot be separated from D phenylam ne 

FORM I SV-2 

830 I UI 

340 I II I 

340 I U1 

340 I UI 

340 J U I 

340 J U I 

340 JU I 

830 I UI 

830 

340 I UI 

340 I VI 

340 I vI 

830 IU I 

340 I UI 

340 I II I 

340 I UI 

340 J U I 

340 I U I 

340 I II I 

340 J U I 

340 JU I 

340 J U I 

340 JU I 

340 I U I 

340 III I 

340 IU I 

340 I UI 

340 I UI 

340 IU I 

340 JU I 

340 IU I 

1-1 

3/90

CAS NUMBER 

HHH===HHHHHHH=HH 

1. 

2. 

3. 

4. 

5. 

6. 

7. 

1F 

COMPOUND NAME 

JUNKNOWN HYDROCARBON 

UNKNOWN HYDROCARBON 


UNKNOWN ALCOHOL 

IPROPANOIC ACID ISOMER 

IHEXANEDIOIC ACID ISOMER 


RT 

HHHHHH 

6.37 

6.68 

7.37 

8.72 

18.13 

25.68 

28.18 

000033 



TENTATIVELY IDENTIFIED COMPOUNDS I 1 

I B07Q95 I 


Lab Code: TMALa_ Came No.: 12047 SAS No.: NA SDG No.: Nom_ 

_ 



Sample wt/vol: 30.5 (g/mL) Q_ Lab File ID: 2123OS16 


% Moisture: _ 5 decanted: (YIN) N 


Concentrated Extract Volume: 500.0 (uL) Date Analyzed: 12/30/92 

Injection Volume: 2.0 (uL) Dilution Factor: 1.0 



Number TICS found: 7 (ug/L or ug/Kg) UG/RG 

I 

I I 


I iHHHHHHHHHHHHIHHHHHI 

I 210 IBJ I 

I 170 IJ I 

1600 IJ I 

210 IBJ I 

I 69 IJ I 

I 100 1 I 

I 69 IJ I 

I 

i I 

FORM I SV-TIC 3/90

1S 


Lab Name: THA/ARLI Contract: WHC 


Date Received: 12/14L 



000040 


807Q96 1 

Lab Code: THWA Case No.: 12047 SAS No.: NA SDG No.: N_ 

:s 

Matrix: (soil/water) SOIL Lab Sample ID: A212047-068 



t Moisture: 4 


Injection Volume: _ 

30.5 ( g/mL) G 

LOW 

decanted: (Y/N) N 


2.0(uL) 


GPC Cleanup: 

GAS NO. 

(YIN) Y PH: 8.8 

COMPOUND 


(ug/L or ug/Kg) yG/KG 

I 

108-95-2--------Phenol 1 

111-44-4 -------- bis(2-Chloroethyl)Ether i 

95-57-8 --------- 2-Chlorophenol I 

541-73-1 -------- 1,3-Dichlorobenzene 1 


95-50-1 --------- 1,2-Dichlorobenzene 1 

95-48-7 --------- 2-Methylphenol 1 

108-60- 1 -------- 2,2'-oxybis(1-Chloropropane)_I 

106-44-5 -------- 4-Methylphenol 1 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne_I 

67-72-1 --------- Hexachloroethane 1 

98-95-3---------Nitrobenzene 1 

78-59-1 --------- Isophorone 1 

88-75-5 --------- 2-Nitrophenol 1 

105-67-9 -------- 2,4-Dimethylphenol 1 

111-91-1 -------- bis(2-Chloroethoxy)Methane_I 

120-83-2 -------- 2,4-Dichlorophenol 1 

120-82-1 -------- 1,2,4-Trichlorobenzene 1 

91-20-3---------Naphthalene 1 

106-47-8 -------- 4-Chloroanil ne 1 

87-68-3 --------- Hexachlorobutad ene I 

59-50-7 --------- 4-Chloro-3-Methylphenol 1 

91-57-6 --------- 2-Methylnaphthalene 1 

1 77-47-4---------Hexachlorocyclopentad e ne — 1 

88-06-2 --------- 2,4,6-Trichlorophenol 1 


91-58-7 --------- 2-Chloronaphthalens 1 

88-74- 4 --------- 2-Nitroaniline 1 

131-11-3 -------- Dimethylphthalate 1 

208-96-8 -------- Acenaphthylene 1 

99-09-2 --------- 3-Nitroaniline 1 

83-32-9 --------- Acenaphthene 1 

51-28-5 --------- 2,4-Dinitrophenol 1 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

820 

340 

820 

340 

340 

820 

340 

820 

I 

IU 

IU 

1 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

III 

IU 

IV 

IU 

IU 

III 

III 

IU 

IU 

IU 

JU 

JU 

IU 

III 

IU 

IU 

IU 

IU 

IU 

IU

1C 

SEMIVOLi1TILE ORGANICS ANALYSIS DATA SHEET 


000041 


B07Q96 1 

Lab Code: THALA _ Case No.: 12047 SAS No.: NA SDG No.: NA - 



Sample wt/vol: 30.5 (9/ML) Q__ Lab File ID: 21231502 


% Moisture: _4 decanted: (YIN) N 





Date Received: 12114192 





(ug/L or ug/Rg) UG/RG St 

100-02-7 -------- 4-Nitrophenol 820 

132-64-9 -------- Dibenzofuran 340 



84-66-2 --------- Diethylphthalate 340 

7005-72-3 ------- 4-Chlorophenyl-phenylether_ 340 

86-73-7 --------- Fluorene 340 

100-01- 6 -------- 4-Nitroan 1 ne 820 

534-52-1 -------- 4,6-Dinitro- 2-methylphenol 820 

86-30-6 --------- N-Nitrosodiphenylamine (1) 340 

101-55-3 -------- 4-Bromophenyl-phenylether 340 

118-74-1 -------- Hexachlorobenzene ( 340 

87-86-5 --------- Pentachlorophenol 820 

85-01-8 --------- Phenanthrene 340 

120-12-7 -------- Anthracene 340 

86-74-8 --------- Carbazole 340 

84-74-2 --------- Di-n-Butylphthalate 46 

206-44-0 -------- Fluoranthene 340 

129-00-0 ------ --Pyrene 340 

85-68-7 ---------Butylbenzylphthalate 340 


56-55-3 --------- Benzo(a)Anthracene 340 

117-81-7 -------- bis(2-Ethylhexyl)Phthalate_l 340 

218-01-9 ------ --Chrysene ( 340 

117-84-0 ------ --Di-n-Octyl Phthalate 340 

205-99-2 -------- Benzo(b)Fluoranthene 340 


50-32-8 --------- Benzo(a)Pyrene 340 

193-39-5 -------- Indeno(1,2,3-cd)Pyrene 340 

53-70-3 --------- Dibenz(a,h)Anthracene 340 

191-24-2 -------- Benzc(g,h,i)Perylene J 340 

(1) - Cannot be separated from Diphenylamine 

FORM I SV-2 

3/90 

i


1F 



Lab Code: THAL8_ Case No.: 12 047 


Sample wt/vol: 30 . 5 (g/mL) 

000042 


B07Q96 1 

Contract: WHC I ' 


Lab Sample ID: A212047-065 

Q Lab File ID: 21231502 

Level: ( low/med) LOW Date Received: 12 /14/92 

t Moisture: 4 decanted: (Y/N) N Date Extracted: 12121/92 

Concentrated Extract Volume: 500.0 ( uL) Date Analyzed: 12Z31/92 

Injection Volume: 2.0 (uL ) Dilution Factor: 1.0 

GPC Cleanup: ( Y/N) Y_ pH: 8.8 


Number TICS found: _ 6 (ug/L or ug/Kg) UGIKG 

I I 1 I I I 

CAS NUMBER I COMPOUND NAMEI RT I EST. CONC. I Q 

1 t:s:asâaa:aaaa I z::aa^:=sasaâ::s:^^sss^s:s I°:::a::s 1 ^âs:s::s::sue I::a=: I 

I 1. (UNKNOWN HYDROCARBON 1 6.65 1 140 IJ 1 

I 2. (UNKNOWN HYDROCARBON I 7.35 1300 ISJ I 

I 

I 3. (UNKNOWN ALCOHOL I 8.68 1 210 1 B 1 

I 4. I PROPANOIC ACID ISOMER t 1 18.12 I 140 IJ 1 

I 5. (UNKNOWN CARBOXYLIC ACID ESTEI 21.12 1 1100 IJ I 

I 6• IHEXANEDIOIC ACID ISOMER 1 25.67 1 210 IJ I 

i I I I i I 

FORM I SV-TIC 3/90 

I

1B 


Lab Name: TMA/ARLI Contract: ?MC 

000043 

EPA SAMPLE NC 

B07Q98 



Sample wt/vol: 30.0 (g/xL) Q_ 

Level: (low/mad) j8g_ 

t Moisture: 4 decanted: (Y/N) iN 

Concentrated Extract volume: 500.0 (uL) 


GPC Cleanup: (YIN) Y pH: _$.8 


108-95-2--------Phenol 

111-44-4 -------- bis(2-Chloroethy 

95-57-8 --------- 2-Chlorophenol_ 

541-73-1 -------- 1,3-Dichlorobenz 

106-46-7 -------- 1,4-Dichlorobenz 

95-50-1 --------- 1,2-Dichlorobenz 

95-48-7 --------- 2-Methylphenol_ 

108-60-1 -------- 2,2'-oxybis(1-Ch 

106-44-5 -------- 4-Methylphenol_ 

621-64-7 -------- N-Nitroso-Di-n-P 



78-59-1 --------- Isophorone 

88-75-5 --------- 2-Nitrophenol 

105-67-9 -------- 2,4-Dimethylphen 

111-91-1 -------- bis(2-Chloroethc 

120-83-2 -------- 2,4-Dichlorophen 


91-20-3---------Naphthalene 

106-47-8 -------- 4-Chloroanil ne 

87-68-3 --------- Hexachlorobutad ene 



77-47-4 --------- Hexachlorocyclopentad ene 


95-95-4 --------- 2,4,5-Trichlorophanol 


88-74-4 --------- 2-Nitroaniline 



99-09-2 --------- 3-Nitroaniline 

83-32-9 --------- Acenaphthene 









340 JU 

340 IV 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

340 JU 

830 JU 

340 JU 

830 JU 

340 JU 

340 JU 

830 JU 

340 JU 

830 JU 

I_

Lab Name: TEA/ARLI 

1C 






% Moisture: _ 4 decanted: (Y/N) K 



GPC Cleanup: ( YIN ) Y- pH: 8.8 


100-02-7 -------- 4-Nitrophenol 1 

000044 

EPA SAMPLE No. 

Contract: WHC 

B07Q98 


Lab Sample ID: x212047-13B 

Lab File ID: 



Date Analyzed: 12/31192 




I I 

830 IU 

132-64-9 -------- Dibenzofuran 1 340 IU 

121-14-2 -------- 2,4-Dinitrotoluene i .340 IU 

606-20-2 -------- 2,6-Dinitrotoluene i 340 IU 

84-66-2 --------- Diethylphthalate i 340 IU 

7005-72-3 ------- 4-Chlorophenyl-phenylether_I 340 IU 

86-73-7 --------- Fluorene I 340 IU 

100-01-6 -------- 4-Nitroan 1 ne I 830 IU 

534-52-1 -------- 4,6-Dinitro-2-methylphenol I 830 IV 

86-30-6 --------- N-Nitrosodiphenylamine (1) ,I 340 III 

101-55-3 -------- 4-Bromophenyl-phenylether I 340 IU 

118-74-1 -------- Hexachlorobenzene I 340 IU 

87-86-5 --------- Pentachlorophenol 1 830 IU 

85-01-8 --------- Phenanthrene I 340 IU 

120-12-7 -------- Anthracene 1 340 IU 

86-74-8 --------- Carbazole 1 340 1U 

84-74-2 --------- Di-n-Butylphthalate i 340 IU 

206-44-0 -------- Fluoranthene i 340 IU 

129-00-0 -------- Pyrene i 340 III 

85-68-7 --------- Butylbenzylphthalate 1 340 III 

91-94-1 --------- 3,3'-Dichlorobenzidine I 340 1U 

56-55-3 --------- Benzo (a) Anthracene ( 340 IU 

117-81-7 -------- bis(2-Ethylhexyl) Phthalate— 1 340 1U 

218-01-9 -------- Chrysene 1 340 IU 

117-84-0 -------- Di-n-Octyl Phthalate 1 340 IU 

205-99-2 -------- Benzo(b)Fluoranthene 1 340 IU 

207-08-9 -------- Benzo(k)Fluoranthene 1 340 IU 

50-32-8 --------- Benzo(a)Pyrene 1 340 III 

193-39-5 -------- Indeno(1,2,3-cd)Pyrene I 340 IU 

53-70-3 --------- Dibenz(a,h)Anthracene I 340 IU 

191-24-2 -------- Benzo(g,h,i)Perylene I 340 

I 

III 

I. 

FORM I SV-2 3/90

000045 

1F EPA SAMPLE NO. 


TENTATIVELY IDENTIFIED COMPOUNDS I B07Q98 


Lab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: pia_ 

Matrix: ( soil/water) SOIL Lab Sample ID: A2 12047-138 

Sample wt/vol: 30.0 (q/mL) ^_ Lab File ID: 21231S09 

Level: ( low/med) LOW Date Received: 12/14/92 

t Moisture: _ 4 decanted: (Y/N) N 



Injection Volume: 2.0(uL) Dilution Factor: 1.0 



Number TICS found: 9 (ug/L or uq/Kq) UG/RG 

CAS NUMBER I COMPOUND NAME I RT 

as:aaâamszaaas: I sa^ss^:s:a^^:mssas^:a:^ l :^â::a: 

1. (UNKNOWN HYDROCARBON I 6.37 

2. ISUBST. BENZENE I 6.42 

3. (UNKNOWN HYDROCARBON ( 6.68 


5. (UNKNOWN ALCOHOL I 8.72 


7. IPROPANOIC ACID ISO MER I 18.13 

S. (UNKNOWN CARBOXYLIC ACID ESTEI 21.15 

9. IHEXANEDIOIC ACID ISO MER I 

I I 

25.68 


a^^^ôssas I :^^sa I 

1 240 I BT I 

69 I JI 

170 IBJ I 

1 1600 IBJ I 

210 IBJ I 

1 

69 IBJ I 

69 I J I 

1 560 IJ I 

140 IBJ I 


1 

I 

1 

I

IS 

SEMIVOLIITILE ORGANICS ANALYSIS DATA SHEET 

400046 


B07Q99 


Lab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: N_ 


Sample wt/vol: 30.7 (g/mL) Q__ 

Level: (low/mad) L40W 

% Moisture: 4 decanted: (YIN) N 





108-95-2--------Phenol 

111-44-4 -------- bis(2-Chloroethyl)Ether 

95-57-8 --------- 2-Chlorophenol 



95-50-1 --------- 1,2-Dichlorobenzene 

95-48-7 --------- 2-Methylphenol 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_ 

106-44-5 -------- 4-Methylphenol 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne_ 



78-59-1 ------- --Isophorone 

88-75-5 ------- --2-Nitrophenol 

105-67-9 -------- 2,4-Dimethylphenol 

111-91-1 -------- bis(2-Chloroethoxy)Methane_ 



91-20-3---------Naphthalene 

106-47-8 -------- 4-Chloroanil ne 



91-57-6 --------- 2-Methvinaphthalene 




88-74-4 --------- 2-Nitroaniline 



99-09-2 --------- 3-Nitroaniline 

83-32-9 --------- Acenaphthene 


Lab Sample ID: A212047-07B__ 







(ug/L or ug/Kg) yG/KG Q 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

810 

340 

810 

340 

340 

810 

340 

810 

IU 

IU 

IU 

IU 

IV 

IU 

IU 

III 

IU 

IU 

III 

IU 

IU 

III 

IU 

IU 

IU 

IU 

IU 

IU 

IV 

U 

U 

U 

U UUUUU I 

3/90


iC 





Level: ( low/med) LOW_ 

Contract: WHC 

SAS No.: NA 

000047 


B07Q99 

SDG No.: NA 


Lab File ID: 21231S03 


t Moisture: _ 4 decanted: ( Y/N) N Date Extracted: 12/21/92 






i 

I I 

100-02-7 -------- 4-Nitrophenol I 810 IU 1 

132-64 -9 -------- Dibenzofuran 1 340 I U 1 

121-14-2 -------- 2,4-Dinitrotoluene 1 340 I U 1 

606-20 -2 -------- 2,6-Dinitrotoluene 1 340 I U 1 

84-66 -2 --------- Diethylphthalate 1 340 IU 1 

7005 -72-3 ------- 4-Chlorophenyl -phenylether_ 1 340 I U 1 

86-73-7 --------- Fluorene 1 340 1U 1 

100-01-6 -------- 4-Nitroan 1 ne 1 810 IU 1 

534-52 -1 -------- 4,6-Dinitro -2-methylphenol 1 810 IU 1 

86-30-6 --------- N-Nitrosodiphenylamine ( 1) _1 340 IU 1 

101-55 - 3 -------- 4-Bromophenyl -phenylether 1 340 IU 1 

118-74-1 -------- Hexachlorobenzene 1 340 1 U 1 

87-86-5 --------- Pentachlorophenol 1 810 I U 1 

85-01 -8 --------- Phenanthrene I 340 IU 1 

120-12-7 -------- Anthracene 1 340 IU 1 

86-74 -8 --------- Carbazole 1 340 1 U 1 

84-74-2 --------- Di-n-Butylphthalate 1 340 I U 1 

206-44-0 -------- Fluoranthene 1 340 IU 1 

129-00-0 -------- Pyrene 

85-68-7 --------- Butylbenzylphthalate 1 340 I U 1 

91-94 -1 --------- 3,3'-Dichlorobenzidine 1 340 I U 1 

56-55-3 --------- Benzo (a)Anthracens I 340 IU 1 

117-81-7 -------- bis(2 -Ethylhexyl ) Phthalate_ I 340 1 U 1 

218-01-9 -------- Chrysene 1 340 IU 1 

117-84 -0 -------- Di-n-Octyl Phthalate I 340 1 U 1 

205-99-2 -------- Benzo (b)Fluoranthens 1 340 1U 1 

207-08-9 -------- Benzo (k)Fluoranthene 1 340 IU 1 

50-32-8 --------- Benzo (a)Pyrene i 340 I U1 

193-39-5 -------- Indeno ( 1,2,3-cd ) Pyrene I 340 I U 1 

53-70 - 3 --------- Dibenz ( a,h)Anthracens 1 340 I U 1 

1 340 I U 1 

191-24-2 -------- Benzo (g,h,i)Perylene 1 340 

^l ^ - ÂTT/1^' I1Y C^MAY9 ^'DI^ }fYf1T1 Il 1'1110 Y1V^ 9111 TA 

FORM I SV-2 

I 

I U I 

I I 

3/90

Lab Name: 

IF 







Contract: WHC 

000048 


B07Q99 

SAS No.: NA SDG No.: KA - 


Q__ Lab File ID: 21231503 

Date Received: 12,/14/92 

% Moisture: —4 decanted: (YI N) i}± Date Extracted: 12/21/92 

Concentrated Extract Volume: 500.0 (uL) Date Analyzed: 12 /31/92 




Number TICS found: 8 (ug/L or ug/Rg) UG/RG 

I 

I 

I CAS NUMBER 

I 

COMPOUND NAME 

Is:ssa^^sxsz-zags: I assaâssâ:se::s::a:mss: 

I 1. IUMMOWN HYDROCARBON 

2. I ( UNKNOWN HYDROCARBON 

I 3. (UNKNOWN ALCOHOL 

I 4. I UNYHOWN ALCOHOL 

I 5. IPROPANOIC ACID ISOMER 

I 6. I HEXANEDIOIC ACID ISOMER 

f 7. I UNXNOWN ACID 

I 8. 

IOCTADECANOIC ACID ISO MER 

1 

I 

i 

I I 

RT EST. CONC. I I Q I 

mâasn^ (asa^sa^::p I ^::aa I 

6.67 

7.35 

8.70 

9.02 

18.10 

25.65 

27.98 

28.15 

I 

I 

I 

I 

I 

I 

I 

1 

170 

1600 

240 

100 

68 

100 

100 

140 

IJ I 

IBJ I 

I BJ I 

IBJ I 

I J I 

1 B I 

IJ I 

IJ I 

FORM I SV-TIC 3/90



% Moisture: _ 3 

1B 



30.2 ( g/mL) G 

r 

I !^ 

decanted: (Y/N) i)„_ 



000049 


I I 

I B07QB0 1 

Lab Code: MINA Case No.: 12047 SAS No.: NA SDG No.: ice, 

Matrix: (soil/water) SOIL Lab Sample ID: 

Lab File ID: 








I I 

I 

1 108-95-2--------Phenol 1 

340 IU 

I 

1 111-44-4 -------- bis(2-Chloroethyl)Ether 1 340 I U I 

1 95-57-8 --------- 2-Chlorophenol 1 340 I U I 

1 541-73-1 -------- 1,3-Dichlorobenzene 1 340 I UI 

1 106-46-7 -------- 1,4-Dichlorobenzene 1 340 I UI 

i 95-50-1 --------- 1,2-Dichlorobenzene 1 340 I UI 

1 95-48-7 --------- 2-Methylphenol 1 340 I II I 

1 108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_I 340 I II I 

1 106-44-5 -------- 4-Methylphenol 1 340 I U I 

1 621-64-7 -------- N-Nitroso-Di-n-Propylam ne_1 340 IU I 

1 67-72-1 --------- Hexachloroethane 1 340 IU I 

1 98-95-3---------Nitrobenzene 1 340 I U I 

1 78-59-1 --------- Isophorone 1 340 I U I 

1 88-75-5 --------- 2-Nitrophenol I 340 I U I 

i 105-67-9 -------- 2,4-Dimethylphenol 1 340 IU 

1 111-91-1 -------- bis(2-Chloroethoxy)Methane_1 340 1U 

1 120-83-2 -------- 2,4-Dichlorophenol 1 340 I UI 

1 120-82-1 -------- 1,2,4-Trichlorobenzene 1 340 IU 

1 91-20-3---------Naphthalene 1 340 IU I 

1 106-47-8 -------- 4-Chloroanil ne 1 340 IU 

1 87-68-3 --------- Hexachlorobutad ene 1 340 1U I 

1 59-50-7 --------- 4-Chloro-3-Methylphenol I 340 1 U I 

1 91-57-6 --------- 2-Methylnaphthalene I 340 IU I 

1 77-47-4 --------- Hexachlorocyclopentad e^ i •340 IU 

i 88-06-2 --------- 2,4,6-Trichlorophenol 1 340 I U I 

1 95-95-4 --------- 2,4,5-Trichlorophenol 1 820 I U I 

1 91-58-7 --------- 2-Chloronaphthalene 1 340 I U I 

1 88-74-4 --------- 2-Nitroaniline 1 820 I U I 

1 131-11-3 -------- Dimethylphthalate 1 340 IU I 

i 208-96-8 -------- Acenaphthylene 1 340 IU I 

1 99-09-2 --------- 3-Nitroaniline 1 820 IU 

1 83-32-9 --------- ACenaphthene 1 340 1 U I 

1 51-28-5 --------- 2,4-Dinitrophenol 1 820 IU I 

FORM I SV-1 

1.0 

3/90

1C 


Lab Name: TKA/ARLI Contract: WHC I 

Lab Code: TffWA Case No.: 12047 SAS No.: NA SDG No.: NA 

I 

000050 


I B07QBO J 

Matrix: (soil/water) SOIL Lab Sample ID: A212047-03D 

Sample wt/vol: 30.2 (g/mL) ti` 

Level: (low/mad) WX 

3 Moisture: ^3 decanted: (YIN) t)___ 



Lab File ID: 2.1230514 





GPC Cleanup: ( YIN) Y. PH: 8.8 


CAS NO. (ug/L or ug/Kg) UG/KG Q 

100-02-7 -------- 4-Nitrophenol J 

132-64-9 -------- Dibenzofuran l 

121-14-2 -------- 2,4-Dinitrotoluene i 

606-20-2 -------- 2,6-Dinitrotoluene J 

84-66-2 --------- Diethylphthalate l 

7005-72-3 ------- 4-Chlorophenyl-phenylether_1 

86-73-7 --------- Fluorene i 

100-01-6 -------- 4-Nitroan 1 ne 1 

534-52-1 -------- 4,6-Dinitro-2-methylphenol,l 

86-30-6 --------- N-Nitrosodiphenylamine (1) -1 

101-55-3 -------- 4-Bromophenyl-phenylether I 

118-74-1 -------- xexachlorobenzene l 

87-86-5 --------- Pentachlorophenol I 

120-12-7 -------- Anthracens 

86-74-8 --------- Carbazole 

84-74-2 --------- Di-n-Butylphthalate 

206-44-0 -------- Fluoranthene 

129-00-0 -------- Pyrene 

85-68-7 --------- Butylbenzylphthalate 

91-94-1 --------- 3,31-Dichlorobenzidine 

56-55-3 --------- Benzo(a)Anthracene 

117-81-7 -------- bis(2-Ethylhexyl)Phthalate_ 

218-01- 9 ------- -Chrysene 

117-84-0 ------- -Di-n-Octyl Phthalate 

205-99-2 -------- Benzo(b)Fluoranthens 

207-08-9 -------- Benzo(k)Fluoranthene 

50-32-8 --------- Benzo(a)Pyrene 

193-39-5 -------- Indeno(1,2,3-cd)Pyrene 

53-70-3 --------- Dibenz(a,h)Anthracens 

191-24-2 -------- Benzo(g,h,i)Perylene 

1) - Cannot be separated from D phenylam ne 

FORM I SV-2 

820 

340 

340 

340 

340 

340 

340 

820 

820 

1 

IU 

I U 

IU 

JU 

JU 

IU 

JU 

JU 

JU 

1 

1 

1 

1 

1 

1 

1 

1 

340 

340 

340 

820 

340 

340 

340 

84 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

JU 

JU 

JU 

JU 

JU 

JU 

JU 

IJ 

JU 

JU 

JU 

JU 

JU 

JU 

JU 

JU 

JU 

JU 

JU 

JU 

JU 

JU 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

1 

I 

1-1 

3/90 

I

1F EPAPB L. 



1 B07QBO 


Lab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: gam_ 

Matrix: (soil/water) SOIL y Lab Sample ID: A212047-03D 

Sample wt/vol: 30.2 (9/ML) s^ Lab File ID: 21230514 

Level: (low/mod) LOW. Date Received: 12/14/92 

% Moisture: _ 3 decanted: (Y/N) N 


Injection Volume: 2.0 (UL) 



Number TICS found: _j5 (ug/L or ug/Kg) UG/KG 

I 

I I 

I I 


I RT I EST. CONC. _I Q- I 

aassass:^saa:s: I asaaass:asaaasas::aaaas:sa ga I Asa::o I asa:sssa:asa: I s:sa: I 

1. (UNKNOWN HYDROCARBON 6.37 170 IBJ 1 1 1 

2. (UNKNOWN HYDROCARBON 1 6.68 1 170 IJ 1 

3. (UNKNOWN HYDROCARBON 1 7.37 1 1600 _1BJ 1 

4. 1UNKNOWN ALCOHOL 1 8.72 1 270 1 1 

I 

5. 1PROPANOIC ACID ISOMER 




1 18.13 1 

1-1- 

240 i J 1 

1-1 

FORM I SV-TIC 3/90

1D 


340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

810 

340 

810 

340 

340 

810 

340 

810 

00005: 


I I 

I B07QB1 I 

Lab Name: TMA/ARLI Contract: WHC I 1 


•K^ 

Matrix: ( soil/water) SOIL Lab Sample ID: A212047-04B 

Sample wt/vol: 30 . 4 (q/mL) G File ID: 21230515 

Level: ( low/mad) 

t Moisture: _3 decanted: (YIN) N 





108-95-2--------Phenol 

111-44-4 -------- bis (2 -Chloroethyl) Ether 

95-57 -8 --------- 2-Chlorophenol 

541-73 - 1 -------- 1,3-Dichlorobenzons 


95-50 - 1 --------- 1,2-Dichlorobanzens 

95-48 -7 --------- 2-Mathylphenol 

108-60-1 -------- 2,2'-oxybis ( 1-Chloropropans)_ 



98-95-3 --------- Nitrobanzene 

78-59 - 1 --------- Isophorone 

88-75-5 --------- 2-Nitrophenol 

105-67-9 -------- 2,4-Dimethylphanol 

111-91-1 -------- bis (2-Chloroethoxy) Methane 


120-82-1 -------- 1,2,4-Trichlorobenzens 

91-20-3-------- -Naphthalene 

106-47-8 -------- 4-Chloroanil ne 


59-50-7 --------- 4-Chloro -3-Methylphenol 



88-06 -2 --------- 2,4,6 -Trichlorophenol 

95-95 -4 --------- 2,4,5-Trichlorophenol 

91-58 -7 --------- 2-Chloronaphthalene 

88-74-4 --------- 2-Nitroaniline 

131-11- 3 -------- Dimethylphthalate 


99-09 -2 --------- 3-Nitroaniline 

83-32-9 --------- Acenaphthene 

51-28 -5 --------- 2,4-Dinitrophenol 





CONCENTRATION UNITS: - 

(uq/L or uq/Kq) UG/KG Q 

III 

II 

III_ 

III 

III 

III 

III 

III 

III 

III 

III 

III 

III 

III 

III 

III 

III 

U 

U UUUUUUUUUUUUU 

3/90

1C 


Lab Name: TMA/ARLI Contract: MC I 

Lab Code: TMALa^ Case No.: 12047 SAS No.: NA SDG No.: NA 

Matrix: ( soil/water) 


Level: ( low/zed) 

% Moisture: _ 3 



GPC Cleanup: (YIN) 

CAS NO. 

30.4 (9/Z+) Q__ 

LOW 

decanted: (Y/N)iN 

Volume: 50 0.0 (uL) 

2.0 (uL) 

1 PH: 8.4 

COMPOUND 

000053 


B07QB1 I 









100-02 -7 -------- 4-Nitrophenol 1 

132-64-9 -------- Dibenzofuran 1 

121-14-2 -------- 2,4-Dinitrotoluene I 


84-66 -2 --------- Diethylphthalate 1 

7005 -72-3 ------- 4-Chlorophenyl -phenylether_ I 

86-73-7 --------- Fluorene I 

100-01-6 -------- 4-Nitroan 1 ne I 

534-52-1 -------- 4,6-Dinitro-2-methylphenol I 

86-30-6 --------- N-Nitrosodiphenylamine (1)_1 

810 

340 

340 

340 

340 

340 

340 

810 

810 

340 

III 

IU 

J U 

III 

III 

I V 

III 

JU 

IU 


118 -74 -1 -------- Hexachlorobenzene I 


85-01-8 --------- Phenanthrene ( 

120-12 -7 -------- Anthracene ( 

86-74-8 --------- Carbazole 1 


206-44-0 -------- Fluoranthene 1 

129-00-0 ------ --Pyrene 1 

85-68-7 ------- --Butylbenzylphthalate 1 


56-55-3 --------- Benzo ( a)Anthracene 1 

117-81-7 -------- bis(2 -Ethylhexyl)Phthalate_ I 

218 -01-9 ------- -Chrysene 1 

117-84-0 ------- -Di-n-OCtyl Phthalate 1 

205-99 -2 -------- Benzo (b)Fluoranthene 1 

207-08-9 -------- Benzo ( k)Fluoranthene ( 

50-32-8 --------- Benzo ( a)Pyrene 1 

193-39-5 -------- Indeno ( 1,2,3-cd)Pyrene 1 

53-70 -3 --------- Dibenz (a,h)Anthracene 1 

191 -24 -2 -------- Benzo(g,h,i)Perylene 1 

340 

340 

810 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

JU 

IU 

IU 

IU 

JU 

JU 

IU 

I U 

IU 

JU 

Iv 

III IU_ 

IU 

IU 

J U 

JU 

IU 

J U 

J U 

IU 

1 

FORM I SV-2 3/90 

1


1F 



Lab Code: TMALA _ Case No.: 12047 


000054 


B07QB1 


SAS No.: NA SDG No.: $a_ 


Sample wt/vol: 30.4 (g/mL) Q_ Lab File ID: 21230S15 

Level: (low/med) LOW Date Received: 12/14/92 

t Moisture: ^3 decanted: ( Y/N) N Date Extracted: 12 /21/92 



GPC Cleanup: (Y/N) y_ pH: 8.4 


Number TICS found: _-3 (ug/L or ug/Kg) yG/I{G 


I 1. (UNKNOWN HYDROCARBON 

I 2• (UNKNOWN HYDROCARBON 

I 3. 

(UNKNOWN ALCOHOL 

I 

i 

I 


I I 

I Q I 

1 6.65 1 170 IJ I 

1 7.33 1 1500 1 B I 

1 8.68 1 

200 IBJ I 

1 

1-1 

FORM I SV-TIC 3/90

18 


I 

000055 


I B07QS2 1 


Lab Code: TMALA Casa No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 30.6 (VML) G 

Level: (low/med) IOW 

% Moisture: _ 4 decanted: (YIN) N 






Lab File ID: 


Date Extracted: 1,2/21/92 





I 

I I 

108-95-2--------Phenol l 340 IU 

1 

111-44-4 -------- his (2-Chloroethyl)Ether I 340 III 1 

95-57-8 --------- 2-Chlorophenol 1 340 1U 1 

541-73-1 -------- 1,3-Dichlorobenzene 1 340 IU 1 

106-46-7 -------- 1,4-Dichlorobenzene l 340 III 1 

95-50-1 --------- 1,2-Dichlorobenzene I 340 IU 1 

95-48-7 --------- 2-Methylphenol 1 340 IU 1 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_1 340 I U1 

106-44-5 -------- 4-Methylphenol l .340 I UI 

621-64-7 -------- N-Nitroso-Di-n-Propylaa ne -___l 340 IU 

67-72-1 --------- Nexachloroethane l 340 1U 1 

98-95-3---------Nitrobenzene 1 340 IU 1 

78-59-1 --------- Isophorone I 340 I U1 

88-75-5 --------- 2-Nitrophenol I 340 I U1 

105-67-9 ------ -- 2,4-Dimethylphenol l 340 IU 1 

111-91-1 --------bis(2-Chloroethoxy) Methane_1 340 III 1 

120-83-2 -------- 2,4-Dichlorophenol l 340 I U1 

120-82-1 -------- 1,2,4-Trichlorobenzene I 340 1U 1 

91-20-3---------Naphthalene 1 340 IU 1 

106-47-8 ------ --4-Chloroanil ne l 340 I U1 

87-68-3 --------- Hexachlorobutad ene 1 340 I U1 

59-50-7 --------- 4-Chloro-3-Methylphenol l 340 I U1 

91-57-6 --------- 2-Methylnaphthalene 1 340 IU 1 

77-47-4---------Hexachlorocyclopentad - 1 340 IU 

88-06-2 --------- 2,4,6-Trichlorophenol 1 340 I U1 

95-95-4 --------- 2,4,5-Trichlorophenol 1 820 I U1 

91-58-7 --------- 2-Chloronaphthalene 1 340 1 U1 

88-74-4 --------- 2-Nitroaniline 1 820 I U1 

131-11-3 -------- Dimethylphthalate I 340 I U1 

208-96-8 -------- Acenaphthylene I 340 IU 1 

99-09-2 --------- 3-Nitroaniline I 820 I U1 

83-32-9 --------- Acenaphthene I 340 I U1 

51-28-5 --------- 2,4-Dinitrophenol I 820 IU I 

FORM I SV-1 

3/90 

I

1C 


00005G 


Lab Name: TKA/AR.LI 

Lab Code: THALA Case No.: 12047 

Contract: WHC 

SAS No.: NA 

B07QB2 

SDG No.: N_ 

Matrix: (soil/water) Lab Sample ID: A212047-08B 

Sample wt/vol: 30.6 (9/ML) Sr__ Lab File ID: 

Level: (low/med) Date Received: 

t Moisture: _4 decanted: (Y/N) N_ Date Extracted: 12/21/92 



GPC Cleanup: (Y/N) Y_ 


pH: 9.7 





I 

100-02-7 -------- 4-Nitrophanol 1 

820 

132-64-9 -------- Dibenzofuran 1 340 

121-14-2 -------- 2,4-Dinitrotoluene 1 340 


84-66-2 --------- Diethylphthalate 1 340 

7005-72-3 ------- 4-Chlorophenyl-phenylether l 340 

86-73-7 --------- Fluorene I 340 

100-01- 6 -------- 4-Nitroan 1 ne 1 820 

534-52-1 -------- 4,6-Dinitro-2-methylphanol, l 820 

86-30-6 --------- N-Nitrosodiphenylamine (1)_1 340 

101-55-3 -------- 4-Bromophenyl-phenylether 1 340 

118-74-1 -------- Hexachlorobenzene 1 340 

87-86-5 --------- Pentachlorophenol 1 820 

85-01-8 --------- Phenanthrene 1 340 

120-12-7 -------- Anthracene ( 340 

86-74-8 --------- Carbazole 1 340 

84-74-2 --------- Di-n-Butylphthalate 1 340 

206-44-0 -------- Fluoranthene 1 340 

129-00-0 -------- Pyrene 1 340 

85-68-7 --------- Butylbenzylphthalate 1 340 

91-94-1 --------- 3,3'-Dichlorobenzidine 1 340 

56-55-3 --------- Benzo(a)Anthracens 1 340 

117-81-7 -------- bis(2-Ethylhexyl)Phthalate-1 

340 

218-01-9 -------- Chrysene 1 340 

117-84-0 -------- Di-n-Octyl Phthalate 1 340 

205-99-2 -------- Benzo(b)Fiuoranthene i 340 

207-08-9 -------- Benzo(k)Fluoranthena ( 340 

50-32-8 --------- Benzo(a)Pyrene 1 340 

193-39-5 -------- Indeno(1,2,3-cd)Pyrene 1 340 

53-70-3 --------- Dibenz(a,h)Anthracene 1 340 

191-24-2 -------- Benzo(g,h,i)Perylene 1 340 

I 

FORM I SV-2 3/90

000057 

IF EPA SAMPLE NO. 



I B07QB2 




Sample wt/vol: 30.6 (g/nL) Q_ Lab File ID: 21231SO4 

Level: (low/mod) LOW Date Received: 17, 1/ 4/92 

% Moisture: _ 4 decanted: (Y/N) N Date Extracted: 12/21/92 





CAS NUMBER 

1. 

2. 

3. 

4. 

5. 

6. 

7. 

8. 

COMPOUND NAME 

SUBST. BENZENE 





PROPANOIC ACID ISOMER 

UNKNOWN CARBOXYLIC ACID ESTE 

HEXANEDIOIC ACID ISOMER 


(ug/L or ug/Kg) UG/RG 

RT 

saa::sis 

6.38 

6.67 

7.37 

8.70 

9.03 

18.12 

21.12 

25.67 


68 IJ 1 

170 IJ 1 

1700 1BJ 1 

240 1BJ 1 

100 1BJ 

100 IJ 1 

650 - IJ I 

100 1 BJ I 

1-1 

FORM I SV-TIC 3/90

000058 

1B EPA SAMPLE NO. 


Lab Name: TMA/ARLI Contract: MC 

I B07QB3 

Lab Code: THAj,I Case No.: 12047 SAS No.: NA SDG No.: gam_ 



Level: ( low/mod) 

% Moisture: 17 



GPC Cleanup: (Y/N) 

CAS NO. 

SOIL Lab Sample ID: A212047 

30.7 (g/mL) Q _ Lab File ID: 2123150 

LOW Date Received: 12/14/9 

decanted: (YI N) TN Date Extracted: 12/21/9 

Volume: 500.0 (uL) Date Analyzed: 12/31/9 

2.0 (uL) Dilution Factor: 1 

3C_ pH: 9.2 


COMPOUND (ug/L or ug/Kg) UQ/KG Q 

108-95-2--------Phenol 1 390 J U I 

111-44-4 -------- bis(2-Chloroethyl)Ether 390 1 1 II I 

95-57-8 --------- 2-Chlorophenol 390 1 1U I 

541-73-1 -------- 1,3-Dichlorobenzene 390 1 U- I 

106-46-7 -------- 1,4-Dichlorobenzene 390 IU 

1 95 -50-1 --------- 1,2 -Dichlorobenzene 1 390 III I 

1 95-48-7 --------- 2-Methylphenol 1 390 III I 

1 108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_1 390 III I 

1 106-44-5 -------- 4-Methylphenol 1 390 I II I 

1 621-64-7 -------- N-Nitroso-Di-n-Propylam ne_1 390 I II I 

1 67-72-1 --------- Hexachloroethane 1 390 I II I 

1 98-95-3---------Nitrobenzene 1 390 I II I 

1 78-59-1 --------- Isophorone 1 390 1U I 

1 88-75-5 --------- 2-Nitrophenol 1 390 1U I 

1 105-67-9 -------- 2,4-Dimethylphenol 390 1U 1 I 

1 111-91-1 -------- bis(2-Chloroethoxy)Methane_1 390 1 U I 

1 120-83-2 -------- 2,4-Dichlorophenol 1 390 I II I 

1 120-82-1 -------- 1,2,4-Trichlorobenzene 1 390 I U I 

1 91-20-3---------Naphthalene 1 390 T I 1 

106-47-8 -------- 4-Chloroanil ne 1 390 IU 1 

1 87-68-3 --------- Hexachlorobutad ens 1 390 (U I 

1 59-50-7 --------- 4-Chloro-3-Methylphenol 1 390 III I 

1 91-57-6 --------- 2 -Methylnaphthalene 1 390 1U 1 

1 77-47-4 --------- Hexachlorocyclopentadad e^ 1 390 1U I 

1 88-06-2 --------- 2,4,6-Trichlorophenol 1 390 1 U I 

1 95-95-4 --------- 2,4,5-Trichlorophenol 1 940 1U I 

1 91-58-7 --------- 2-Chloronaphthalene 1 390 1U 1 

1 88-74-4 --------- 2-Nitroaniline 1 940 1U I 

1 131-11-3 -------- Dimethylphthalate 1 390 1U I 

1 208-96-8 -------- Acenaphthylene 1 390 1U I 

1 99 -09 -2 --------- 3 -Nitroaniline 1 940 1 U I 

1 83-32-9 --------- Acenaphthene 1 390 1 U I 

1 51-28-5 --------- 2,4-Dinitrophenol 1 940 1U - I 

FORM I SV-1 3/90

1C 


000059 


B07QB3 I 


Lab Code: TMXLA_ ,Case No.: 12047 SAS No.: NA SDG No.: NA 



Sample wt/vol: 30.7 (g/mL) Q__ Lab File ID: 21231S05 

Level: (low/mad) Date Received: 12/14/92 

% Moisture: _ 17, decanted: (Y/N) N Date Extracted: 12/21/92 



GPC Cleanup: (YIN) Y 9.2 



I 

100-02-7 -------- 4-Nitrophenol 1 940 

132-64-9 -------- DibenzoPuran 1 390 



84-66-2 --------- Diethylphthalate 120 

7005-72-3 ------- 4-Chlorophenyl-phenylether_) 390 

86-73-7 --------- Fluorene 1 390 

100-01-6 -------- 4-Nitroan 1 ne 1 940 

534-52-1 -------- 4,6-Dinitro-2-methylphenol 1 940 

86-30-6 --------- N-Nitrosodiphenylamine (1) _1 

390 

101-55-3 -------- 4-Bromophenyl-phenylether 1 390 

118-74-1 -------- Hexachlorobenzene 1 390 


85-01-8 --------- Phenanthrene 1 390 

120-12-7 -------- Anthracene 1 390 

86-74-8 --------- Carbazole 1 390 

84-74-2 --------- Di-n-Butyl hthalate 1 390 

206-44-0 -------- Fluoranthena 1 390 

129-00-0 -------- Pyrene 1 390 


91-94-1 --------- 3,3'-Dichlorobenzidine 1 390 

56-55-3 --------- Benzo(a)Anthracene 1 390 

117-81-7 -------- bis(2-Ethylhexyl)Phthalate_1 390 

218-01-9 -------- Chrysene 1 390 

117-84-0 -------- Di-n-Octyl Phthalate 1 390 

205-99-2 -------- Benzo(b)Fluoranthene 1 390 

207-08-9 -------- Benzo(k)Fluoranthene 1 390 

50-32-8 --------- Benzo(a)Pyrene 1 390 

193-39-5 -------- Indeno(1,2,3-cd)Pyrens 1 390 

53-70-3 --------- Dibenz(a,h)Anthracene 1 390 


FORM I SV-2 

3/90

000060 

IF 




( B07QB3 

Lab Name: TEA/ARLI Contract: )HC I I 



Sample wt/vol: 30.7 (9/ML) Q Lab File ID: 21231505 

Level: (low/med) Date Received: 12/14/92 

% Moisture: 17 decanted: (Y/N)i}± Date Extracted: 12/21/92 

Concentrated Extract Volume: 500.0 (UL) Date Analyzed: 12 /31/92 

Injection volume: 2.0 (uL) Dilution Factor: 1.0 




CAS NUMBER 

1. 

2. 

3. 

4. 

5. 

6. 

7. 

8. 

9. 

I COMPOUND NAMEI RT I 

^n^saaa^â^^^m^^ses^ssm=r 1 emâassa I 

1 

ISUBST. BENZENE 6.38 1 I 

(UNKNOWN HYDROCARBON 6.67 1 I 

[UNKNOWN HYDROCARBON I 7.35 I 

[UNKNOWN ALCOHOL 1 8.70 [ 

[UNKNOWN ALCOHOL [ 9.03 [ 

IPROPANOIC ACID ISOMER [ 18.12 [ 

1UNKNOWN CARBOXYLIC ACID ESTEI 21.12 i 

1HEXANEDIOIC ACID ISOMER [ 25.67 [ 

[UNKNOWN HYDROCARBON 1 29.03 1 


79 IJ 1 

160 IJ I 

1500 1W 1 

200 IBJ 1 

120 IBJ 1 

79 IJ 1 

710 (J 1 

240 1 W 1 

79 IJ I 

1-1 

FORM I SV-TIC 3/90

1B 


000061 


I i 

I B07QBS I 




s 


Sample wt/vol: 30.1 (g/mL) Q__ Lab File ID: $121,50 _ 

Level: ( low/zed) Date Received: 12 /14/92 

3 Moisture: _5 decanted: ( Y/N) .r Date Extracted: 12 /21/92 



GPC Cleanup: (YIN) y_ pH: 8.4 


CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 0' 

108-95 -2--------Phenol I 

111-44-4 -------- bis(2 -Chloroethyl ) Ether I 350 

95-57-8 --------- 2-Chlorophenol I 350 

541-73 - 1 -------- 1,3-Dichlorobenzene I 350 1 

106-46-7 -------- 1,4-Dichlorobenzene I 350 1 

95-50-1 --------- 1,2-Dichlorobenzene I 350 1 

95-48 -7 --------- 2-Methylphenol I 350 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_I 350 

106-44-5 -------- 4-Methylphenol I 350 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne_I 350 

67-72-1 --------- Hexachloroethane I 350 

98-95-3-------- -Nitrobenzene I 350 

78-59-1 --------- Isophorone I 350 

88-75-5 --------- 2-Nitrophenol I 350 

105-67-9 -------- 2,4-Dimethylphenol I 350 

111-91-1 -------- his (2 -Chloroethoxy ) Methane — 

350 

120-83-2 -------- 2,4-Dichlorophenol I 350 

120-82 - 1 -------- 1,2,4-Trichlorobenzens I 350 

91-20-3-------- -Naphthalene 350 

I 

106-47-8 -------- 4-Chloroanil ne 350 

I 

87-68-3 --------- Hexachlorobutad ene I 350 

59-50-7 --------- 4-Chloro - 3-Methylphenol I 350 

91-57-6 --------- 2-Methylnaphthalene 350 

I 

77-47-4 --------- Hexachlorocyclopentad e^ne l 

350 

88-06-2 --------- 2,4,6-Trichlorophenol ( 350 


I 

91-58 -7 --------- 2-Chloronaphthalene I 350 

88-74 -4 --------- 2-Nitroaniline I 840 

131-11-3 -------- Dimethylphthalate 350 

I 

208-96 -8 -------- Acenaphthylene 350 

I 

99-09-2 --------- 3-Nitroaniline 840 

I 

83-32-9 --------- Acenaphthene I 350 


I 

840 

I 

I 

I 

350 

I

000062 

1C SPA SAMPLE N0. 


I 1 

I B07QBS 1 

Lab Name: TMA/ARLS Contract: WHC I 1 




Level: (low/med) LOW_ 

t Moisture: 5 decanted: ( Y/N) N 



GPC Cleanup: (YIN) y_ pH: -.4 



Lab File ID: 







I 1 

100-02-7 -------- 4-Nitrophenol 1 

840 1 U 

132-64-9 -------- Dibenzofuran 1 350 IU 1 

121-14-2 -------- 2,4-Dinitrotoluene 1 350 1U 1 


1 

1U 

84-66-2 --------- Diethylphthalate 1 350 1U 1 

7005-72-3 ------- 4-Chlorophenyl-phenylether_1 350 1 U I 

86-73-7 --------- Fluorene 1 350 1U 1 

100-01- 6 -------- 4-Nitroan 1 ne 1 840 1U 1 

534-52-1 -------- 4,6-Dinitro-2-methylphenol 1 840 1 U 1 

86-30-6 --------- N-Nitrosodiphenylamine (1)_1 350 I U1 

101-55-3 -------- 4-Bromophenyl-phenylether 1 350 IU 1 

118-74-1 -------- Hexachlorobenzene 1 350 1U 1 

87-86-5 --------- Pentachlorophenol 1 840 1U 1 

85-01-8 --------- Phenanthrene 1 350 1U 1 

120-12-7 -------- Anthracene 1 350 1U 1 

86-74-8 --------- Carbazole 1 350 1U 1 

84-74-2 --------- Di-n-Butylphthalate 1 .350 1U_ 1 

206-44-0 -------- Fluoranthene 1 350 1 U1 

129-00-0 -------- Pyrene 1 350 1U I 

85-68-7 --------- Butylbenzylphthalate 1 350 1U 1 

91-94-1 --------- 3,3'-Dichlorobenzidine I 350 I U1 

56-55-3 --------- Benzo(a)Anthracene 1 350 1U 1 

117-81-7 -------- bis(2-Ethylhexyl)Phthalate_I 350 1 U1 

218-01-9 ---- ----Chrysene 1 350 I U1 

117-84-0 --------Di-n-Octyl Phthalate 1 350 1 U1 

205-99-2 -------- Benzo(b)Fluoranthene 1 350 1U 1 

207-08-9 -------- Benzo(k)Fluoranthene 1 350 1U 1 

50-32-8 --------- Benzo(a)Pyrene 1 350 1U 1 

193-39-5 -------- Indeno (1, 2, 3 -cd) Pyrene I 350 1 U1 

53-70-3 --------- Dibenz(a,h)Anthracene I 350 1 U1 

191-24-2 -------- Benzo(g,h,i)Perylene I 350 

I 

1 UI 

I I 

FORK I SV-2 3/90 

1 

1

1F 



000063 


I 

( B07QB8 I 

Lab Nam *: TMA/ARLI Contract: VHC I I 


.s 

SAS No.: NA SDG No.: jam_ 

Matrix: ( soil/water) SOIL _ 

Lab Sample ID: A212047-1OB 

Sample wt/vol: 30.1 (VML) G Lab File ID: 21231S06 


Moisture: _5, decanted: (YIN) rK 



Injection Volume: 2.0 (UL) Dilution Factor: 1.0 



Number TICS found: _5 (uq/L or uq/Kg) UG/KG 


svc^âasaa^^^z: I a:a:vas:aaaas::a:aa:^:: 

1. [UNKNOWN HYDROCARBON 

2. [UNKNOWN HYDROCARBON 

3. [UNKNOWN ALCOHOL 


5. IHEXANEDIOIC ACID ISOMER 

I 

RT 

I 

EST. CONC. 1 

I I 

I Q I 

^^:I sac::aaa:aaa 1 a^sa:l 

6.37 1 280 IBJ 1 

7.37 1 1400 1BJ 1 

8.72 1 210 1BJ 1 

18.13 [ 70 1 J I 

1 25.68 1 100 

I 

[BJ I 

I I 

FORM I SV-TIC 3/90

18 


0000 ^ 

EPA SAMPLE O. 

I I 

1 s07Qa9 1 


Lab Code: TMALa_ Case No.: 12047 

1^ 



Lab Sample ID: A212047 


Level: ( low/med) 

% Moisture: _4 




CAS NO. 

30.2 (g/mL) Q_ Lab File ID: 2123150 

j W Date Received: 12/14/9 

decanted: (YIN) N 


Volume: 500.0 (uL) Date Analyzed: 12/31/9 

2.0 (uL) Dilution Factor: _1 

Y_ pH: 9.3 


COMPOUND (ug/L or ug/Rg) UG/KG Q 

I 

108-95-2--------Phenol 1 

I 

340 IU 

111-44-4 -------- bis(2-Chloroethyl ) Ether 1 340 I II 1 

95-57-8 --------- 2 -Chlorophenol I 340 III 1 

541-73 - 1 -------- 1,3-Dichlorobenzene 1 340 I II 1 

106-46-7 -------- 1,4-Dichlorobenzene I 340 III 1 

95-50-1 --------- 1,2-Dichlorobenzene I 340 III 1 

95-48 -7 --------- 2-Methylphenol 1 340 1D 1 

108-60-1 -------- 2,2`-oxybis(1-Chloropropane)_1 340 IU 1 

106-44-5 -------- 4-Methylphenol 1 340 IU 1 

621-64-7 -------- N-Nitroso -Di-n-Propylam ne_1 340 III 1 

67-72 - 1 --------- Hexachloroethans 1 340 III 1 

98-95-3-------- -Nitrobenzene 1 340 III 1 

78-59 - 1 --------- Isophorone 1 340 III 1 

88-75-5 --------- 2-Nitrophenol I 340 IV 1 

105-67-9 -------- 2,4-Dimethylphenol 1 340 III 1 

111-91-1 -------- bis(2 -Chloroethoxy ) Methane_I 340 IU 1 

120-83 -2 -------- 2,4-Dichlorophenol 1 340 III 1 

120-82-1 -------- 1,2,4-Trichlorobenzene 1 340 III 1 

91-20-3-------- -Naphthalene 1 340 I II 1 

106-47 -8 -------- 4-Chloroanil ne 1 340 I II 1 

87-68-3 --------- Hexachlorobutad ene 1 340 IU 1 

59-50-7 --------- 4-Chloro- 3-Methylphenol I 340 J U 1 

91-57-6 --------- 2-Methylnaphthalene 1 340 IU I 

77-47-4 --------- Hexachlorocyclopentad —ne e — I 340 IU 1 

88-06 -2 --------- 2,4,6-Trichlorophenol 340 III 1 

1 

95-95 -4 --------- 2,4,5 -Trichlorophenol 1 830 I II 1 

91-58-7 --------- 2-Chloronaphthalene 1 340 IU 1 

88-74 -4 --------- 2-Nitroaniline 1 830 IU 1 

131-11 - 3 -------- Dimethylphthalate 1 340 III 1 

208-96-8 -------- Acenaphthylene I 340 I II 1 

99-09-2 --------- 3-Nitroaniline 830 1 I II 1 

83-32 -9 --------- Acenaphthene 340 1 III 1 

51-28 -5 --------- 2,4-Dinitrophenol 830 I U I 

1 

FORM I SV-1 

I 

1 

3/90

1C 


Lab Name: TMA/ARLI Contract: NBC I 

830 

340 

340 

340 

340 

340 

340 

830 

830 

340 

340 

340 

830 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

U 

U 

IU 

I U 

U 

IU U 

U 

IU UU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

IU 

000065 


I B07QB9 I 

Lab Code: rya_ Case No.: 12047 SAS No.: NA SDG No.: NA_ 




% Moisture: 4 




CAS NO. 

30.2 (g/mL) G 

LOW 

decanted: (Y/N)iN 


2.0(UL) 

100-02-7--------4-Ni 

Y_ pH: 9.3 

COMPOUND 




7005-72-3 ------- 4-Chlorophenyl-phenylether, 

86-73-7 --------- Fluorene 

100-01-6 -------- 4-Nitroan 1 ne 

534-52-1 -------- 4,6-Dinitro-2-methylphenol_, 

86-30-6 --------- N-Nitrosodiphenylamine (1)_' 

101-55-3 -------- 4-Bromophenyl-phenylether 

118-74-1 -------- Hexachlorobenzene 

87-86-5 --------- Pentachlorophenol 

85-01-8 --------- Phenanthrene 

120-12-7 -------- Anthracene 

86-74-8 --------- Carbazole 

129-00-0 -------- Pyrene 


91-94- 1 --------- 3,3'-Dichlorobenzidine 


117-81-7 -------- bis(2-Ethylhexyl)Phthalate_ 

218-01-9 ------- -Chrysene 

117-84-0 ------- -Di-n-Octyl Phthalate 

205-99-2 -------- Benzo(b)Fluoranthene 


50-32-8 --------- Benzo(a)Pyrene 


53-70-3 --------- Dibenz(a,h)Anthracene 


;1) - Cannot be separated from D phenylam ne 


Lab File ID: 




Dilution Factor% 1.0 



FORM I SV-2 3/90

IF 




000066 


B07QB9 



Sample wt/vol: 30.2 (g/mL) Q Lab File ID: 21231507 


% Moisture: _4 decanted: ( Y/N)iN 






I 

CAS NUMBER 

I^saaasaasaass: 

1. 

2. 

3. 

I 4. 

I 5. 

I 

6. 

7. 

COMPOUND NAME 

SUBST. BENZENE 




PROPANOIC ACID ISOMER 

UNKNOWN CARBOXYLIC ACID ESTE 

HEXANEDIOIC ACID ISOMER 


(ug/L or ug/Kg) UG G 

I 

I I 

RT 

I EST. CONC. I Q 1 

:s^sass^ I aassaasas^ss I mss:^ I 

6.40 I 69 IJ 1 

6.68 I 140 IJ I 

7.37 

8.72 

18.13 

I 

I 

I 

1400 

210 

69 

IBJ 

IBJ 

11 

I 

I 

21.13 I 620 IJ 

25.68 I 69 IBJ 1 

I 1-1 

FORM I SV-TIC 3/90

18 


Lab Name: TKh/ARLI Contract: WHC I 

000067 


I 807000 I 

Lab Code: THE_ Case No.: 12047 SAS No.: NA SDG No.: Nn_ 

s 


Sample wt/vol: 30.3 (g/mL) 0__ 


4 Moisture: _5 decanted: (YIN) N_ 



GPC Cleanup: (Y/N) Y— pH: 9.4 


Lab Sample ID: A212047-12B__ 







(ug/L or ug/Rg) UG/RG 0 

108-95-2--------Phenol I 340 IU 

111-44-4 -------- bis(2-Chloroethyl)Ether I 340 III 

95-57-8 --------- 2-Chlorophenol I 340 III 

541-73-1 -------- 1,3-Dichlorobenzene I 340 III 


95-50-1 --------- 1,2-Dichlorobenzene I 340 III 

95-48-7 --------- 2-Methylphenol I 340 IU 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_I 340 III 

106-44-5 -------- 4-Methylphenol 1 340 III 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne_I 340 III 

67-72-1 --------- Hexachloroethane I 340 III 

98-95-3---------Nitrobenzene I 340 III 

78-59-1 --------- Isophorone I 340 IU 

88-75-5 --------- 2-Nitrophenol i 340 III 

105-67-9 -------- 2,4-Dimethylphenol I 340 III 

111-91-1 -------- bis(2-Chloroethoxy)Methane_) 340 IU 

120-83-2 -------- 2,4-Dichlorophenol ( 340 III 

120-82-1 -------- 1,2,4-Trichlorobenzens I 340 III 

91-20-3---------Naphthalene I 340 IU 

106-47-8 -------- 4-Chloroanil ne I 340 III 

87-68-3 --------- Hexachlorobutad ene I 340 III 

59-50-7 --------- 4-Chloro-3-Methylphenol I 340 III 

91-57-6 --------- 2-Methylnaphthalene I 340 IU 

77-47-4 --------- Hexachlorocyclopentad —ne e — I 340 IU 

88-06-2 --------- 2,4,6-Trichlorophenol I 340 IU 

95-95-4 --------- 2,4,5-Trichlorophenol i 830 III 

91-58-7 --------- 2-Chloronaphthalene I 340 III 

88-74-4 --------- 2-Nitroaniline I 830 III 

131-11-3 -------- Dimethylphthalate I 340 III 

208-96-8 -------- Acenaphthylene I 340 III 

99-09-2 --------- 3-Nitroaniline I 830 III 

83-32-9 --------- Acenaphthene i 340 III 

51-28-5 --------- 2,4-Dinitrophenol I 830 

I 

IU 

1_

lc 



Lab Code: TMALh 


Case No.: 12 047 

SAS No.: NA 


B07000 

SDG No.: NA 

Lab Sample ID: A212047-12B. 

Sample wt/vol: 30.3 (9/ML) Q__ Lab File ID: 21231508 

Level: ( low/mod) Date Received: 12/14/92 

4 Moisture: ^5 decanted: ( Y/N) N_— Date Extracted: 12/21/92 



GPC Cleanup: ( YIN ) Y pH: 9.4 



100-02 -7 -------- 4-Nitrophenol 1 

I 

I 

830 I U 

132-64-9 -------- Dibenzofuran 1 340 I U 1 

121-14 -2 -------- 2,4-Dinitrotoluene 1 340 IU 1 

606-20-2 -------- 2,6-Dinitrotoluene 1 340 IU 1 

84-66 -2 --------- Diethylphthalate 1 340 I U 1 

7005-72-3 ------- 4-Chlorophenyl -phenylether_ 1 340 IU 1 

86-73-7 --------- Fluorene 1 340 IU 1 

100-01-6 -------- 4-Nitroan 1 ne I 830 1 U 1 

534-52-1 -------- 4,6-Dinitro-2-methylphenol I 830 I U 1 

86-30-6 --------- N-Nitrosodiphenylamine ( 1) _1 340 1U 1 

101-55-3 -------- 4-Bromophenyl -phenylether 1 340 IU 1 

118-74-1 -------- Hexachlorobenzene I 340 IU 1 


85-01-8 --------- Phenanthrene 1 340 I II 1 

120-12-7 -------- Anthracene 1 340 IU 1 

86-74-8 --------- Carbazole 1 340 I U 1 

84-74-2 --------- Di-n-Butylphthalate 1 340 J U 1 

206-44-0 -------- Fluoranthene 1 340 I U 1 

129 - 00-0 ------- -Pyrene 1 

I 

1 

340 IU 1 

85-68-7 -------- -Butylbenzylphthalate 1 340 IU 1 

91-94 -1 --------- 3,3'-Dichlorobenzidine I 340 1 U 1 

56-55 -3 --------- Benzo(a)Anthracene 1 340 IU 1 

117-81-7 -------- bis(2-Ethylhexyl ) Phthalate_1 340 I U 1 

218-01-9 ------- -Chrysene 1 340 I U 1 

117-84-0 ------- -Di-n-Octyl Phthalate 1 340 IU 1 

205-99-2 -------- Benzo (b)Fluoranthens 1 340 I U 1 

207-08-9 -------- Benzo ( k)Fluoranthene 1 340 I U 1 

50-32 -8 --------- Benzo (a)Pyrene 1 340 I U 1 

193-39-5 -------- Indeno(1,2,3-cd ) Pyrens 1 340 I U 1 

53-70-3 --------- Dibenz(a,h)Anthracene 1 340 I U 1 

191-24-2 -------- Benzo ( g,h,i)Perylene 1 340 I U I 

(1) - Cannot be separated from Diphenylamine 

FORM I SV-2 

3/90

0000sf 



TENTATIVELY IDENTIFIED COMPOUNDS I i 

I B07000 I 




Sample wt/vol: 30.3 (VAL) S:— Lab File ID: 21231508 

Level: (low/mod) Date Received: 12/14/92 

Moisture: _5 decanted: (YIN) N 




GPC Cleanup % ( Y/N) X_ pH: 9.4 


Number TICS Pound: 4 (ug/L or ug/Kg) t!C/KG 

I I I I I I 

i CAS NUMBER I COMPOUND NAME I RT I EST. CONC. I Q I 

Ia^sa:masasaaa^ I Ysiîiasiaîtiiîiisî^îi^ I aa^âv I a^^saa^^s^â I ^^âa I 

I 1. 

I 2. 

I 3. 

4. 

I 

ISUBST. BENZENE 

(UNKNOWN HYDROCARBON 

(UNKNOWN ALCOHOL 


I 

I 6.40 I 

I 7.37 i 

I 8.72 I 

I 25.68 I 

1- 1 

69 IJ 

1500 I BJ 

210 I BJ 

69 IBJ 

I 

I 

I 

I 

I 

FORM I SV-TIC 3/90

1D 

PESTICIDE ORGANICS ANALYSIS DATA SHEET 

0000 70 


I 

I 

I B07Q93 I 


Lab Code: =ALA Case No.: 12047 SAS No.: NA SDG No.: jam_ 




Extraction: (SepF/font/Sonc) SONC 

Concentrated Extract Volume: 5000 (uL) 




319-84-6 -------- alpha-BHC I 


Lab File ID: 





Sulfur Cleanup: (Y/N) N 



I 

I 

1.81U 

319-85-7 -------- beta-BHC i 1.81U 

319-86-8 -------- delta-BHC ( 1.81U 

58-89-9 --------- gamma-BHC (L ndane) i 1.81U 

76-44-8---------Heptachlor 1 1.81U 

309-00-2 -------- Aldrin i 1.81U- 

1024-57-3 ------- Heptachlor epoxide i 1.81U 

959-98-8 -------- Endosulfan I I 1.81U 

60-57-1 --------- Dieldrin I 3.51U 

72-55-9 --------- 4,4 1 -DDE I 3.51U 

72-20-8 --------- Endrin 1 3.51U 

33213-65-9 ------ Endosulfan II 1 3.51U 

72-54-8 --------- 4,4 0 -DDD I 3.51U 

1031-07-8 ------- Endosulfan sulfate I 3.51U_ 

50-29-3---------4,4'-DDT I 3.51U 

72-43-5 --------- Methoxychlor I 18 III 

53494-70-5 ------ Endrin ketone I 3.51U 

7421-36-3 ------- Endrin aldehyde I 3.51U 

5103-71-9-------alpha-Chlordane I _ 1.81U 

5103-74-2-------gamma-Chlordane I 1.81U 

8001-35-2 ------- Toxaphene I 180 

IU 

12674-11-2 ------ Aroclor-1016 I 35 IU 

11104-28-2 ------ Aroclor-1221 I 71 IU 

11141-16-5 ------ Aroclor-1232 I 35 III 

53469-21-9 ------ Aroclor-1242 I 35 III 

12672-29-6 ------ Aroclor-1248 1 35 IU IU- 

11097-69-1 ------ Aroclor-1254 I 35 

11096-82-5------Aroclor-1260 I 35 

I 

IU 

I_ 

FORM I PEST 3/90

ID 


Lab Name: TMA/ARLI Contract: )HC 

Lab Code: TMALh 



% Moisture: 4 decanted: (Y/N) N 

Extraction: (SepF/Cont/Sonc) SONIC 


Lab File ID: 

000071 


I B07Q94 

Case No.: .2 1 047 SAS No.: NA SDG No.: NA- 





^ I 

1 319-84-6 -------- alpha-BHC ( 





Sulfur Cleanup: (YIN) tN 


(ug/L or ug/Kg) UG/RG Q. 

1 

1.81U 

1 319-85-7 -------- beta-BHC I 1.81U 

1 319-86 - 8 -------- delta-BHC 1 1.81U 

1 58-89-9 --------- gamma-BHC ( L ndane) i 1.81U 

1 76-44-8---------Heptachlor 1 1.81U 

1 309-00-2 -------- Aldrin 1 1.81U 

1 1024-57-3-------Heptachlor epoxide 1 1.81U 

1 959-98-8 -------- Endosulfan I 1 1.81U 

1 60-57-1 --------- Dieldrin 1 3.41U 

1 72-55-9 --------- 4 1 4'-DDE 1 3.41U 

1 72-20-8 --------- Endrin 1 3.41U 

1 33213-65-9 ------ Endosulfan II i 3.41U 

1 72-54-8 --------- 4 t 4 l -DDD 1 3.41U 

1 1031-07-8 ------- Endosulfan Sulfate 1 3.41U 

1 50-29-3---------4,4'-DDT 1 3.41U 

1 72-43-5 --------- Methoxychlor 1 18 IU 

1 53494-70-5 ------ Endrin ketone 1 3.41U 

i 7421-36-3 ------- Endrin aldehyde 3.41U 

1 

1 5103-71-9-------alpha-Chlordane 1 1.81U 

1 5103 -74-2-------gamma -Chlordane 1 1.81U 

1 8001 - 35-2 ------- Toxaphene 1 180 I U 

1 12674-11-2 ------ Aroclor-1016 1 34 IU 

i 11104-28 -2 ------ Aroclor - 1221 1 69 IU 

1 11141-16-5 ------ Aroclor - 1232 i 34 IU 

1 53469-21-9 ------ Aroclor-1242 1 34 IU 

1 12672-29-6 ------ Aroclor-1248 1 34 IU 

1 11097-69-1 ------ Aroclor-1254 1 34 IU 

1 11096 -82 -5 ------ Aroclor-1260 1 34 IU 

FORM I PEST 

3/90

1D 


.ab Name: TMAIARLI Contract: WHC 

000072 


B07Q95 

.ab Code: THALA Case No.: 12047 -SAS No.: NA SDG No.: Jam_ 

Atrix: (soil/water) SQIL_ 

ample wt/vol: 30.6 (q/mL) Q__ 

Moisture: 5 decanted: (YIN) 7N 

xtraction: (SepF/font/Sonc) SONG 

oncentrated Extract Volume: 5000 (uL) 

njection Volume: 1.00 (uL) 

PC Cleanup: ( YIN ) Y _ pH: 7.3 

Lab.Sample ID: A212047-05B 

Lab File ID: 


Date Extracted: 12/21/92 1/92 



Sulfur Cleanup: (Y/N) )L_ 


CAS NO. COMPOUND (ug/L or ug/Rg) UG/XG Q. 

I I 

I I 

1 319-84-6 -------- alpha-BHC I 1.81U 

I 

J 319-85-7 -------- beta-BHC J 1.81U J 

J 319-86-8 -------- delta-BHC 1 1.81U I 

i 58-89-9 --------- gamma-BHC (L ndans) J 1.81U 1 

1 76-44-8---------Heptachlor 1 1.810 I 

1 309-00- 2 -------- Aldrin 1 1.81U 1 

1 1024-57-3-------Heptachlor epoxide 1 1.81U 1 

J 959-98-8 -------- Endosulfan I J 1.81U I 

i 60-57-1 --------- Dieldrin I 3.41U I 

1 72-55-9 --------- 4,4'-DDE 1 3.41U I 

J 72-20-8 --------- Endrin J 3.41U I 

i 33213-65-9 ------ Endosulfan II J 3.41U I 

72-54-8 --------- 4,4'-DDD I 3.41U I 

J 1031-07-8 ------- Endosulfan sulfate J 3.41U I 

1 50-29-3---------4,4'-DDT ( 3.41U I 

J 72-43-5 --------- Methoxychlor 1 18 JU I 

J 53494-70-5 ------ Endrin ketone J 3.41U I 

1 7421-36-3 ------- Endrin aldehyde J 3.41U I 

1 5103-71-9-------alpha-Chlordane 1 1.81U I 

1 5103-74-2-------gamma-Chlordane J 1.81U I 

1 8001-35-2 ------- Toxaphene J 180 JU I 

12674-11-2 ------ Aroclor-1016 J 34 JU I 

J 11104-28-2 ------ Aroclor-1221 J 69 JU I 

1 11141-16-5 ------ Aroclor-1232 J 34 IU I 

J 53469-21-9 ------ Aroclor-1242 J 34 JU I 

J 12672-29-6 ------ Aroclor-1248 1 34 JU I 

J 11097-69-1 ------ Aroclor-1254 J 34 JU I 

1 11096-82-5 ------ Aroclor-1260 

I_ 

1 

I 

34 

JU 

I I 

FORM I PEST 3/90

1D 


000073 


I 

1 

B07Q98 I 

:,ab Name: TMA/ARLI Contract: WHC I I 

:,ab Code: TMAL7t Case No.: 12047 SAS No.: NA 

s 

SDG No.: NA 

iatrix: (soil/water) SOIL 


>ample wt/vol: 30.7 (q/mL) G Lab File ID: 

t Moisture: 4 decanted: (Y/N) N Date Received: 12/14/92 

;xtraction: (SepF/Copt/SOnc) SONC Date Extracted: 12/21/92 

:oncentrated Extract Volume: 5000 (UL) Date Analyzed: 01/06/93 


SPC Cleanup: (Y/N) Y_ pH: 8.8 Sulfur Cleanup: (Y/N) L7_ 


CAS NO. COMPOUND (uq/L or uq/Rq) UG/RG Q 

319-84-6 -------- alpha-BHC 1 

I 

1.71U 

I I 

319-85-7 -------- beta-BHC 1 1.71U 1 

319-86-8 -------- delta-BHC 1 1.71U I 

58-89-9 --------- gamma-BHC (L ndane) 1 1.71U 1 

76-44-8---------Heptachlor 1 1.71U 1 

309-00-2 -------- Aldrin 1 1.71U _ 1 

1024-57-3-------Heptachlor epoxide 1 1.71U 1 

959-98-8 -------- Endosulfan I 1 1.71U 1 

60-57-1 --------- Dieldrin 1 3.41U 1 

72-55-9 ---------- ,4'-DDE 1 3.41U 1 

72-20-8 --------- Endrin 1 3.41U 1 

33213-65-9 ------ Endosulfan II 1 3.41U 1 

72-54-8 --------- 4,4'-DDD 1 3.41U 1 

1031-07-8 ------- Endosulfan sulfate 1 3.41U 1 

50-29-3---------4,49-DDT 1 3.41U 1 

72-43-5 --------- Methoxychlor 1 17 I U1 

53494-70-5 ------ Endrin ketone 1 3.41U 1 

7421-36-3 ------- Endrin aldehyde 1 3.41U 1 

5103-71-9-------alpha-Chlordane i 1.71U 1 

5103-74-2-------gamma-Chlordane 1 1.71U 1 

8001-35-2 ------- Toxaphene 1 170 IU 1 

12674-11-2 ------ Aroclor-1016 1 34 IU 1 

11104-28-2 ------ Aroclor-1221 1 68 IU 1 

11141-16-5 ------ Aroclor-1232 1 34 I U1 

53469-21-9 ------ Aroclor-1242 1 34 I U1 

12672-29-6 ------ Aroclor-1248 1 34 IU 

11097-69-1 ------ Aroclor-1254 1 34 IU 

11096-82-5 ------ Aroclor-1260 1 34 

I 

I U1 

I I 

FORM I PEST 3/90 

1

1D 



000074 


B07Q99 

Lab Code: TMhLh _ Case No.: 12047 SAS No.: NA SDG No.: NA 

_ 



Sample wt/vol: 30.4 (VRL) G_ 


Extraction: ( SepF/Copt/Sonc) SQNC 

Concentrated Extract Volume: 5000 


GPC Cleanup: (YIN) y _ pH: 9.0 

Lab File ID: 

Date Received: 12f14/92 


( uL) Date Analyzed: 01 /06/93 


Sulfur Cleanup: (Y/N) $_ 


CAS NO. COMPOUND (ug/L or ug/Rg) lL7G/RG 

^ I 

319-84 -6 -------- alpha -BHC 1 1.71U 

319-85-7 -------- beta-BHC 1 1.71U 

319-86 -8 -------- delta -BHC 1 1.71U 

58-89 -9 --------- gamma -BHC (L ndane) 1 1.71U 

76-44-8---------Heptachlor 1 1.71U 

309-00-2 -------- Aldrin 1.71U 

1024 -57-3-------Heptachlor epoxide 1 1.71U 

1 959-98 -8 -------- Endosulfan I 1 1.71U 

1 60-57 - 1 --------- Dieldrin 1 3.41U 

1 72-55 -9 --------- 4 t 4' -DDE 1 3.41U 

1 72-20 - 8 --------- Endrin 1 3.41U 

1 33213-65-9 ------ Endosulfan II 1 3.41U 

1 72-54-8 --------- 4 1 4'-DDD 1 3.41U 

1 1031 - 07-8 ------- Endosulfan sulfate 1 3.41U 

1 50-29-3-------- -4,4'-DDT 1 3.41U 

1 72-43 -5 --------- Methoxychlor 1 17 IU 

i 53494-70-5 ------ Endrin ketone 1 3.41U 

1 7421-36-3 ------- Endrin aldehyde 1 3.41U 

1.71U 

1 5103-71-9-------alpha-Chlordane 

1 

1 5103-74-2-------gamma-Chlordane 1 1.71U 

1 8001-35-2 ------- Toxaphene 1 170 IU 

1 12674-11-2 ------ Aroclor-1016 1 34 IU 

1 11104-28-2 ------ Aroclor-1221 69 1 I U 

1 11141-16-5 ------ Aroclor-1232 ( 34 I U 

1 53469-21-9 ------ Aroclor-1242 34 IU 

1 

1 12672-29-6 ------ Aroclor-1248 34 1 I U 

1 11097-69-1 ------ Aroclor- 1254 1 34 IU 

1 11096-82-5 ------ Aroclor-1260 

( 34 IU 

I 

FORM: I PEST 

I 

I_ 

F1 

3/90

ID 


000075 

EPA SAXPLE NO. 

I B07QB0 

Lab Name: TMA/ARLI Contract: WHC 1- 

Lab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: NA_ 




Extraction: (SepF/font/SOnc) SONC 



GPC Cleanup: (Y/N) Y— pH: 8.8 

Lab Sample ID: A212047-03D 

Lab File ID: 





Sulfur Cleanup: (YIN) 19 


CAS NO. COMPOUND (ug/L or ug/Rg) yG/KG Q 

I I 

1 319-84-6 -------- alpha-BHC 1 

I 

1.71U 

1 319-85-7 -------- beta-BHC 1 1.71U 

1 319-86- 8 -------- delta-BHC 1 1.71U 

i 58-89-9 --------- gamma-BHC (L ndane) 1 1.71U 

1 76-44-8---------Heptachlor 1 1.71U 

1 309-00- 2 -------- Aldrin 1 1.71U 

1 1024-57-3-------Heptachlor spox de 1 1.71U 

1 959-98- 8 -------- Endosulfan I 1 1.71U 

i 60-57-1 --------- Dieldrin 1 3.31U_ 

1 72-55-9 --------- 4,4 0 -DDE 1 3.31U 

1 72-20-8 --------- Endrin 1 3.31U 


1 72-54-8 --------- 4,4 1 -DDD 1 3.31U 

i 1031-07-8 ------- Endosulfan sulfate 1 3.31U 

1 50-29-3---------4,4'-DDT 1 3.31U 

1 72-43-5 --------- Methoxychlor 1 17 1U 

1 53494-70-5 ------ £ndrin ketone 1 3.31U 

i 7421-36-3 ------- Endrin aldehyde 1 3.31U 

1 5103-71-9-------alpha-Chlordane I 1.71U 


1 8001-35-2 ------- Toxaphene I 170 1U 

1 12674-11-2 ------ Aroclor-1016 I 33 1U 

1 11104-28-2 ------ Aroclor-1221 1 67 IU 

11141-16-5 ------ Aroclor-1232 i 33 IU 

1 53469-21-9 ------ Aroclor-1242 1 33 IU 

i 12672-29-6 ------ Aroclor-1248 I 33 IU 

i 11097-69-1 ------ Aroclor-1254 1 33 IU 

1 11096-82-5 ------ Aroclor-1260 

I 

FORM I PEST 

I 

I 

33 

IU 

I_ 

3/90

00007E 

1D EPA SAMPLE NO. 


I B07QB1 1 




Sample wt/vol: 30.8 (g/mL) G_ Lab File ID: 

% Moisture: 3 decanted: (YIN) H_ 

Extraction: (SepF/Copt/Sonc) SONC 

Concentrated Extract Volume: 5000 (UL) 


GPC Cleanup: (YIN) Y. pH: 8.4 






Sulfur Cleanup: (YIN) 9 


(ug/L or ug/Rg) UG/RG Q, 

319-84-6 -------- alpha-BHC 1.71U 

319-85-7 -------- beta-BHC 1.71U 

319-86-8 -------- delta-BHC 1.71U 

58-89-9 --------- gamma-BHC (L ndane) 1.71U 

76-44-8---------Heptachlor 1.71U 

309-00-2 -------- Aldrin 1.71U 

1024-57-3-------Heptachlor epoxide 1.71U 

959-98-8 -------- Endosulfan I 1.71U 

3.31U 

72-55-9 --------- 4,4' -DDE 3.31U 

72-20-8 --------- Endrin 1 3.31U 


72-54-8 -------- -4,4' -DDD 3.31U 

1031-07-8 ------ -Endosulfan sulfate 1 3.31U 

50-29-3---------4,4'-DDT 1 3.31U 

72-43-5 -------- -Methoxych or 1 17 III 

53494-70-5 ------ Endrin ketone 1 3.31U 

7421-36-3 ------- Endrin aldehyde i 3.31U 

5103-71-9-------alpha-Chlordane I 1.71U 


8001-35-2 ------- Toxaphene I 170 IU 

12674-11-2 ------ Aroclor-1016 I 33 IU 

11104-28-2 ------ Aroclor-1221 I 67 IU 

11141-16-5 ------ Aroclor-1232 1 33 IU 

53469-21-9 ------ Aroclor-1242 1 33 IU 

12672-29-6 ------ Aroclor-1248 1 33 IU 

11097-69-1 ------ Aroclor-1254 1 33 IU 

11096-82-5 ------ Aroclor-1260 1 33 IU 

I I_ 


I 

I


ID 



latrix: (soil/water) SOIL 

Sample wt/vol: 30.6 ( g/mL ) G 

t Moisture: 4 decanted: (Y/N) NI_ 

Extraction: (SepF/Copt/Sono) SONC 

:oncentrated Extract Volume: 5000 (uL) 

Injection volume: 1,00 (UL) 



319-84-6 -------- alpha-BHC 1 

0000'77 


B07QB2 I 

Contract: WHC _I 


Lab Sample ID: A212047-OOB_ 

Lab File ID: 







(ug/L or ug/Kg) UUG/RG Q 

I I 

1.71U 

319-85-7 -------- beta-BHC 1 1.71U 

319-86-8 -------- delta-BHC 1 1.71U 

58-89-9 --------- gamma-BHC (L ndane) 1 1.71U 

76-44-8---------Heptachlor 1 1.71U 

309-00-2 -------- Aldrin 1 1.71U 

1024-57-3-------Heptachlor epoxide 1 1.71U 

959-98-8 -------- Endosulfan I 1 1.71U 

60-57-1 --------- Dieldrin i 3.41U 

72-55-9 --------- 4,4 1 -DDE 1 3.41U 

72-20-8 --------- Endrin 1 3.41U 


72-54-8 --------- 4,4 0 -DDD 1 3.41U 

1031-07-8 ------- Endosulfan sulfate 1 3.41U 

50-29-3---------4,4'-DDT 1 3.41U 

72-43-5 --------- Methoxychlor 1 17 IU 


7421-36-3 ------- Endrin aldehyde ( 3.41U 

5103-71-9-------alpha-Chlordane 1 1.71U 

5103-74-2-------gamma-Chlordane 1 1.71U 

8001-35-2 ------- Toxaphene 1 170 IU 

12674-11-2 ------ Aroclor-1016 1 34 IU 

11104-28-2 ------ Aroclor-1221 1 68 Iv 

11141-16-5 ------ Aroclor-1232 1 34 IU 

53469-21-9 ------ Aroclor-1242 1 34 IU 

12672-29-6 ------ Aroclor-1248 1 34 IU 

11097-69-1 ------ Aroclor-1254 1 34 IU 

11096-82-5 ------ Aroclor-1260 1 34 

I 

FORD I PEST 3/90 

IU 

I_ 

I

1D 


1111 P 


B07QB3 I 


Lab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: NA — 



% Moisture: 17 decanted: (Y/N) 1'_ 

Extraction: (SepF/font/SOnc) SONG 




I 


319-84-6 -------- alpha-BHC 1 

Lab Sample ID: A212042-09B- 

Lab File ID: 





Sulfur Cleanup: (Y/N)rK 



I 

I 

2.OIU 

319-85-7 -------- beta-BHC 1 2.OIU 

319-86-8 -------- delta-BHC 1 2.OIU 

58-89-9 --------- gamma-BHC (L ndane) I 2.OIU 

76-44-8---------Heptachlor 1 2.OIU 

309-00-2 ------ --Aldrin 1 2.OIU 

1024-57-3-------Heptachlor epoxide 1 2.OIU 

959-98-8 -------- Endosulfan I i 2.OIU 

60-57-1 --------- Dieldrin 1 3.91U 

72-55-9 ---------- 4,4'-DDE 1 3.91U 

72-20-8 --------- Endrin 1 3.91U 


72-54-8 --------- 4,4'-DDD 1 3.91U 


50-29-3---------4,4'-DDT 1 3.91U 



7421-36-3 ------- Endrin aldehyde 1 3.91U 

5103-71-9-------alpha-Chlordane 1 2.OIU 

5103-74-2-------gamma-Chlordane 1 2.OIU 

8001-35-2 ------- Toxaphene 1 200 IU 

12674-11-2 ------ Aroclor-1016 1 39 IU 

11104-28-2 ------ Aroclor-1221 1 79 IU 

11141-16-5 ------ Aroclor-1232 1 39 IU 

53469-21-9 ------ Aroclor-1242 1 39 IU 

12672-29-6 ------ Aroclor-1248 1 39 IU 

11097-69-1 ------ Aroclor-1254 ( 39 IU 

11096-82-5 ------ Aroclor-1260 

i 

39 IU 

I 

I_ 


I


1D 


Contract: WHC 




% Moisture: 5 decanted: (YIN) N_ 

Extraction: (SepF/font/Sonc) SONC 





000079 

I 


B07QBS I 

i 

Lab Sample ID: A212047-1OB 

Lab File ID: 





Sulfur Cleanup: (Y/N)iN 


(ug/L or ug/Rg) UG/RG 

I- 

319-84-6 -------- alpha-BHC I 

1.8 

319-85-7 -------- beta-BHC I 1.8 

319-86-8 -------- delta-BHC I 1.8 

58-89-9 --------- gamma-BHC (L ndane) I 1.8 

76-44-8---------Heptachlor I 1.8 

309-00-2 -------- Aidrin I 1.8 

1024-57-3-------Heptachlor epoxide I 1.8 

959-98-8 -------- Endosulfan I I 1.8 

60-57-1 --------- Dieldrin I 3.4 

72-55-9 --------- 4,4'-DDE I 3.4 

72-20-8 --------- Endrin I 3.4 

33213-65-9 ------ Endosulfan II I 3.4 

72-54-8 --------- 4,4'-DDD I 3.4 

1031-07-8 ------- Endosulfan sulfate I 3.4 

50-29-3---------4,4'-DDT I 3.4 

72-43-5 --------- Methoxychlor I 18 

53494-70-5 ------ Endrin ketone I 3.4 

7421-36-3 ------- Endrin aldehyde I 3.4 

5103-71-9-------alpha-Chlordane I 1.8 

5103-74-2-------gamma-Chlordane I 1.8 

8001-35-2 ------- Toxaphene I 1S0 

12674-11-2 ------ Aroclor-1016 I 34 

11104-28-2 ------ Aroclor-1221 I 70 

11141-16-5 ------ Aroclor-1232 I 34 

53469-21-9 ------ Aroclor-1242 I 34 

12672-29-6 ------ Aroclor-1248 I 34 

11097-69-1 ------ Aroclor-1254 I 34 

11096-82-5 ------ Aroclor-1260 I 34 

FORM I PEST 

I 

U 1 

U I 

U I 

U 1 

U 1 

U I 

U I 

U I 

U I 

U I 

U 

U 1 

U 1 

U i 

U 1 

U 1 

U 1 

U 1 

U 

U I 

U 

U i 

U 1 

U 1 

U I 

U 1 

U 1 

1 

3/90

1D 


:Ab Name: TMA/ARLI Contract: WHC 

000080 


B07QB9 

gab Code: THALA Case No.: 12047 SAS No.: NA SDG No.: NA 

Satrix: (soil/water) SOIL 

,ample wt/vol: 30.7 (g/mL) G_ 


3xtraction: (SepF/font/sonc) SONC 



;PC Cleanup: (Y/N) y_ pH: 9.3 



Lab File ID: 

319-84-6 -------- alpha-BHC 1 








I 

I 

1.71U 

319-85-7 -------- beta-BHC 1 1.71U 

319-86-8 -------- delta-BHC 1 1.71U 

58-89-9 --------- gamma-BHC (L ndane) 1 1.71U 

76-44-8---------Heptachlor I 1.71U 

309-00-2 -------- Aldrin I 1.71U 

1024-57-3-------Heptachlor epoxide 1 1.71U 

959-98-8 -------- Endosulfan I I 1.71U 

60-57-1 --------- Dieldrin 1 3.41U 

72-55-9 --------- 4,4 0 -DDE i 3.41U 

72-20-8 --------- Endrin 1 3.41U 


72-54-8 --------- 4,4'-DDO 1 3.41U 


50-29-3---------4,41-DDT 1 3.41U 




5103-71-9-------alpha-Chlordane 1 1.71U 


8001-35-2 ------- Toxaphene 1 170 IU 

12674-11-2 ------ Aroclor-1016 1 34 IU 

11104-28-2 ------ Aroclor-1221 1 68 IU 

1 11141-16-5 ------ Aroclor-1232 i 34 IU 

1 53469-21-9 ------ Aroclor-1242 1 34 1U 

1 12672-29-6 ------ Aroclor-1248 1 34 1U 

1 11097-69-1 ------ Aroclor-1254 1 34 IU 

1 11096-82-5 ------ Aroclor-1260 1 34 IU 

FORM I PEST 

3/90

ID 



000081 


B07QC0 

Lab Code: TMALA Case No.: 12047 SAS No.: ETA SDG No.: KA 



i Moisture: 5 decanted: (Y/N) N 

Extraction: (SepF/Cont/Sonc) SONC 





Lab File ID: 

Date ReceiVed: 12/14/92 






(ug/L or ug/Kg) tUG/KG 

I 

319-84-6 -------- alpha-BHC 1.7 

319-85-7 -------- beta-BHC 1.7 

319-86-8 -------- delta-BHC 1 1.7 

58-89-9 --------- gamma-BHC (L ndane) 1.7 

76-44-8---------Heptachlor 1 1.7 

309-00-2 -------- Aldrin i 1.7 

1024-57-3-------Heptachlor epox de 1 1.7 

959-98-8 -------- Endosulfan I 1.7 

60-57-1 --------- Dieldrin 3.4 

72-55-9 --------- 4,4'-DDE 3.4 

72-20-8 --------- Endrin 1 3.4 

33213-65-9 ------ Endosulfan II 3.4 

72-54-8 --------- 4 0 4'-DDD 1 3.4 

1031-07-8 ------- Endosulfan sulfate 3.4 

50-29-3---------4r4'-DDT 3.4 

72-43-5 --------- Methoxychlor 1 17 

53494-70-5 ------ Endrin ketone 3.4 

7421-36-3 ------- Endrin aldehyde 1 3.4 

5103-71-9-------alpha-Chlordane 1.7 

5103-74-2-------gamma-Chlordane 1.7 

8001-35-2 ------- Toxaphene 1 170 

12674-11-2 ------ Aroclor-1016 34 

11104-28-2 ------ Aroclor-1221 1 69 

11141-16-5 ------ Aroclor-1232 1 34 

53469-21-9 ------ Aroclor-1242 1 34 

12672-29-6 ------ Aroclor-1248 34 

11097-69-1 ------ Aroclor-1254 1 34 

11096-82-5 ------ Aroclor-1260 I 34 


S

1D 



UUU740 


I ^ 

B07Q96 I 


Matrix: (soil/water) SOIL Lab Sample ID: A212047-o6B 

Sample wt/vol: 30.9 (g/mL) G Lab File ID: 

% Moisture: 4 decanted: (YIN) N Date Received: - 12/14/92 

Extraction: (SepF/font/Sonc) SONC Date Extracted: 12/21/92 

Concentrated Extract Volume: 5000 (uL) Date Analyzed: 011 06/93 


GPC Cleanup: (YIN) Y pH: 8.8 Sulfur Cleanup: (YIN) 1N 


CAS NO. COMPOUND (ug/L or ug/Kg) UG KG Q_ 

I 

I 

1.71U 

319-84-6 ------- -alpha-BHC 1 

319-85-7 ------- -beta-BHC 1.71U 1 I 

319-86-8 -------- delta-BHC 

1.71U 

58-89-9 --------- gamma-BHC (L ndane) 1 

. 

I 

1 

76-44-8---------Heptachlor 1 1.71U I 

309-00-2 -------- Aldrin 1 1.71U I 

1 1024-57-3-------Heptachlor epoxide i 1.71U 

1 959-98-8 -------- Endosulfan I 1.71U 

1 

1 60-57-1 --------- Dieldrin i 3.31U 

1 72-55-9 --------- 4,4'-DDE 3.31U 

1 

1 72-20-8 --------- Endrin 3.31U 1 _ 


1 72-54-8 --------- 4,4'-DDD 1 3.31U 

1 1031-07-8 ------- Endosulfan sulfate 1 3.31U 

1 50-29-3---------4,4'-DDT 1 3.31U 

1 72-43-5---------Methoxychlor 1 17 IU 

1 53494-70-5 ------ Endrin ketone 1 3.31U 

1 7421-36-3 ------- Endrin aldehyde 1 3.31U 

1 5103-71-9-------alpha-Chlordane i 1.71U 


1 8001-35-2 ------- Toxaphene 1 170 IU 

1 12674-11-2 ------ Aroclor-1016 1 33 IU 

1 11104-28-2 ------ Aroclor-1221 1 68 IU 

1 11141-16-5 ------ Aroclor-1232 I 33 IU 

1 53469-21-9 ------ Aroclor-1242 1 33 IU 

1 12672-29-6 ------ Aroclor-1248 1 33 IU 

1 11097-69-1 ------ Aroclor-1254 1 33 IU 

1 11096-82-5 ------ Aroclor-1260 1 33 JU 

FORM I PEST 

i 

1 

3/90

GENERAL CHEMISTRY RESULTS 

CASE N0. 12-047 

Soil Sample #: 

807Q93 607Q94 B07QBO 

B07QB1 807Q95 B07Q96 

B07Q98 807Q99 B07QB2 

B07QB3 B07QB8 807QB9 

807000 


The holding time for the pH analysis was 

exceeded. Careful review of the QC analysis 

indicate the data is reliable. 

Sample B07Q93 (A2-12-047-01) yielded a 120% 

recovery for the Sulphate analysis. The high 

recovery can be due to the dilution required 

prior to spiking the sample in order to work 

within the calibration range. 

No other problems were encountered during sample 

analysis. All QC results were acceptable. 

r 

Ernest azq z 

VO 9Q °13- 

000011

TWA Inc. REPORT York Order / 02 o12- 

Received: 12114192 Results by Sample 

SAMPLE ID 007093 FRACTION Qjk TEST CODE YCCLPS MAKE Anions in Solids - VR232 

Date i Time Collected 12107192 1 Category 

ANIONS AND WET CHEMISTRY - SOLIDS 

ANALYSIS METHOD RESULT UNITS LIMIT 

Fluoride 300.0 1.5 mg/Kg 0.2 

PH 9045 7.7 pN .1 

Sulfate 300.0 50 mg/Kg 2. 

FORM I

000015 

IRA Inc. REPORT York Order ! A2-12-047 

Received: 12/14/92 Results by Sample 

SAMPLE ID 907094 FRACTION UL TEST CODE YCCLPS NAME Anions in Solids - 1111232 

Date 4 Time Collected 12107192 Category 

ANIONS AND NET CHEMISTRY - SOLIDS 

ANALYSIS METHOD RESULTNU ITS LIMIT 


PH 9045 6.9 PH .1 


FORM I

000016 

TMA Inc. REPORT York Order 9 A2-12-047 

Received: 12/14/92 Resutts by Sample 

SAMPLE ID 0070!0 FRACTION 2X TEST CODE YCCLPS NAME Anions In Solids - VN232 

Date L Time Collected 12/09192 Category 




PH 9045 8.8 PH .1 


FORM I

TMA Inc. REPORT York Order i A2o79-Oa7 


SAMPLE ID $07091 FRACTION 049 TEST CODE WCCLPS NAME Anions in folids - YR232 

Date t Time Collected 12109/92 Category 


ANALYSTS METHOD RESULT UNITSLIMIT 


PH 9045 8.4 PH .1 


FORM I

000018 

TWA Inc. REPORT York Order 0 A2-12-047 

Received: 12/14192 Results by saupte 

SAMPLE ID 107095 FRACTION Off_ TEST CODE YCCLPS. NAME Anions in Solids - MR232 

Date i Time Collected 12108/92 

- Category 

ANIONS AND YET CHEMISTRY - SOLIDS 



PH 9045 7.3 PH .1 


FORM I

000019 

TMA Inc. REPORT York Order ! A2-12-047 

Received: 12/14/92 Results by Suple 

SAMPLE ID 007096 FRACTION 0¢111, TEST CODE yCCLPS NAME Anions in Solids - UN232 

Date i Time Collected 12108/92 Category 



Fluoride 300.0 1.2 mg/K g 0.2 

PH 9045 8.8 PH .1 


FORM 1

000020 

TWA Inc. REPORT Work Order 8 A2-12-047 

Received: 12114192 Resuits by Sample 

SAMPLE ID 1107099 FRACTION 2ZL TEST CODE WCCLPS NAME Anions in Solids - WR232 

Date 4 Time Collected 12108/92 category 




PH 9045 9.0 pH .1 

Sulfate 300.0 17 no/Kg 2. 

FORM I

000021 

TRA Inc. REPORT York OPder 9 A2-12-047 

Received: 12/14192 Results by Sample 

SAMPLE 10 807012 FRACTION HL TEST CODE VCCL ►S NAME Anions in Solids - VN232 

Data i Time Collected 12110192 Category 



Fluoride 300.0 0.8 mg/K g 0.2 

pN 9045 9.7 pH .1 


FORK I

000022 

TNA Inc. REPORT work Order IF A2-12-047 

Received: 12114/92 Results by sampte 

SAMPLE ID 907093 FRACTIOU QM TEST CODE WCCLPSNAME Anions in solids - VN232 

Date i Time Cottected 12110192 Category 



Ftuoride 300.0 0.8 m g /K g 0.2 

PH 9045 9.2 pH .1 


FORM I

000023 

TWA Inc. REPORT York Order 8 A2-12-047 


SAMPLE ID 9070s8 FRACTION 108 TEST CODE YCCLPS MAKE Anions in Solids - YR232 

Date 6 Time Collected 12/09192 Category 




PH 9045 8.4 PH .1 


FORM I

I Nam 

• 2 6^/6m 9{ 0'009 070)inS 

Rd t'6 9106 Rd 

Z'0 071/Ow 9 . 0 0.009 oplion7i 

TPS[Y STM 11rim ZBIM SiS TM 

=0 11 0 4 - AV1stN3HO 1lR ONY SHOINV 

Moes700 POZOO1100 OW11 9 0700 

*Pilot 1NVN alt 1000 1331 f" NO{lovEd 69010i 01 3ldNVS 

s7does Aq :37nsay 26 1 yti21 %PDA10204 

1tO-2L-ZV 0 + sP+O VaOR 1sOd31 'sui V81' 

îî1t)()(1

Received: 12/14192 

TRA Inc. REPORT 

Results by Sample 

Work Order 9 AZQP AP 2 5 

SAMPLE ID 007000 FRACTION 12A TEST CODE VCCLPS NAME Anions in Solids - V0232 

Date t Time Collected 12/09/92 

_Category 




PH 9045 9.4 pH .1 


FORM I

TMA Inc. REPORT York Order 8 A2-T2-047 

Received: 12114/92 Results by Sampie 

000026 

SAMPLE ID 507098 FRACTION 139 TEST CODE UCCLPI NAME Anions in Solids - Y4232 

Date L Time CoLlected 12/08/92 

Category 

ANIONS AND VET CHEMISTRY - SOLIDS 



PH 9045 8.9 pH .1 


FORM I

Westinghouse 

Hanford Company 

Custody Forte Initiator Al-la , ÊTZEIL 

CHAIN OF CUSTODY 

Company Contact WV SETZER Telephone 376-2413 

P ro ject Designation/Sampling Locations 300-NR-1 Collection Date /•^' T9Z 

Ice Chest No. CMC- /7/ Field Logbook No. EFL- ,1062 

Dill oflLeding/Airbill No. 9s•'/ 900 76 23 offsite Property No. l/.2Y D-e/ZZol 

Method of Shipment OVERNIGHT AIR SERVICE 

Shipped to TMAMORCAL 

Possible Samale Hazards/Remarks None detected with field instruments. Maintain at 4C. 

` 

1^9 1,250mi 

Sasple Identifitati°an 

aG: LMetals,lig,Cn 

t4T 

1,120ml aG:CLP;VOA 

1,950ml aG: CLP; Semi -VOA, PCB/PEST,Anions (F,SO4,NO2,NO3)PH 

1. - - , - 

100S rz•7.gi 

- 

2) 07 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 

q^4 1,120ml aG:CLP;VOA 

1,950ml aG:CLP;Semi-VOA,PCB/PEST,Anions (F 

WVS /Z,7. 42. 

3) -i aG:CLP;ICP/AA Metals,Hg,Cn 

1,120ml a . I Vy 

1,950ml aG:CLP;Semi-VO (F 

1,1000ml G:Gross alpha/beta,Gamma Spec,Sr- 

NO3) 

14.U-235/238,Pu-239/240,Am-241 

(i Field Transfer of Custody Chain of Possess ion (Sign and Print Names) 

Reli is Received by 

^,Z aî 

Date/Time: 

Relinquished by: Rec4ived by: Date/Tina:: 

Relinquished by: Received by: Date/T ime: 

Relinquished by: Received by: Date/Time: 

Disposal method: I Disposed by- I Date/Time: 

D 

I A-iy-9 2- ®is oo 'k 

Ctmnents * 'Received /z-J2-92 is %M411V0tZji ; OPCN ed 14'IY-91- -1«3 

A-6000 . 407 (12/90) (EF) WEF061 

Chain of Custody

0 

Westinghouse 

Hanford Comr 

a 


Custody Fora Initiator 

Company contact WV SEEER 

Tetephona 376-2413 

Project Designation/Sampling Locations 100-NR-1 Collecti on oat& /$' 9.9ti 

Ice Chest No. O'Y)L 17! Plaid Logbook No. EFL- IM7- 

BILL of*Lading/Airbill No. 'd67 -?ao '74 1 - offsite Proper ty No. ^l^93ô D/Z231t.3^ 

Method of shipment OVERNIGHT AIR SERVICE 


Possible SamoL& Hazards/Reamrks None detected with field instruments. Maintain at 4C. 

sasple Identification 

1,250m] a metals,lig,Cn 


1,950ml aG: CLP; Semi -VOA, PCB/PEST,Anions (F,SO4,NO2,NO3)PH 

P41 ^ /z•^qL • 

2) ,& ^9^/ 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 

1,120ml aG.CLP;VOA 

1,950ml aG:CLP;Semi-VOA,PCB/PEST,Anions (F,SO4,NO3) 

3)aGXLP;ICP/AA Metals,Hg,Cn 

1,120m1 a : wv5 

1,950m1 aG:CLP;Semi-VOA,P 

SO4,NO3), 

1,1000m1 G.Gross alpha/beta,Gaflmla Spec,Sr,-90, - 

35/238,Pu-239/240,Am-241 

f1 Field Transfer of Custody Chain of Possession (Sign and Print Names) 

Reli fished Ree IVed by: 

" 4 ^ 4 

Relinquished try: Rece4ved by: Date/Tim- 

Relinquished by: Received by:

9 

I 

Westinghouse 

Hanford Company SAMPLE ANALYSIS REQUEST • 

Collector &- 497-= ^ e^ Date /2-iD • 92, 

Company Contact WV SE17ER Telephone (509)376-2413 

Sample 

Number 

Date 

Collected 

Time 

Collected 

Number and Type of Sample Containers/Analysis Required 

1-250mi aG CLP;ICP/AA Metals,Hg,Cn 

1-120ml aG CLP;VOA 

1 r950mi aG CLP;Semi-VOA,PCB/PEST 

„ o7D93 S /.2 7 .92 O io b Anions(F,SO4,NO2,NO3)FH 

„'^;,,, ' .qzU-335,L238o,i?ao;?dnro _^n1 

4 

1-250mi aG CLP;ICP/AA Metals,Hg,Cn 

/ 1-120mi -% CLP;VOA 

1-950ml A CLP;Semi-VOA,PCB/PEST 

AP4,94 $ /-'7 . 7-9z / 19^ Anions(F,SO4,NO2,NO3)PH 

6kJn9 /L - /O •S LL 

1-250ml aG CLP;ICP/AA Metals,Hg,Cn 


-950ml aG CLP; Semi -VOA, PCB/PEST 

^TT /^ z /' L Anions(F,SO4,NO2,NO3)PH 

Q/v5 /L'/6 • c!L 

- 1 



-950ml aG CLP;Semi-VOA,PCB/PEST 

DTI B/ /^• j/J/5 Anions(F,SO4,NO2,NO3)PH 

1--I.890m1 r r -^••h-/ti +- r^ c ,• c^_on1•_1^ 

us 

*Type of Sample A = Air „L = Liquid SE = Sediment T = Tissue X, Other 

DL = 'Orum Liquids O = Oil SL = Sludge W = Water 

DS = Drum Solids S = Soil SO = Solid WI = Wipe 

Field Information FROM 100-FR-3 Drilling 

Special Handling and/or Storage Maintain at 4C 

Possible Sample Hazards NA 

A •6000-406 (06/91) WEF060

1 

r Westinghouse 

L ..Hanford Company 

n 

Cdatody Form initiator 

Canpany Contact 

(4la , 5,-77- =VG 


WV SETZERTelephone 376-24I3 

Project Designation/Saipling Locations 100-NR -1 4 Collection Date /17•y. 9z 

Ice Chat No. S)9)L a3 S Field Logbook No. EFL- 1642 

Bill ol*Lading/AirbiLL No. 0- .`/ 904 7A Z'T offaite Proper ty No. AA79 Q-6 = 91°' 



Possible Sample Hazards /Reeatrks None detected with field instruments. Maintain at 4C. 

,ZSUMI au:l.i.l r ;I6l`/AA rletials,ng,l.n 

,120ml aG:CLP;VOA 

%?, 950ml aG:CLP;Semi-VOA,PCB/PEST,Ani.ons (F,SO4,NO2,NO3)PH 

2 ftwas /z. ,t' .Tz— 

2)&7q6 'q ,250ml aG:CLP;ICP/AA Metals,Hg,Cn 

v1,120ml aG:CLP;VOA _• 

q 950ml aG:CLP;Semi-VOA,PCB/PEST,Anions (F,SO4,NO3) 

, 

was /x • td •4L 

3),go7,p ,?R250ml aG:CLP;ICP/AA Metals,Hg,Cn 


`/1,950ml aG:CLP;Semi-VOA,PCB/PEST,Anions (F,SO4,NO3) 

ltJUS yZ•ia•gL - 

fl Field Transfer of Custody Chain of Possession (Sign and Print Names) 

Reli fished : Rea ived by: Ml -. h 73 )^ 

Date/Time: 

1-1-H-91 &?00 

Relinquished by. Received by: Date/Time: 



Dlsoosal Method: I Disposed by: I Date/Time: 

comaents: * geceived @ 7mAl Y'oaecol I2-/2-92 

A-6000-407 (12190) CEO) WEF061 

Chain of Custody 

oêNed /2 /y-9z -W3

I 

r Westinghouse 


0 

Custody Form Initiator 

Ccmpsny Contact WV SMER 

/ 

//l 11 rC^,GTL . 3! . 

P roject Designation/Sampling Lo ca tions 100-NR-1 

Ice Chest No. rs rnt! ^3't 

Dill of*Leding/AfrbitL No. 

NQthod of Shipment OVERNIGHT AIR SERVICE 

shipped to TMA/NORCAL 


Telephone 376-2413 

Cottection Date 

i yp^^9^t ,L5UmI ata:LLl';1t.V/ AA McLais,Ng,Ln 

1 120ml aG:CLP;VOA 

1,950ml aG: CLP; Semi -VOA, PCB/PEST, Anions (F,SO4,NO2,NO3)PH 

241 

wus ^F.yZ 

1L•S' 9r 

Field Logbook No. EFL- J6t'.t_ 

offsite Property No. /Lq,; -el -612Z'Ep 

2) 250ml aG:CLP;ICP/AA Metals,Hg,Cn 

1,1 G:CLP;VOA 

1,950ml aG: i-VOA,PCB/PEST,Anions (F,SO4,NO3) `—' 

1,1000ml G:Gross a p Gamma Spec ,Sr-90,C-14,U-235/238,Pu-239/240,Am-241 

3) 1,250ml aG: CLP; ICP/AA Metal s, Hg,Cn 


W US 

1,950mi aG:CLP;Semi-VOA, PCB/PEST,Anions (F,SO4,NO3 

1,1000ml G:Gross alpha/beta, Gamma Spec, Sr-90,C-14,U-235 Pu-239/240,Am-241 

r Field Transfer of Custody Chain of Possession (Sign and Print Names) 

Rat fishad h; Received by: KQ/^M I'f- )JItMT 

Date/Time: 

Relinquished by: Received by: Date/Tim- 

Relinquished by: Received by: Date/Tim- 

Relinquished by: Received by: Date/Time:- 

comments: *Rece;ved G 7MA190RCA1 ; ope.ved lz-1 `1-92 • A13 

A-6000 .407 (12190) CEF) WEF06 1 


tion 

in 

u-

El 

Westinghouse 


SAMPLE ANALYSIS REQUEST 

Collector /Zjej— &Erzee— Date 1,7 •10.92_ 

Company Contact WV SETZER Telephone (509)376-2413 

Sample Date Time 

Number Collected Collected 

g 12z ,I9 /^S?4.^ 



1-120mi aG CLP;VOA 

1-950m1 aG AnionVOA,PCB 

( F , /PEST 

Anions (F SO4,NO2,NO3)PH 

d lUS/3• d • 4L 



1-950ml aG CLP; Semi - VOA, PCB/PEST 

,^v/ y //i, S /Z X 4L 11)1,5, Anions(F,SO4,NO2,NO3)PH 

w _ 

— $ /^ S 92 /^^D Anions(F,SO4,NO2,NO3)PH . 

/J ,.^ 

^(7//C3 '7 j 

(.vv5 /Z • /a •4 z. 



1-950ml aG CLP; Semi -VOA, PCB/PEST 



1-950ml aG CLP; Semi -VOA, PCB/PEST 

^'T S I^•9.9z /^cb Anions(F,SO4,NO2,NO3)PH 

' u- 2 - 

"Type of Sample A = Air L = Liquid SE = Sediment T = Tissue X-= Other 

DL = Drum Liquids O = Oil SL = Sludge W = Water i 





A •6000 . 406 06/91) WEF060 

d

C 

Westinghouse 


Custody Farm initiator 


Capany contact WV SETZERratephone 376-2413 

Project Designation/Sampting L ocations 100-NR-1 Y Collection Date /,;? • ID-9a 

Ice Cheat No. ,Sm L— /^ 9 e 

^^t ?/^ fi^-1 rf 

BUl aflLading/Afrbitt No. 0k5 I " i Ott /loVq 

Field Logbook No. 

offsfte Property No. 

FF{,_Li1i0^ 



Possible Sample Hazards/Remarks None detected with field instruments. Maintain at 4C. 

1 07a4aR 1,2 Om aG:C 


AA Metals,Hg,Cn 

1,950ml aG:CLP;Semi-VOA,PCB/PEST,Anions (F,SO4,NO2,NO3)PH 

> -> > - 

/z•ro 

444— 

2si33 1,250m1 aG:CLP;ICP/AA Metals,Hg,Cn 


1,950ml aG:CLP;Semi-VOA,PCB/PEST,A nions (F, SO4,NO3) 

> ,.. r > ice_,._ .._ ii 2'tr tti'tfi—Ri 9-'123/L.49 9d1 

3) 50ml aG:CLP;ICP/AA Metals,Hg,Cn 

1,12 P;VOA 

1,950m1 aG:CLP; PCB/PEST, Anions (F,SO4,NO3)' 

1,1000ml G:Gross alpha/be a, 

c Sr-90,C-14,U-235/238,Pu-239/240,Am-241 

rl Field Transfer of Custody Chain of Possession (Sign and Print Names) 

Re ' . hed by-,J)? Ree des 

Reeeived by: Ke&M i •f- U IdAl Date/Time: 

M 



Relinquished by: Received by: Date/Time-- 

Disoosat Method: I Disposed by: I_ Date/Time: 

Comenrs:* Rere;ved /2- l 2-9z @ 'TMalNo c,41 , ®peved 1.2-1 11-92 •KB 

A-6000-407 (12190) CEF) WEF061 

Chain of Custody

Westinghouse 

Hanford Company SAMPLE ANALYSIS REQUEST , 

Collector . I R, Date 12 4 &9 0 ,a 

Company Contact WV SMER Telephone (509)376-2413 

Sample 

Number 

Date 

Collected 

Time. 

Collected 

Number and Type of Sample Containers /Analysis Required 



1-950ml aG CLP;Semi-VOA,PCB/PEST & pH 

Q07 S ,?_/O_ qa 084. 7 300.0/353.2;Anions (IC) F,SO4,NO3, NO2 

S Q=Qa 133'7 

Il,q 

n nne /eee n ewe /nnn •_ n., .f6? 

-250ml aG CLP;ICP/AA Metals,Hg,Cn 

-120ml aG CLP;VOA 

1-950m1 aG CLP;Semi-VOA,PCB/PEST & pH 

300.0/353.2;Anions (IC) F,SO4,NO3,NO2 

. q..^ rnnn n Mn /9An 11..._9A7 _ 

V GJ J/ LJ , 

Â:V /f 'Z- 




300.0/353.2;Anions (IC) F,SO4,NO3, NOZ 

1-1000ml G Gross alpha/beta,Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 


120ml aG CLP;VOA 

1- 1 aG CLP;Semi-V0A,PCB/PEST & pH 

300.0/353.2;Anions (IC) F,SO4,NO3, NO2 

1-1000m1 ross alpha/beta,Gamma Spec,Sr-90,C-14 

- 35/238,Pu-239/240,Am-241 

*Type of Sample A = Air L = Liquid SE = Sediment T = Tissue X = Other 

DL = Drum Liquids 0 = Oil SL = Sludge W = Water 

DS = Drum Solids _. „$ = Soil SO = Solid WI = Wipe 

' I Field Information FROM 100-4?R-1 Drilling 

Special Handling and/or Stora a Maintain at 4C 


A-6000-406 (06191) WEF060

Westinghouse 


Custody Fare Initiator ^7R REESI/F4 


goapmn. contact WV SETZER Telephone 376-2413 

Project Designatio n/Sampling Location: 100-NR-1 Coltectfon Date /a-09-93• 

Ice Chest No. Sin L /7,Q Field Logbook No. EFL- 1613 

Bill of*Lading/A1rbitL Me. VS/ 1700 7/ 2 S 0"afte Property No. 



Possible Sample Haza rds/Reaerks None detected with field instruments. Maintain at 4C. 

Sasple identifi cation 

Metals,Hg,Cn 

1 8 1,120m1 aG:CLP;VOA VOA 


1,1000ml G/P:Gross alpha/beta,Gamma Spec,Sr-90,C-14,U-235/238,Pu-239/240,Am- 

241 

2)6ot7mBq 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 



1,1000ml G:Gross alpha/beta,Gamma Spec,Sr-90,C-14,U-235/238,Pu-239/240,Am-241 

3)807000 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 




() Field Transfer of Custody chain of Possession (Sign and Print Names) 

Relinquished by:iyR 

S /a-09 9 

Received by: 

G•

e 

Westinghouse 


I fry %WZ-- 


Collector Date 11•10 -4L 

Company Contact WV SERER Telephone (509)376-2413 

Sample 

Number 

Date 

Collected 

Time 

Collected 


v -250ml all CLP;ICP/AA Metals,Hg,Cn 


p^Q^ ^' 

S /,2.1- L 091/7 

950ml aG CLP;Semi-VOA,PCB/PEST 

Anions(F,SO4,NO2,NO3)PH 

d-1000ml G Gross alpha/beta, Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241. 

' 



S 

/2 ^r•9^ 09-^-a 

1-950mI aG CLP;Semi-VOA,PCB/PEST 


1-1000ml G Gross alpha/beta, Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 

-250ml aG CLP;ICP/AA Metals,Hg- rCa- 


\,r-950ml aG CLP;Semi-VOA,PCB/PEST 

L^17{^CD S !x`42 Anions(F,SO4,NO2,NO3)PH 

—' -1000ml G Gross alpha/beta, Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 



1-950ml aG CLP;Semi-VOA,PCB/PEST 


1-1000ml G Gross alpha/beta, Gamma Spec, Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 

wV$ 


OL = Drum Liquids 0 = Oil SL = Sludge W = Water 





A-6o00 =406 (06/91) WEF060 

M

SAA U twig put 00,0003 

or ." tot avert. 1 -. 4 t h^l . l h toA-iR-RAT[ : I OA115 /4,^Q- 

K[IY( O R, ISIGNATtA 

CASE RIAIM , 

LWtE Ml— 

us RlleQ: 

6 WO'Ll 

/ 

f TAB 

0 

marcsrololR; 

Atf^ 

YY) — 0507 G? 89 1i^ la 7_11 

1. Custody Seal(s) ejff%-eWWMawt• 

1 ae %rata. 

2. 

Custody Sot% Rot: 

. Chain of Custody(: s^n /Absent• 

Records 

Traffic Reports In /Abawtor 

Packing list 

S. Alrbtll ^tckat 

seet• 

^ I I 

. Alrblll No.: 51 O To^^71 

7. Saeple Tags Proton eat• 

• Saaple TagsUs pbt Listed on 

Rbers u 

Clint of Custody 

• Sample Conditl 

IO.Does Information ^ts/RO• 

on custody 

records. traffic 

reports. and 

sample tags agree 

11.0ate Raclered at tab: f 

! 

1 \\lllq rctml•/ 

12.Tenp of lea cheat ^, C 

I3.Tlae lettered: 

fractton: 

By: 

SMRitE TRAXWO 

- !" 4109% AO aka etteCa rlCare of ree010t%" 

e0r10wa art t0e000t sr.r 

au. Late"41 ra te 00.8 

bM^.11 

roan oca 

^7 q A^- la•O'tr2-ob 

^07G1-1^- 

SZ7ag 15 Az-13- v_t 

0 

Air 11-o^1^1-0 

!X37Q5 197 fl^ 1^-o•fvIIJ 

CDROITÎOR i 

SMlIE SMIhENT fig 

'

[t[I g[D IT ( ►RIMT IIARII: ,_List 

RtITII) m y11 1"A1 

CASE MIEtl: 

SAMPLE ULLITLAT 

GROUP p.: 

SAS Ri•lER: 

bill . 

_n l 

SAWU L06-111 SECT 

%^ SAIKE 

• 

S TA6 

• 

la-11-an 

cwaEwmin 

W 

ePARKs: CÎt^ oa.i^ ct19- 

1. Custody Satl (s)nf- t/Absent• 

t/Rrcke11 

2. Custody Seal ISO: 

1. Chain of Custody Insent $ants 

Records 

. Traffic Reports Inun /AbswdO 

or ►acting list 

S. Alrbill Irbi /Stick" 

t/Absents 

. Alrbfll M.: 

T. Sample 

5rr^js}^7^ 

sent• 

. UWIG Tags td an 

Tagsrtomfoctustz 

S. Saeplo Condition: robsn•/ 

10.Ooes Information 

on custody 


reports, and 

sample tags agree 

(:3$)"o" 

ll.Date Reclered at lab: â 1^ Ct 

12. 1'eep of tee chest 

13. 71me Rectered: 

F raettom 

Arco •: 

By: 

UVII TRMSFIM 

• !"last 90 sad attata "stare of raUlattes 

ea.taMe Sys hobs" Ira.# 

stet bribe" Iqe Mat 

raw ot-t 

^7^ t IYaa^l_O8 

/^7QIo^. ,qa- 1 - 

C7C^Y a3-1.1-cr19-cq 

U 1 4P A.I-Ia-^'t9 - lt 

IF 

CDT OF 

SHIH[R 1

- 

SAMIPU tea IN SWO 

l yEO IT (MINT NAMI: I r t-1 

ri^.urtl 

t/&-iN•OATE 

tit IIIY 61 DItW11@t 

IRMM: 

SAIME UELITUT 

GROW ND.: 

SAS VJM: 

I. Custody Seat(&) .LL&R m'bt/Absent• 

,- i Sct/Irok so 

2. Custody Seal Nos: 

. Cholo of custody Pres t• 

&scores 

. Traffic Reports iR4WADssnt• 

or ►aoklnp list 

S. Atrblll 

^-^MefM ^- /Sttckar 

t/Absamt• 

N. AlrO111 No.: 51t3S6 o7 2 

7. Sasplo Taps 

. Sample Paps /lot listed on 

numbs" l_mts of ^ssnt• Custody 

. Sample Condition: Intac rokM•/ 

IO.Does Infor mation / tn Me 

an custody ^/ 


reports. and 

sample taps .pros l ) 

11.att Recteved at tae: [/ 

MUM of ice chest t 

13. 11 sle Recteved: 

Fraction• 

Area /: 

/y: 

On: 

SAMIE TRANSFER 

o 

"SN A 

^7 

• CNt••t 90 tM •tt•cs mere of r•tet•tl oa 

b.ltwa all tMtmmt MAt 

- -- -^ .000005 

UNIX 

1 

C0&&ETF4Dli 

AM ON 

/ 

pa^l3-oIj•1cY-I 

Ad.! - 6 

aA- la 4 

a 7 o aa- ia-d4 

q 

a.- 

t7 A.t-!^ otlq-o 

d Ate+-I.Z^d1f-i-ol 

ott*t t•eatea Page Me•t 

raw tlt.t 

c^reô^c^be—rcc^.lu^ r^ls a

—UU0-006 

SAMU LWIR MCI r i 

ECElva IT (PRIN T 1: 1^ o k._1, L06-11-RAn : (d 115^`Y2 

.l....... ^...... 

IR1lR: 

SAIRE DELliOT 

0W RD.: 

SAS 

REt1ARRS: 

1. Custody . Seal(1)ent• »a^ ii t !abs 

/srok.n 

. Custody Seal Nos: 

. Chat. of Custod ►r.s.nt/ ant• 

Records 

. Traffic Reports Absent' 

or Few no list 

S. A1rb111AIMII ticker 

IAbeat• 

. AIrb111 No.: î¢ $G`^'oYP7^ 

7. Sawle tags (^liDt.nt• 

S. Semple Tags List t listed on 

IltwWrs Custody 

. Sample Condition: Intac /Rrck.n•/ 

h 

ID.Does Information pa 

on custody 


reports, and 

awls tags agr.. 

11. 0ate Reel d at tab: 

iaJ ^s 6.a 

11.Teaq of ice chest 'C 

is.Ttee Recievd: 

Fraction• 

Area 1: 

Ry: 

• CMtest " end et leea f.r.re of f Utb0 

- 

^ . -PA 

SHIRE 

• 

wi 

",low" art t"beek a.t 

SANIt 

TAS 

IF 

O 

CQWVMIfi 

Anion 

W/ 

-U-aRI'4 

Q^^'^'E'•^g 

A3 - I J..d^B- 69 

^ÎS^ IG 

y- 1-a-o^sA7 

I? -d^^-O 

^^ -Ie1-6'^7^'i3 

â- la_cFB-o5 

pa- la- ^-o 

Ia.°.yj^ 

807 g A"14 P-off•-6 

p^- la-a4E-a 

7 5 

6.108 tgawk /sH 06.8 — 

rosl aC-1 

R[IIAAKf: 

CMITION OF 

SANRE SN1rtENT E; 

-:^ BaoQrea- Kci.:.yecQ a uâ bCt.r.(Îf,^ :+bid.: or,tvaw ^+ s^.r.,p^2

atom 

of (PRINT UM): 

Custody Sul(e) ssate 

rokw 

Custody Seal Mot: 

Chain of Custody -44 sm Abss t• 

Records 

/,^'^^^ 

Traffic Reports LXisantyAbseala 

or Iaoktnq List /;;Ê 

AirbillAi t11 ticker 

/Absot- 

Alrblll Va.: 

. Sample Tags Mtm Absent• 

. Sap1e Tags t st Not Listed on 

Numbersof Custody 

. Simple Condition: tmtac Rroksma/ 

nq 

D.Does Information Te - 

Cn Custody 

records, traffic 

reports, and 

sample tags agm 

I.Date Racteved at Lab: 

t.Ump of ice chest 

aZ 

• CNIKt sm eN attack racers at r-m-rYtoM 

SAMPLE toll vat -000007 

CQR[SIORDIi 

VA SNlt2 A 

SAMPLE IJA 

r CT7 

aele.ae an taswk 116.1 

ate$ tga«k rasa me.$ 

wuwa.a 

YOM VC-1 

p.1 — I 1-GK-1 

oka^ 1.0-44A- 

yr^â-Rare-ut 

^^ A?-1 A.o .aE 

A3--1^-..attS-d4 

^J Aa- a.2.e4g- I6 

8p QA-1 

Qyla.Gaf4

sAMFU LWIR OUT 

0 

LAS RAMP ►A/t aF 

RECEIVED 11 (MIT MAX): 

[CEIVto IT SIG1Alilt[ 

CAK RIIQ[R: 

SAIR+tE OEIt T 

GROW RO.: 

REMARKS: 

1. Custody Seals) rasa /)bast' 

Irokas 

2. Custody Sat In: 

Chain of Custody ►n Absest• 

Records 

. Traffic Reports ^/Absast• 

or tacking L ist 

S. Afrbtll Atrbtll/Stftkor 

Present/Abssst• 

G. Afrbtll No.: 

51 P b ^

u' 

QUESTIONS? CALL -5355 TOLL FREE. 

5188742672 

AIRBILLw„ 5"88742072 

cM u eEfi1^ 

2 3,1• 

°•^ 

1, Fv vz. 

- - - - - HECPWVl B S COPY , - 

Qr( , Prex Y. Rm linbr cw" MOUi+,1 Te,Rx9w^lMrrolNww 

Prw •.1 ..• MceiM.naw Mr.w nM'weos3n 

----/^ 

Cam" 

A 

- DepubrwMFb ?40 ConV" D&P& msl0lmw 

Soew AOAVaa E. Str (W C^wf DAWm to hmw o A, Cnln) 

.y 

p 

Cfry^ Suls jp Peprretl COY Swa jpNaOWrEo 

^1CNI5l h ^ ,.: 9 4 r: L t1nN do v^fl 1 GA `7/^ 6 

MGM ÊFER MEff00Wn M Wkb ) ffAW24 OWOM will WMYOW) iSN01MDHxIM°C11!RMF^f1YA6fw /M 

'3 < v o ff. ^.. 

Yi6lf f N6wea 2 e.Wgwn. r,eE./s ua ] tMlarW r.¢f.Mg me Mu.a Cwa 

yprin ^ 

CM Sias NaP.rM 

SENYICES DEIIYfRYANDSPfCULNMlAF0 """"' M 

• ,arwpurp fmp. No Wk that 

(CMr,Y r++Y wr fic+l 

(CON^'eârvcra're' ewe0) 

At*awiry. 

_ 

q uwensr^.w-- 

l^ 

•.._.^^. "" 1 pHOLp FM tF.wao.ro 

rr......, ^'= 

R....m W ,mM W 1•IM, 

„ row rout 

°i^^^•^^• 

W MfXNGK q n¢x1crF 2 pantaf lRYRUr SVMMde,•^ 

16 pF2EE1f,fR9 56nWLEDEO• q D wwr, ^•D'iâmu iq ^:: {'^ f3ewr l 

12 pFaum-. 52 p FEDEYM.Y • 4E]WWEx G000Sd—d r• 

CM Saxe Zo 

13E]R MWX 53pFMaM 5p Td•1 TWsl TOM • °tl"r2 

1ap RM ME 51 pFE0fl ME 6p^. ICf.. r w h .3 75 X Bl' 

TdY CNrpN-^__^ 

6ovay 0a 0~ 

a-nea^ n .+"....w.......-. .. 

i q OMEN SFFC pp15hrolix2lcn.,a.,w. Y/.9.9 

, 

I^r.,.^^ 

"'^'^ 

OaW,^ma R•cwvee faOE. Enfixoyee NUmeer 

Orr 

_ 

FM _ .•.. 

30 p ECV6 W tl p lfliu 

:ap f EppFrnâr 

6 q , ' q E, w w 

•f p= GF 9 p &1MM1•FCKJA' _ 

op 

L 

q 

- 

x x' N 

_.. 

pnpwsao lno-oofio 

r^n pk plFY MI MAY -.+-.+ .1 P CC Ne4av 

romwr.ux 

12 61 

9wRRmgl 

MwrEOw

TAWAll[I 

Taeer Aeelte,ol la 

RADUATION DOSE RATE SURVEY FORM 

Dille G COWAW -11-?Â L wHc OTHERORD 

Swwyor'a Name —Z?'O,PK 5, /^ / 3 

000010 

5 r88o y^ ^, %^' 

Model No. Model No. AG1 7/ Fsf•I 

Serial NOL 710219 1 O 619 Se rial Noy 407M 

CAma slioa Dale _1^^0<

Page 1 Skinner&Shermm REPORT Work Order f S2-12-219 

Received: 12115/92 01/15/93 14:45:42 

REPORT TNA/NORCAL PREPARED TMA / Skinner & Sherman Labs, 

TO 2030 Wrfaht Ave" ,—BY 300 Second Avenue 

Richmond. CA 94804 P.O. Box 521 

Waltham, MA 02254 CERTIFIED BY 

ATTEN Dan Steurmer ATTEN Client Services 

PHONE (617) 890-7200 CONTACT DP 

CLIENT HANFORD NOR 

COMPANY TMA/NORCAL Hanford 

FACILITY Richmond. CA 

SAMPLES 14 

LARK TO N2-12-073 

TAKEN BY CLIENT 

TRANS FED EX 

TYPE SOIL 

P.O. Y N2-12-075 

INVOICE under separate Cover 

SAMPLE IDENTIFICATION TEST CODES and NAMES used an this rorkorder 

21 807a93 NITR S Nitrate/Nitrite in Soits 

2a 807094 

Q 8070BO 

PA 807061 

a 807095 

03 807096 

2Z 807098 

08 BO7a99 

09 807002 

10 807083 

11 807088 

jZ 8070B9 

13 U07000 

•2 807000 OUPL 

L 807000 SPIKE 

1k LCSS

0000.02 

Page 2 SkimerMeraan REPORT York Order Mi S2-12-219 

Received: 12/15/92 Results by $aple 

I 

SAMPLE 1D 807M SAMPLE N ,, FRACTIONS: A 

I NTTR S

LW0003 

Page 3 Skimer&Sherom0 REPORT York Order i 52-12-219 

Received: 12115/92 Results by SapLe 

SAMPLE ID 007099 SAMPLE R M FRACTIONS: A 

DatQ,L Time Collected 12!09/92 Category SOIL 

NI7R S Q.i9 

mR N/kg 

SAMPLE IO B07QB2 SAMPLE Y QQ FRACTIONS • A 

Date i Time Collected 12/09/92 Category SOIL 

MITR S Q.N. 

mg N/kg 

SAMPLE ID 1107M SAMPLE / 10 FRACTIONS:1A 

YITR S 0_52 

mR N/kg 

Data At Time Collected 12/09/92 Category SOIL 

SAMPLE ID 1107098 SAMPLE Y ,, FRACTIONS: A 

Date i Time Collected 12/09192 Category SOIL 

YITR S 0.56 

mR N/kg 

SAMPLE ID 807089 SAMPLE / U FRACTIONS • A 


YITR S Q.AS _ 

ma .N/kR 

SAMPLE ID BMW SAMPLE f y{ FRACTIONS: A 

Date Q Time Collected 12/09192 Category SOIL 

YITR S Q.i6 

mu N/kg 

SAMPLE ID B07000 DOPL SAMPLE 0 J3 FRACTIONS: 0 


YITR S Q.A2 

wNA9 

iis'mvtmiYi âcYeRw6oilk! mvdce'r iNi

Pape 4 SkimerLshersan REPORT Work Order i 52-12-219 

Received: 12115/92 Results by Sampte 

SAMPLE ID 807000 SPIKE SAMPLE / U FRACTIONS: C 

Dsta,i Time Collected 12/09/92 Category SOIL 

MITR S 19.4 

mg M/kg 

SAMPLE ID LCSS SAMPLE 1` 14 FRACTIONS: A 

Date i Time Collected not specified Category SOIL 

MiTR S 2.03 

Rp N/L 

()000Q 

- —_ :TNirtPm Yrcnda HUpondldl pefalkwirigcvdi,ime: 5timvRSMms,la6ontaria.irc.rcnirowvie^Td NUrtpwtwtilumciercd,ubmine6invd¢'v v^. 

_-.. .. ^'' Faorrtwimmcrvixv dull heavul^bicfemniuc^lonwi,M1,A"swu,ml y ifmlarmifÎmdNfsmtari^rtauimrcntwu mdeaM,aepeQ6efaetlwrWniw- 

3ldAvenue, P.O. BOxS21, Waltham Massachusetts 02254 05 

CAB TEST, FAX.(617)890-38a3' - - 

_

Page 5 Skfiner&Sherman REPORT Work Order 9 S2-12-219 

Received: 12115/92 01/15/93 14:45:42 

TIWRORCAL Ha nford 

QUALITY CONTROL 

MATRIX SPIKE 

Sample ID Sample Result Spike Added Spike Result % Recovery 

S212219-13

000()CC 

Page 6 SkirmAStmr REPORT York Order _t S2-12-219 

Received: 12/15/92 Test Methodology 

TEST CODE MITR S MAKE Nitrate/Nitrite in Soils 

Method not ovsilabte.

7MA 

Thermo Analytical Inc. 

Skinner & Sherman Labs., Inc. 

300 Second Avenue 

Post Office Box 521 

Waltham. MA 022540521 

(617) 890.7200 

FAX (617) 8903883 

January 19, 1993 

TMA/NORCAL 

2030 Wright Avenue 

Richmond, CA 94804 

Attention: Dan Stuermer 

duality Control Narrative 

X30 /) Q g3- ?m^^` 

SCE DW 

Scope 

Ten (10) soil samples were submitted to TMA/Skinner & Sherman 

Laboratories, Inc. on December 15, 1992 from TMA/Norcal. The 

samples were analyzed for the USEPA CLP Target Analyte List 

metals and cyanide. The analysis were performed under 

TMA/Skinner and Sherman work order S212218. 

Methodology 

The samples were prepared, analyzed and reported in accordance 

with the USEPA Contract Laboratory Program Statement of Work 

ILMO2. 

Discussion 

All quality control requirements were met for the samples with 

the following exceptions; 

The antimony, manganese, selenium and cyanide digestion spike 

recovery exceeded the control limit requirements. 

The ICP serial dilution for zinc exceeded the control limit 

requirements. 

The calcium, manganese, and zinc laboratory duplicates exceeded 

the control limit requirements. 

Please feel free to call if there are any questions concerning 

this package. 

Respectfully submitted, 

TMA/SKINNER & SHERMAN LABORATORIES, INC. 

David N. Peterson 

Assistant Laboratory Manager

WESTINGHOUSE/HANFORD 

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE 

Lab Name: SKINNER & SHERMAN LABS. Contract: 68-00-0108 

Lab Code: SKINER Case No.: N2-12-073 SAS No.: SDG No.: B07093 

SOW No.: ILMO2_ 1 

$AMPLE NUMBER: 

B07093 

B07C,94 

507095 

607096 

807098 

607099 

S070F.0 

07061 

B07082 

607063 

B07OB8 

6070B9 

807000 

B07000O 

B071DCOS 

Lab Sam p le ID. 

12218-OIS 

12218-02S 

12218-05S 

12218-065 

12218-07.'. 

12218-OSS 

12218-03S, 

12218-04S 

12213-095 

12218-10S 

12218 - 11S 

12218-12S 

1218-13S 

1218-1.:'S2 

12218-13C)• 

Were 1CP _orr•ections a pp lied: Yes/No YES 

Were LCP :orrections app l i-d? - Yes/No YE5 

If =s-were raw data •generate(,- before 

app lication of background corrections? Yes/No NO 

Comments. 

I that this data Dack.age is in c r mp liance with the terms and 

:onditi: , ns :, f the contract. both technicall y and for comp leteness. for 

other than the conditions detailed abov?. Pel.°ase of the data contained 

in this hardcory data Package and in the computer - readable oata submitted 

::n f L::^•Dr •9Lsk.ette has been authorized the Laborator y Mana ger , or the 

Manager' E. desi gnee.. as verified b y the following signature. - 

gnaturs: — 3c.._.- _ :^.^ _ .v;^me: David N. Paterson 

Date: •/' ^/^1% 3 Title: Asst., Labohator •y Manager, 

4,1A 

COVER PAGE -^ ..N ^_ ILMO2.1 

_


1 

INORGANIC ANALYSIS DATA SHEET 

Lab Name: SKINNER & SHERMAN LABS. Contract: 68-D0-0108 

i 

Lab Code: SKINER Case No.: N2-12-07 3 __°.AS No.: 

, 

SAMPLE NUMBER: 

807493 

SOG No.:.B07Q93 

Matrix (soil/water): SOIL Lab Sam p le ID: 12218-OIS 

Level (low/med): LOW Date Received: 12/15/92 

Solids: 93.9 

Concentration Units (ug/L or m9/Kg dr y wei ght): MG/KG 

;CAS No. Analyte :Concentration :C; Q :M 

1 7429-90-5 !Aluminum 4330 IP = 

;7440-36-0 Antimon y _.7 :U! N :P: - 

17440-38-2 !Arsenic : 1.6 :B: S :F 

17440-39-3 :Barium ::5.6 , , :P 

;7440-41-7 :Ber•y i1ium: 0.211B! 1P- 

;7440-43-9 ;Cadmium 0.32:U: ;P, . 

17440-70-2 :Calcium 5140 :P 

17440-47-3 :Chr,.>mi Lim 

7.4 : 1 :F 

!7440-48-4 :Cobalt' : 13.6 ; !P- -' 

: 74&0-50-S 1 Cou pFr- 30. 6, 

17439-89-6 :Iron 25400 

: 743'a -92- 1 : Lcad ._ ... 1 -. _- 

:7439- o- -4 , l9a Ines i Lim: 4060 1 P 

' 74 3r:^- ''.47- 6 :Merr.'ur y 0.05!U: :QV' _.. 

7,5.40-02-0 ;Nic F.•eL 7,•? :B: :P 

17440-09-7 :Potassium: 486 :B: I?. 

17782-49-2 :Selenium 0.99! 1 + :F 

:7440-22-4 :Silver 1.2 :B! :P 

:7440-23-5 ;Sodium 368 :61 :P 

:7440-28-0 :Titallium 1 0.30:U; 1F 

17440-62-2 :Vanadium 59.1 1 : 1P 

17440-66-6 :zinc 1 47.E 1 1P 

: C y anide 0. 53: U 1 N : CAI 

t; ,iLor BROWN CLar Lty 3e-fore. 7exturu : .. MEDIUM 

Color After: BROWN Clarit y After: Artitaots -: YES 

(-omment S: 

ROCKS 

FORM I - IN 

ILMO2. 1

.,vay.rvwuwvv.n.. •..,...o.wvw.,.......^.....o. .... .... ......v..v,.r.....vounowua:ao.wvuwwww.ra,.ww....... ......uuvwv.•,.nan:.u.. aw"w ... ... w+wm.wm+uwwawuurouawaw.awww. 


1 


Lab Name: SKINNER & SHERMAN LABS. Contract: 68-DO-0108 


B07094 

Lab Code: SKINEP. Case No.: N2-12-073SAS No.: 'SDG No.: B07093 

Matrix (soil/water): SOIL Lab Sam p le ID: 12218-02S 


% Solids: 95.7 - 

Concentration Units (u g /L or mg/Kg dr y wei g ht): MG/KG 

.CAS No. Analyte ;Concentration:C: Q :M 

7429-90-5 :Aluminum I 3940 

7440-. =-0 :Antimon y 1 3.7 ;tip N 

:7440-38-2 :Arsenic 1.1 :B: W :F 

7440- -,= - 7, a1.= 

7440-41-^ ;Ber y llium: 0.19B: .P.: 

;7440-a.--^ :Cadmium e.32:U: :P 

:7440-70-2 (Calcium 4.370 

:7440-4 7 -.'_: ;Chromium 4.9 

;7440 -ac.-4 IC:obalt 12.0 : :P 

:7640-50- 73 : Cor> p-r 21.2 :P 

,7439-kv-e• :Iron 20700 :P 

,74,9-"2-1 'Lead 1.9 :F ; 

7439- c': -4 i Mag ne s i um: :•790 :P 

`langanes e ; 262 ^P 

= 7 -. ;Merc'ut-v 0.0°:I.!1 ICv: 

764.0-02-0 : Nic. k.e1 7.9 : B: : p 

;7440-09-7 

;7782-49-2 

1 7440-2=-4 

:7440-23-5 

;7440---.-0 

:7440-62-2 

:Potassium: 

Selenium 1 

:Silver 

;Sodium 

:Thallium : 

!Vanadium 

387 :B: 

0.92:B: 

1.2 :B: 

235 ;B: 

0.30:U; 

4.4.5 : 

.. 

.P 

:F 

:P 

:P 

;F 

:P 

I 

I 

7440-E•c•-b : Zinc. 

;C y anide 

: 44.'-- 

0.52:U: N 

1P 

;CA: 

Color Sefor.-:: BROWN Clarity Before: Texture: MEDIUM 

Color After: BROWN Clarit y After: Artifacts: YES 

Comments: 

ROCKS 

FORM I - IN L- ILMO2.1

.... n.le aauaJ4YUUY3LYiY pbF4 ptV W ullnugtlPUUnu n: ^/•.•:v.BV•p. a •n.a:•b n: V •:JOtvAtlha.;.3J a U1lU LLJLLU LLUU UUU13U4U1WUC UUI3UYOa000CS aU nYUNpb.G;UUlI t3J.3UUJ:3o UUUUW ODUULIIUt 

Lab Name: SKINNER & SHERMAN LABS 

Lab Code: SKINER 

Matrix (soil/water) 

Level (low/med): 

% Solids: 

Color Before: BROWN Clarity Before: Tex tu re 

Color After: BROWN 

GomMents: 

POCK S 


1 


Clarity After: 

Contract: 68- 1)0-0108 

Case No.: N2-12-073SAS No.: 


B07095 

SDG No,- B07093 

SOIL Lab Sam p le ID: 12218-055 

LOW 

95.0 

Date Received: 12/-15/92 

Concentration Units (u g /L or mg/K g dr y weight): MG/KG 

, 1 

;CAS No. ; Anal y te :Concentration;C: O ;M _. 

, 

;7429-90-5 ;Aluminum ; 4620 

;7440-36-0 ;Antimon y 5.0 :B; 0 .1 ;P- 

17440-38-2 ;Arsenic 0.u'2!B: ;F - 

: 7440-39- 3 ; 

Bar lum 52.4 1 1 ;P 

1 7440-41-7 ;Ber y llium; 0.25;8; ;P_ - 

1 7440-43- q ;Cadmium i 0.32:U1 ;P 

;7440-70-2 :Calcium 5310 ; :P : 

;7440-47-3 ;Chromium 4.8 1 1 ;P 

;7440-48-4 :Cobalt 15.8 :P . 

,7440-50-8 :Copper i 18.4 ;P 

;7439-89 -e• ;Iron ; 25,300 :P 

:7439- 1; 2-1 )Lead ; 2.2 ; 1 ;F 1 = 

:7439- rq 5-4 ;Magnesium: 7•990 ; :P 

743`x -96 —Q_: Man ,-3anese ; 338 t P" i 

:74Z9-97-6 :Mercur y' 0.05 ; U: :CV: 

;7440-02-0 ;Nic k el ; 7.6 ;B; ;P 

;7440-09-7 ;Potassium: 455 ;B; ;P 

;7782-49-2 ;Selenium ; 2.3 ; : + :3° 

;7440-22-4 :Silver- 1.5 1 6 ; :P 

;7440-2.3-5 ;Sodium : 356 :B; ;F ; "- 

;7440-28-0 ;Thallium ; 0.29;U: :F 

;7440-62-2 :Vanadium ; 56.9 ; ; ;P 

;7440-E•6-6 ;Zinc 53.6 IP : 

:C yanide 0.52:U; N ;CA: - 

FORM I - IN 

Artifacts 

MEDIUM 

YES: 

ILMO2.1

..,u. n gWh:.q/mo[NtlNnntlt4mfvu,:mnnr yAP.:: >.:.:.: v. .r... ..rUp.:JV.•SOUHUU

I 

.............w vvnntmualuftf1111tiHtIl1U13Hai%nvlA:aiLLA . i)0UW>i1JiG.: JbtJ11SW:xt'utw:pi,aaebbLAiltiiYltlt^tliHfl}EittUUULNIWIlUU11111I51iStlU11iN3104tUN:•v:]bo .a): .:•gnv: •:•p:n:::.^Ce.:::CJI\>buuLtH1W 


1 



.> is 

r 

607098 

Lab Name: SKINNER & SHERMAN LABS. Contract: 68-DO-0108 ; 

Lab Code: SKINER Case No.: N2-12-073SAS No.: SOG No.: 607093 


Level (Low/med): LOW Date Received: 12/15/92 

Solids: 96.4 

Concentration Units (ug/L or mg/K g dry weight): MG/KG 

;CAS No. 

r ^ Analyte IConcentration!C; r 

0 M 

;7429-90-5 

{7440-36-0 

;7440-38-2 

'440-39-3 

17440-41-7 

;7440-43-9 

;7440-70-2 

;Aluminum 

;Antimon y 

;Arsenio 

; Bar iLIM 

;Ber y llium; 

;Cadmium i 

;Calcium ; 

3460 ; ; 

3.6 ;U: 

0.7915; 

49.6 ; ! 

0.2515; 

0.321U1 

5120 

N 

-;P 

;P 

;F 

SP 

.P 

;P 

;P 

;7440-47-3 

(7440-48-4 

7440-50-8 

;Chromium 

;Cobalt 

;Copp er 

1 3.6 

12.4 

15.4 

1 1P 

-;P 

•!P 

74.?,9-c•9 -F. Iron ! 22200 

743-^^-1 ;L_.ad 1.8 ; „F 

;Magi-IeS1URl; 3850 ;P 

Man-îane el 

__ -97-E: 

7 440-02-0 

; Mer •CUr . 

;Nickel 

0. 05 ; U I 

7.5 !8; 

: c V 

;P 

;7440-09-7 

;7"S2-49-2 

r'7440 -22-4 

7,!a0 - '23 - 5 

7440-28-0 

;Potassium! 

'Selenium ! 

;Silver ; 

, Sodium ; 

;Thallium 

407 ;BI 

0.9018! 

13 . p B; 

7_•16 181 

0.311U1 

+ 

IP 

;F 

.1P 

; p 

!F 

7440-62-2 ;Vanadium 48.7 ; ..1P 1 

; 7440-66-i5, ; Ziric 39.6 ; ; :P 

!C y anide 0.511U; N :CA; 

:olor before: SPOWN Clarity Before: . T ixtr_ire•: COARSE 

Color After: BROWN Clarity After: . Artifact:e.: YES 

Comments: 

ROCKS 

FORM I - IN 

ILMO2.1.

. . v.•....•,..o........ .,.•v...,v ...:................v......,..•..., ouwv.........,..—.. ,

..,....,.u,. ,,.......v.,.,a.wuuaueauaobeuufww)auuuauaabulwlmuu:nruuhmnwn,:,un.:.nnmmun:um:.omww2tum,:fw+tuuuuruuaauulltual4atbuûrtunuwnmmxaulemuu,va::J.u.uuno:mmwm. 


1 




B070BO 

Lab Code: SKINER Case No.: N2-12-073SAS No.: SDG No.; B07093 

Matrix (soil/water): SOIL Lab Sam p le ID: 12218-03 $ 


Solids: 94.8 

Concentration Units (ug/L or m g /K g dr y weight): MG/KG 

;CAS No. Anaiyte ^Concentration!C! 0 !M 

;7429-90-5 ;Aluminum 1 4490 1 1 1P 

17440-36-0 !Antimon y, 3.7 1 1J! N !P ! 

;7440-38-2 1Arsenic 1.4 !B! !F : 

17440-39-3 !Barium 45.0 1 1 1P i- 

;7440-41-7 ;Ber y llium! 0.1815; I ! _ 

!7440-43-9 ;Cadmium 0.321U1 !.P I - 

:7440-70-2 !Calcium 1 2000 1 1P ! 

1 7440-47- 3 !Chromium 9.2 1 1P I 

!7440-48-4 !Cobalt 5.6 IS: iP 

'7440-50-8 !Copp er 16.4 ! ;P - 

17439-89-6 !Iron 9770 1 1 1P I - 

'7439-92-1 !Lead 6 ,4 ! 1 

I F ! 

! 74 39-95-4 I Magn? s i umi t 2810 I i :P 

! 76 '?- yt,-_ 1 Man9ana =_ _ . L•9 2 t P 

:7439-97-6 ! I°lercur y 0. 0 5: U 1 ;-CV; 

17440-02-0 lNiokeI i 1.0.2 1 1P ! - 

17440-09-7 !Potassium! 535 !B! 1, P 

17782-49-2 (Selenium 1.2 1 1 S 1 F 1 - 

l74 40-22-4 !Silver t 0.78:U: !P I 

17440-23-5 !Sodium 333 Is: 1P ! 

17440-28-0 (Thallium 1 0.30101 JF I 

17440-62-2 !Vanadium 1 23.2 1 1 r1P I 

!7440-66-6 !Zinc 28.5 1 1 ,!P ! 

!C y anide 0.49:U1 N :CA: 

i 

Color Before: BROWN Clarity Before: 

Color- After: BROWN Clarity After: 

Comments. 

ROCKS 

FORM I - IN 

i 

Texture: MEDIUM 

Artifacts: YES 

a 

ILMO2.1

...... ....... .. ........n.r... .. ... ..... e....,..y wUUHUUU.Yb.A ionNUnUUaa poUe:w nu iv ............ ..nnnOM.h'v:a4aB R..... ,IIIN0HHHNHNN` 


1 




B070B1 

Lab Code: SKINER Case No.: N2-12-073SA 5 No.: SDG No.: 807093 

Matrix (soil/water): SOIL Lab. Samp le ID: 12218-04S 


Solids: 95.6 

Concentration Units (ug/L or m g /K g dr y wei g ht): MG/KG 

;CAS No. Analyte :Concentration :C; 0 'iM 1 

7429-90-5 ;Aluminum : 5370 .P 

,7440-36-0 !An t imon y: 3.8 .U: N :P 

;7440-38-2 :Arsenic 1 1.6 ;BI :F 

;7440-39-3 ;Barium 6'1:1 , ;P 

:7440-41-7 :Ber y llium: 0.23:6: :P _. 

17440-43-9 1Cadmium 0.33:U: :P 

;7440-70-2 !Calcium 2170 : :P 

7440-47- 3 :Chromi um : 11.2 , _:P 

'7440-48.-4 ;Cobalt 10.0 :BI :P 

,7440-50-8 ;Coo p er 16.° i 1P 

17439-89-_• I I r • on i 10700 : P .. 

. 7 ,17, 14 - 1 -v-, - L ;Lead : _.'? ;F 

''439 -9 5 -4. 1Maanesium: 3610 - 

, 7 4.T?_.:,F,- 5 :Man•.,anese: 702 ;P - 

?,U-a,,7_y., M•e. _ L11-Y , 0.05; U1 :CV: - 

. 7440-0 2 -0 1 Nick,? 1. 17 . 6 ;P , 

^440-09-7 :Potassium! 731 :5: :P 

:7782-4.9-2 :Selenium 0.91:B: S -;F I 

;7440-22-4 !Silver- : 0.82:U: ^P 1 -. 

7440-23-5 Sodium ! 216 ;B: :P 

17440-28-0 ;Thallium 1 0.311U! .F 

;7440-62-2 !Vanadium 23.9 

7 440-66-6 :Zinc 37.1 : :P - 

:Cyanide : 0.;O;U: N 'CA: 

Color Before: GROWN Clarity Before: rextur-:: 

Color After: BROWN Clarity After: - A t:Lf - is 

Comments: 

ROCKS 

FORM I - IN 

MEDIUI 

YES 

T^ 

ILMO2.1

.v..........a.:,unno..:...r...,:mnnv n...... ,nUYYUUN11xiNt1At6{wxbUieStkta4UUU pDixtl,ixw++tl8bxvaWnu.... .. :SStultq,aa auiWiulxUUiittlttl1x1HI1xtllxAwxxxtAwfwxwwxNxp:xwHiutxxtiWxtlwlwupounpu 


1 


Lab Name: SKINNER & SHERMAN LABS. Contract: 68-DO-0108 1 


BO7QB2 

Lab Code: SKINER Case No.: N2-12-O73SAS No.: SDG No.: 507093 

Matrix (soil/water): SOIL Lab Sam p le ID: 12218-O91S 


Solids: 95.7 

Concentration Units (ug/L or mg/K g dr y weight): MG/KG 

t t t 

;CAS No. ; Analyte 1Concentrat ion: C1 

;7429-90-5 Aluminum t 4090 

7440-36-0 ;Antimon y; 3.6 1L!1 N :P 

7440-38-2 :Arsenic : 0.68161 IF.: _- 

17440-39-'• !Barium '_..: :P 

:7440-41-7 ;Ber y llium; O.12:B: :P_: 

;7440-43-9 :Cadmium 0.3-:L!1 ;9- 

17440-70-2 ;Calcium 5390 ; ; 

17440-47-3 ;Chromium 1 1 ;P 

17440-4.8-4 ;Cobalt 4.3 ;B; :P ; 

17440-50-8 :Copp er i L__ :P - 

:7439-89-6 (Iron 7560 :P , 

'7439-92-1 ;Lead : _.1 1 :F t - 

:743 1'-G5-4. iMagl'lesiLlm; 247e' ;P - 

;7439-97-E. :Mercur y 0.05; U: :CV; 

:7440-02-0 1Nic! • .eI '_.. ;P , - 

17440-09-7 ;Potassium; 88e. :B; 

;7782-49-2 ;Selenium n.SO;B; + ;F 

;7440-22-4 :Silver O.77;U; 

:7440-23-5 ;Sodium 263 :B; :P. 

:7440-28-0 :Thallium 1 O.31:U1 :F 

:7440-62-2 ;Vanadium t 13.8 ; :P 

,7440-66-6 'Zinc ; 24.1 ; :P ; - 

1C ,/anide 2. 52; U: N :CA; 

Color Before; BROWN Clarity B?fore: Texture: MEDIUM 

Color After: BROWN Clarity After: Artifacts; YES 

Comments: 

ROCKu' 

FORM I - IN 

10 

ILMO2.1_


1 



,M , 

iP.; 

;r' 

;P 

;P 

i ,P 

P 

P 

.P 

I P. 

:F 

i CV; 

P. 

;P • 

;F 

;P 

;P 

;F 

P 

i CA; 


807083 

Lab Code: SKINEP. Case No.: N2-1.2-073SAS No. : SDG No.; 607093 



Solids: 85.4 

Concentration Units (ug/L or mg/K g dr y wei ght): MG/KG - 

;CAS No. Analyte ;Concentration;C; 0 

17429-90-5 ;Aluminum 1 1890 1 1 

;7440-36-0 ;.AntimonY 1 4.1 :U1 N 

'7440-38-2 :Arsenic 0.83;8: 

:7440-3 :)-'• oari%im 15.3 ;6: 

;7440-41-7 :°•ervllium: 0. 11; U; 

7440-43- •- . - admi umi ; 0.35:U; 

;7440-70-2 ;lCaICiL.IM 3670 

;7440-47-3 ;Chromium 1 4.5 

;7440-45-4 ;Cobalt 1 2.1 181 

:7440-50-._ : Copp er 5.3 1S: 

;7439-89-6 'Iron 3520 

!7439-92 .-1 -ead 2.0 

1 7&39-95-4 , , .a•an? =.i -.am ; 1320 

-,...,°a-a.'n . is n •..anes? 7.3. 8 

743'x-':a 7_h Mer-'•^!r'r 0. 061 1. 1 : 

' 7440-02-0 Nirl• , 1 5. 4 ; B i 

1 74.40-09-7 ;Potassium: 390 ;B; 

;7732- 4 4-2 `*elenium ; 1.1 i 1 

:7440-22-4 Silver ; 0. 86; U: 

7440-23-5 _odium 104 :B; 

1 7440-28-0 . hallium 0. 33; U: 

1 7440-62-2 :Vanadium 6.6 181 

17440-66-E• .Zinc ; 13.6 i 

•anide 0. 59; U1 N 

Color Before: BROWN Clarity Before: 

Color After- BROWN Clarity After: 

^';omments; 

ROCK 

f 

FORM I - IN 

Textur- . COARSE 


-ILMO2.1


1 


Lab Name: SKINNER & SHERMAN LABS. Contract: 68-DO-0108 : 


B070B8 

Lab Code: SKINER Case No.: N2-12-0735AS No.: SDG No.: 807093 



% Solids: 94.3 

Concentration Units (ug/L or mg/K g dry weight): MG/KG 

f 

ICAS No. Analyte !ConcentrationiC! 0 .M. 

;7429-90-5 !Aluminum 5890 !P 

;7440-36-0 ;Antimon y 3.q 1U! N .P. 

;7440-38-2 !Arsenic 2.0 !F: ! 

; 7r.40- 9-3 1 Barium 51. 6 ;P ! 

;7440-41-7 !Ber y llium! 0.21;B! :P 

;7440-43-9 ;Cadmium 1 0.34; 1j : !P 

;7440-70-2 ;Calcium 2 540 .P °- 

17440-47-3 ;Chromium 10.9 ! IP 

17440-48-4 !Cobalt 6.0 !B: 

;7440-50-8 :Copper : 7 .0 !P 

:7439-89-6 ;Iron 11900 :P 

7 .139- 142-1 11_ead 

Magnesium: 3_•-,o ; P 

. ?;..3d.-gar,-•i ; Man9ane s °: 1I+3 

7439-97-6 !MerC%Ur y 0.05; U1 ; C-V; 

. 7440-^D'^-0 N ic4;e1 11.7 ' rr 

;7440-09-7 ;Potassium) 1140 1 .P 

;7782-49-2 :Selenium I 1.5 ! ; + !F 

!7440-22-4 :Silver I 0.82;U! :P 

;7440-23-5 Sodium 8 3 .0 !B! !P 

;7440-28-0 !Thallium 1 0.33:6! !F - 

'7440-62-2 !Vanadium { 22.4 ! 1 IP ! - 

7440-66-6 !Zinc 32.9 : ! :P 

.C y anide 0. 53:U! N ICA! 

color Before: BROWN Clarity 6e-tore: Texture: FINE 

Color After: BROWN Clarity After: Artifacts: 

Comments: 

FORM 1 - LN LLMO2.1 

-

..... ......... i.... ^......:•.v....HHNwvvwu NVwww.. ............ ..^. ..... ....^ .. .•u 44vN4]'YN]ll11111NNY11YH 4Y1W NNNNINHN H11uNH UN4.l.n]w H.t]F.Yf11t,1NHNN 44NNf:,. N, 


1 

INORGANIC ANALYSIS DATA SHEET - 


i 


B070B9 

Lab Code: SKINER Case No.: N2-12-073SAS No.: SDG No.: B07093 

Matrix (soil/water): SOIL Lab Sample ID: 12218-12S 


Solids: 95.6 

Concentration Units (u g/L or mg/Kg dry weight): MG/KG 

;CAS No. ; Anal y te ;Concentration;C; O :M,; 

;7429-90 -5 :Aluminum 1 3'970 

;7440-36-0 :Antimony ; 3.6 IU; N ;P 

1 7440-38-2 ;Arsenic 0.74;6; ;F 

; 7440-39- 3 ; Bar ium 4.7. 1 1 1 ; P, 

;Ber y llium; 0.2216; t : - 

1 74 4 0-43-9 ;Cadmium 0.32;U: ;P 

;7440-70-2 ;Calcium 5970 1 ;P_: 

1 7440-47-3 :Chromium ; 4.3 ; ; ;P ; -- 

;7440-48- 4 :Cobalt 13.3 ;P 

;7440-50-8 ;Co pp er ; L^,.1 ; :P 

17439-89-6 ;Iron 23soo ; :P -- 

;7439-92-'6 :Lead 2.0 ; ; ;F 

7439- ag -4 ;Mal-1e B1 Um; 5100 

Manyane»'- 

744.y-97-^^• ;Mercur y 0.05;Ui ;Cv: - 

1 7440-02-0 ;Nickel 6.6 ISi ;P _- 

;7440-09-7 ;Potassium; 560 :B; :P - 

:7782-49-2 :Selenium ; 0.6.3:U1 + ;F 

;7440-22-4 ;Silver 0.92:6: IP 

;7440-23-5 ;Sodium ''01 :B; :P 

;7440-28-0 ;Thallium ; 0.30; U; ;F 

;7440-62-2 ;Vanadium 51.6 ; ; IP : 

;7440-66-6 ;Zinc 41.1 ; 1 ;P , - 

:C y anide t 0.4.91U1 N ;ACA; 

, ': ,:,lor Before: GREY Clarity 3eforP: Texture.- COARSE 

Color After: GREY Clarit y After-': Artifacts: YES 

1'omment-i 

STONE`_. 

FORM 1 - IN 

fV . 

ILMO2.1

...^YJNn1YJafYYev 1YYYY1w1.......Y..:^Y.^JY:.:v.n y. ...........v.LLYWY/,...LL.:YYLLWYYIWtYJV4Y.YYYi1WYLL114JY.Y.lYY4Y44UY 4Y 11U41111UlWYOVY4{tY4W11144 - 'Wl uu.iuw ..... ... .. ^.....- 


1 


Lab Name: SKINNER & SHERMAN LABS. Contract: 68-DO-0108 I 

1 


807000 

Lab Code: SKINER Case No.: N2-12-073 5AS No.: SDG No.: 807093 

Matrix (soil/water): SOIL Lab Sam p le ID: 12218-135 



Concentration Units (u g /L or m g /Kg dr y weight): MG/KG 

; 

ICAO. No. 

Color Befor = : GREY 

Color After: GREY 

Comments: 

STONES 

7429-')0-5 

;7440-36-0 

;7440-38-2 

!7440-39-3 

17440-41-7 

;7440-43-? 

;7440-70-2 

;7440-47-3 

;7440-43-4 

17440-50-8 

7439-?9 -6 

743'a-^_-L 

7439--c--4 

-+ -- 

743 - -6 

;7440-02-0 

;7440-09-7 

17782 - 4'4-2 

17440-22-4. 

7440-23-5 

;7440-28-0 

17440-62-2 

17440-6t-6 

1 1 

1 Anal y te IConcentration!C: a IM 

;Aluminum 2950 ; IP - 

:Antimon y; 7.6 ;U; N ;P 

;Arsenic ; 0.951s! ;F 

;Barium /+4,7 ;P 

;Ber y llium: 0.21;B; ;P 

;Cadmium 0.32; U; ;P 

;Calcium 5430 ! ; IP 

;Chromium ; '2.2 ;P 

;Cobalt 11.8 ; ;P 1 _ 

;Copper 13.5 IP 

:Iron ; 20800 i ;P 1 

;Lead ; 1.9 IF 

:Magnesium: 3.710 ;P 1 

_ 

:Manganese; 247 i i ;P . 

;Mercur y 0.05;U; ICVI- 

;Nickel 7.2 16l ;P 

;Potassium! 386 ;B; IP 

;Selenium ; 0.60; U; IF ! __ 

;Silver ; 1.4 16; IP ! 

Sodium ; 224 ;B; ;P ;- 

;Thallium ; 0.291U; ,F 

,Vanadium ! 45.4 1 ; ;P 

:- inc ; 36.E i IP ; 

'.'_ yanide 0. 49; U; N LcA1 - 

Clarit y Before: -texture: MEDIUM 

Clarit y After: • A rtifacts; YES 

FORM I -- IN 

1 

1 

ILMO2.1

eA 

Thermo Analytical Inc.C` " o. 

TMAINorcal _ -- _ - ^^^ ; i - 

_-2030 Wri ht Avenue ------- IVED 

'`y 

a o. 80 0 _ _ 

_ _ 

DMO A . 

Richmond, h CA 94804-004 

0 

-----...^ 

(510)235-2633 FaxNo. / 

March 24, 1993 

Ref. TMA /Norcal N2 -12-078-7138 

Ms. Briana Colley 

Westinghouse Hanford Company 

2355 Stevens Drive 

MSIN H4-23 

345 Hills Street / 3000 Area 

Richland, WA 99352 

Dear Ms. Colley: 

SENT BY FEDERAL EXPRESS 

Enclosed in the Summary Data Section, are the gross alpha, gross beta, 14C, 9DSr, 

isotopic uranium, isotopic plutonium, 241 Am, and gamma scan results for the soil 

samples from 100-NR-1 Location we received 14 December 1992. The QA/QC results 

are also given in the Summary Data Section. The Summary Data Section is numbered 

pages 1 to 50 and the appendices are numbered pages 51 to 389. 

Please call if you have any questions concerning this data. 

Sincerely, 

Dinkar P. Kharkar, Ph.D, 

Manager, Nuclear Programs 

DPK/ss 

Enclosures: Section 1 and 2 

Appendices 

1993 

`

SDG 7138 Client Westinghouse Hanford 

Contact Dinkar P. Kharkar Contract MBH-SVV-069262 

1.0 GENERAL 


Soil sample results from 100-NR-1 Location (TMA/Norcal Group 7138) are 

reported herein. TMA/Norcal Group 7138 is comprised of the seven samples 

listed on the Chain-of-Custody documents and is identified as Samples 1 

through 7. 

1.1 CHAINS-OF-CUSTODY 

This report includes data from samples delivered under Chain-of- 

Custody documents Field Logbook No. EFL-1062 and EFL-1063. 

1.2 SAMPLE VOLUME 

1000 mL bottles of samples were received for the analyses. 

1.3 MISSING SAMPLES 

All samples were accounted for in an undamaged condition. 

1.4 HOLDING TIMES 

2.0 QUALITY CONTROL 

Samples were collected between 12/09/82 and 12/17/92 and sample 

processing was initiated within 180 days of collection. 

The internal quality control consisted of one sample each of a laboratory 

control, a blank, and a replicate. All original analyses were performed 

with QC samples 7138-8 through 12. 

The QC samples were prepared and labelled by the quality control officer. 

Copies of The QC notebook pages are included in the data package. 

2.1 LABORATORY CONTROL SAMPLES 

Case Narrative Section 

Page 1 of 3 

The LCS recoveries for all nuclides were good except for gross alpha 

and 239,240pu which were 72% and 528 respectively and did not pass 

the 3 c total limits. However, the gross alpha recovery plus 1 c 

error on the recovery was within 3 c total protocol limits. We are 

investigating the low LCS recovery of 239.240Pu. The chemical yield 

and the plutonium spectrum were good and we did not find any obvious 

reason for low recovery. The MDA of 238 PU was higher than RDL due 

to high background. The higher MDA of 241 Am was due to low chemical 

yield. 

rma


Contact Dinkar P. Kharkar Contract MBU-SVV-069262 

2.2 BLANKS 

CAS$ NARRATIVE 

MDA's for all the analyses meet the RDL requirements except for 

238 Pu and 239,240pu which were higher due to lower chemical yields. 

The 90Sr error was underlined because the counting error was bigger 

than both the MDA and the result implying that the MDA may not be a 

good estimate of the "real" minimum detectable activity. 

2.3 REPLICATES 

3.0 ANALYTICAL NOTES 

The results were satisfactory for all replicate analyses. The 

higher MDA of 241 Am of sample number 7138-10 (replicate of 7138-1) 

was due to higher background. The higher MDA's of the gamma 

nuclides were due to smaller aliquots available for analysis. The 

higher MDA of 59 Fe was due to the short half-life of 59 Fe. The 90Sr 

error was underlined because the counting error was bigger than both 

the MDA and the result, implying that the MDA may not be a good 

estimate of the "real" minimum detectable activity. 

3.1 Gross Alpha Analyses: The average MDA for gross alpha was 6 t 2 

pCi/g. Positive gross alpha concentrations above RDL was not found 

in any of the samples except in sample number 7138-3. 

3.2 Gross Beta Analyses: The average MDA for gross beta was 5 t 1 

pCi/g. Positive gross beta concentrations above RDL was found in 

all the samples except in sample numbers 7138-3, 6, and 7. 

3.3 Carbon-14 Analyses: The average MDA was 20 t 6 pCi/g. All sample 

results were less than RDL. No positive 14C was found in any of the 

samples. 

3.4 Strontium-90 Analyses: The average yield for ten analyses was (71 

t 266). The lowest yield was 41% and the highest was 838. The 

average MDA was 0.9 t 0.2 pCi/g. Positive 90Sr concentration was 

not found in any of the samples except in sample number 7138-2. The 

results of the remaining samples were below RDL. 

3.5 Uranium-233, 234. 234. and 238 Analyses: The average yield for ten 

analyses was (67 t 27%). The lowest yield was 49% and the highest 

was 888. The average MDA was 0.1 t 0.1 pCi/g. Concentrations of 

234U and 238 U above the RDL were found in all of the samples except 

in sample numbers 7138-2 and 3. 


Page 2 of 3 

TM

SDG 713$ Client Westinghouse Hanford 

Contact Dinkar P. Kharkar Contract MSH-SVV-069262 


3.6 Plutonium-238, 239/240 Analyses: The average yield for twelve 

analyses was (60 1 358). The lowest yield was 23% and the highest 

was 78%. The average RDA was 0.07 t 0.09 pCi/g. Positive plutonium 

concentration above RDL was not found in any of the samples. All 

sample results were below RDL. The MDA of 7138-2 was higher than 

RDL due to higher background. Sample numbers 7138 -3 was counted for 

535 minutes, lower than the nominal count time of 700 minutes. 

3.7 Americium-241 Analyses: The average yield for ten analyses was (65 

t 37%) . The lowest yield was 38% and the highest was 86%. The 

average MDA was 0.04 t 0 . 03 pCi / g. Positive americium concentration 

above the RDL was not found in any of the samples. All sample 

results were below the RDL. 

3.8 Ga^ylA Scan Analyses: Gamma scan analysis found positive 60Co and 

Cs concentration in sample number 7138-4 

concentration in sample numbers 7138-1 and 5. 

and positive 6000 


Page 3 of 3 

THE

TMA NORCAL 

REPORTING GROUP 7138 

N212078=10 807088 

REPLICATE 

SDG 7138 

Contact Dinkar Kharkar 

REPLICATE 

Lab sample id N212078-10 

Dept sampLe id 7138-010 

ORIGINAL 


Dept sample id 7138-001 

Received 12/14/92 

% moisture 5.9 

Client Westinghouse Hanford 

Contract MSH-SVV-069262 

CLient Sample id BO70B8 

Matrix SOIL 

Collected 12/09/92 

Chain of custody id EFL-1063 

REPLICATE 2a ERR MDA RDL OUALI- ORIGINAL 2a ERR NOR OUALI- RPD 3a PR( 

PARAMETER PCi/G (COUNT) PCi/G pCi/G HERS TEST PCi/G (COUNT) PCi/G FIERS % TOT LIN 

Gross Alpha 3:9 3.9 5 10 U 80A 3.1^- 3.9 5-- U^ 

Gross Bete 24 4.5 5 10 BOB 21 4.8 6.„ 13. 54 

Uranium 233/234 ::'0.54- 0.21 0:1 0.3 U -0.37 0.14 0.1'.... .'3Z.: 84 - 

Uranium 2350 0.047 0.2 0.3 U ..: U 0.013 0.027 0:1 U - 

Uranium 238 .0.56 0.21 0.1 0.3 U 0.35 - 0.14 0;08.. .':'46':. 84 

PLutonium 238 -'0.002 0.021 0.04 0.05 U PU -0.006, 0.022 0:04': U 

Plutonium 239/240 ,0:002- 0.009 0.02 0.05 U :: PU -0.006 0.011 0:03. U 

Americium 241 '0.003 0.031 0.06 0.05 U > AM 0.006 0.015 0.03" U -. 

Strontium 90 1,4 : 0.37 0.9 2 1 Y 0.76 0.84 0.3 U 59'': 130 - 

Carbon 14 

GAMMA SCAN ANALYTES 

--6.3" 

., 

9.7 20 ' 50 U, :. C 

- 

4.7 ' 9.1 2os, U 

- 

Potassiuo 40 16•:.. 2.3 GAN v 1.2 6 40 

Iron 59 U - 0.7 0.05 U GAM U ;; D3, ' , U 

Chromium 51 U. .. 3 U GAM U ,' ...1 '.. U _ 

Cobalt 60 0:28 0.23 0.05 GAM - 0.098' 0.056 96 191 

Zinc 65 U 0.4 U GAM U - 0.2 " U - 

Ruthenium 106 U 1 U GAN U 0-5.. U - 

Cesium 134 .0 0.1 U GAM U .., 0.06 U- 

Cesium 137 ..; U 0.1 0.05 U .::. GAM U::: 006 U: -: 

Europiun 152 U`:',' 0.2 0.1 U ::, GAM U`:4: O.T " U - 

Europium 154 U.. 0.1 0.1 U ;:.. GAN U :: 0.08 U 

Radium 226 0:50', 0.19 GAN 0.54 0.11 8' 71 

Thorium 228 0:8G.': 0.12 GAM 1.2^: 0.10 - 40% 41 

Thorium 232 f:2..-- 0.56 GAN 0.90; 0.24. 29;-, 93 

Lab id TMAN 

Protocol WHC-HEMS 

REPLICATES Version Ver 1.0 

Page 1 Form DVD-REP 

SUMMARY DATA SECTION Version 2.23 

Page 13 Report date 03/24/93

TMA NORCAL 

REPORTING GROUP 7138 ^ . 

. N212078-01 B07QBB " 

DATA SHEET 


Contact Dinkar Kharkar Contract MBH-SVV-069262 

Lab sample id N212078-01 Client sample id B070B8 

Dept sample id 7138-001 Matrix SOIL 

Received 12/14/92 Collected 12/09/92 

% moisture 5.9 Chain of custody id EFL-1063 

PARAMETER CAS NO 

RESULT 

pCi/G 

2a ERR 

(COUNT) 

MDA 

pCi/G 

RDL 

pCi/G 

QUALI- 

PIERS TEST 

Gross Alpha Alpha 3.1 3.9 5',' 10 U 80A 

Gross Beta Beta 21 4.8 6- 10 80B 

Uranium 233/234 0.37"' 0.14 '011-': 0.3 U 

Uranium 235 15117-96-1 .0:013: 0.027 6.11 0.3 U;:...' U 

Uranium 238 7440-61-1- ,'0::35.. 0.14 -b08 0.3 U 

Plutonium 238 13981-16-3 =0.006 0.022 0.'04 0.05 U:',: PU 

Plutonium 239/240 -6.006 0.011 0':03.'. 0.05 Us,. PU 

Americium 241 14596-10-2 0.006 0.015 0703 0.05 U'41 AM 

Strontium 90 10098-97-2 0_76 0.84 O.8- 2 U.'" Y 

Carbon 14 14762-75-5 4:7. 9.1 20., 50 U"'. C 


Potassium 40 13966-00 -2 17 1.2 - -'" GAM 

Iron 59 14596-12-4 U b%:3 0.05 U':- - GAM 

Chromium 51 14392-02-0 U., 1;,. U..., GAM 

Cobalt 60 10198-40-0 0.098 0.056 -- 0.05 GAM 

Zinc 65 13982-39-3 U'', 0:`2 U..: GAM 

Ruthenium 106 13967-48-1 U .0..5 U GAM 

Cesium 134 13967-70- 9 U.: .0.06 U^ GAM 

Cesium 137 10045-97-3 U; 0.06'- 0.05 U:: GAM 

Europium 152 14683-23 -9 U"... . -,0.1' 0.1 Uc GAM 

Europium 154 15585 - 10-1 U'. ,'0.08, 0.1 Ui: GAM 

Radium 226 13982-63 -3 0 s54- 0.11 GAM 

Thorium 228 14274-82-9 1:2 0.10 - GAM 

Thorium 232 7440-29-1 090' 0.24 GAN 

Lab id MAN 

Protocol WHC-HEIS 

DATA SHEETS Version Ver 1.0 

Page 1 Form DVD-DS 



THA NORCAL 


N212078-02: B07QB9 - 

D A T A S H E E T 

BUG 7138 ,s Client Westinghouse Hanford 

Contact Dinkar Kharkar Contract MBH-SVV-069262 

Lab sample id N212078-02 Client sample id B070B9 


Received 12/14 192 Collected 12/09/92 



RESULT 

pCi/G 

2a ERR 

(COUNT) 

MDA 

pCi/G 

ROL 

pCi /G 

QUALI- 

PIERS TEST 

Gross Alpha Alpha 489 5.9 7" 10 U^.'- _: BOA 

Gross Beta Beta 38.. 5.2 5 1 . 10 80B 

Uranium 233/234 0:076 0.065 "01', 0.3 U`s.^. _' U 

Uranium 235 15117-96-1 0: 1013.. 0.026 0.1 0.3 U."i U 

Uranium 238 7440-61-1 - 6.22 0.089 'O::bB' 0.3 X,'.`>;', U 

Plutonium 238 13981-16-3 -0.016 0.027 DA `. 0.05 U,:z, PU 

Plutonium 239/240 -0'>i 0.022 '0:04- 0.05 U.'., PU 

Americium 241 14596-10-2 -0:003 0.030 0:'06' 0.05 Wr _ AM 

Strontium 90 10098-97-2 80 0.64 0.8 2 _-- 

Y 

Carbon 14 14762-75-5 7.1 9.1 20... 50 ,>.:....._..,, III; C 


Potassium 40 13966-00-2 69 1.6 - GAM 

Iron 59 14596 - 12-4 U-..t O:'6 0.05 U34; _ GAM 

Chromium 51 14392-02-0 U?:: 3.•' U11, GAM 

Cobalt 60 10198-40-0 U' 0.1 0.05 UÌ GAM 

Zinc 65 13982-39-3 U°' 0':3.' U"' GAM 

Ruthenium 106 13967-48-1 U.' 1.'. U GAM 

Cesium 134 13967-70-9 U:• 0.1. U'.:. GAM 

Cesium 137 10045-97-3 U_.. .0 1 ... 0.05 U,,._. GAM 

Europium 152 14683-23-9 U'> .O.^2. .. 0.1 U": GAM 

Europium 154 15585-10-1 ' U"-. -0.1 0.1 U':A, ^. GAM 

Radium 226 13982-63-3 :-037 0.18 - GAM 

Thorium 228 14274-82-9 ' 0.47 0.19 GAM 

Thorium 232 7440-29-1 '.'...0'49 0.41 ",. , GAM 

Lab id TMAN 






THA NORCAL 


N212078-03' B07QCO 

DATA SHEET 

BOG 7138 







RESULT 

pCi /G 


Contract MBH-SVV-069262 

Client sample id B07000 

Matrix SOIL 



2a ERR 

(COUNT) 

MDA 

pCi/G 

RDL 

pCi /G 

QUALI- 

FIERS TEST 

Gross Alpha Alpha 11. 6.1 6 10. _. 80A 

Gross Beta Beta 9.1. 4.0 6-; 10 .'T SOB 

Uranium 233/234 0.29 0.13 ,'0.1 -. 0.3 J`" _' U 

Uranium 235 15117-96-1 '::0:019 0.037 -071 0..3 U:>:.-_. U 

Uranium 238 7440-61-1 0.29." 0.13 - 0A 0.3 J.:;:: U 

Plutonium 238 13981-16-3 --0'043'. 0.068 0Y2r 0.05 U,` PU 

Plutonium 239/240 '0:017 0.017 0.07:..;. 0.05 U^:a"- PU 

Americium 241 14596-10-2 .-0:006 0.017 0:04'. 0.05 U : AM 

Strontium 90 10098-97-2 .0736.. 1.9 0.9 2 U8 Y 

Carbon 14 14762-75-5 ,177' 6.3 10' 50 U.;: C 


Potassium 40 13966-00-2 9 14 0.87 - - GAN 

Iron 59 14596-12-4 U 072' 0.05 U'::!: GAM 

Chromium 51 14392-02-0 U 1.. ,. U:;" ., GAM 

Cobalt 60 10198-40-0 U'. 0.04 0.05 ulo GAM 

Zinc 65 13982-39-3 U., . 0.1 U':>: GAM 

Ruthenium 106 13967-48-1 U.: 0.3. U' GAM 

Cesium 134 13967-70-9 U:.: '0.05' U;:., GAM 

Cesium 137 10045-97-3 DY, 0704' 0.05 U:.I GAN 

Europium 152 14683-23-9 .U':.: ..`0:07- 0.1 V, GAM 

Europium 154 15585 -10-1 . U.`,: ..0:05 0.1 U1, 

Radium 226 13982-63-3 0739" 0.069" _' GAM 

Thorium 228 14274-82-9 -. 0.'S4 0.051 ', . _ GAM 

Thorium 232 7440-29-1 0.17 - ........_.,. GAM 

Lab id TMAN 






N21268-64. 

SDG 7138 







TKA NORCAL 


DATA SHEET 

RESULT 

pCi/G 


Contract MBH-SVV-069262 

Client sample id B070D7 

Matrix SOIL 

Collected .12/16/92 


2a ERR 

(COUNT) 

HDA 

pCi/G 

RDL 

PCl/G 

QTJALI- 

FIBRE TEST 

Gross Alpha Alpha .. 3.4 4.5 6 10 80A 

Gross Beta Beta 30 4.7 5 10 80B 

Uranium 233/234 0.39, 0.19 O.:l 0.3 U 

Uranium 235 15117-96-1 0.044 0.2 0.3 U : :,, U 

Uranium 238 7440-61-1 .0::34 0 0.15 0.1 0.3 U 

Plutonium 238 13981-16-3 

0.021 0-04 005 U: s PU 

Plutonium 239/240 01.15 0.042 0.^04 0:05 PU 

Americium 241 14596-10-2 0X25 0.019 0.'*02 0.05 AM 

Strontium 90 10098-97-2 0 -59 0.24 0.8 2 U ;:: Y 

Carbon 14 14762-75-5 -4.7 8.3 20 50 U I-J C 


Potassium 40 13966-00-2 13 2.3 GAM 

Iron 59 14596-12-4 U, 3:-' 0.05 U^- GAM 

Chromium 51 14392-02-0 U. 9: Ul- GAM 

Cobalt 60 10198-40-0 81 1.3 0.05 GAM 

Zinc 65 13982-39-3 U. 2 U.. GAM 

Ruthenium 106 13967-48-1 U 4 U. GAM 

Cesium134 13967-70-9 U ' . 0.6 CAN 

Cesium 137 10045-97-3 0.61 0.37 0.05 GAM 

Europium 152 14683-23-9 U.:. 0.6 0.1 U-'.*:: GAM 

Europium 154 15585-10-1 U 0.4 0.1 U,: r GAM 

Radium 226 13982-63-3 0.57 GAM 

Thorium 228 14274-82-9 U:, 0 : 6 U . GAM 

Thorium 232 7440-29-1 3.` U 

Lab id TMAN 






TMA NORCAL 


X212078-'05' 807QD8 

DATA SHEET 

SDG 7138 s Client Westinghouse Hanford 

Contact Dinkar Rharkar Contract MSH-SVV-069262 

Lab sample id N212078-05 Client sample id B070D8 


Received 12121/92 Collected 12 1 16/92 



RESULT 

pCi/G 

2a ERR 

(COUNT) 

MDA 

pCi/G 

RDL 

pCi/G 

QUALI- 

PIERS TEST 

Gross Alpha Alpha 8.5 4.3 5.: 10 Jz:: 80A 

Gross Beta Beta 14.. 2.8 4:< 10 - ... 80B 

Uranium 233 /234 0 .46 0.18 ' 0'2 0.3 U 

Uranium 235 15117-96-1 0.034 0.068 ^0J1. 0.3 U':,: 'y... 

Uranium 238 7440-61-1 0.59 0.21 .-0.1-: 0.3 - U 

Plutonium 238 13981 - 16-3 0.008 0.022 0.05 0.05 PU 

Plutonium 239/240 0:025 0.028 --005 0.05 PU 

Americium 241 14596-10-2 -0 : 008 0.022 '0.04 0.05 U,t: AM 

Strontium 90 10098-97-2 0 : 002 0.42 ''0^7'- 2 U:° Y 

Carbon 14 14762-75-5 -5:5 8.7 :20" 50 U C 


Potassium 40 13966-00-2 16' 1.0 GAM 

Iron 59 14596-12-4 U ^`" O'.^5 0.05 U-%;.- GAM 

Chromium 51 14392-02-0 U. 2..; w GAM 

Cobalt 60 10198-40-0 4:3 0.17 0.05 GAM 

Zinc 65 13982-39-3 U 0.3 tv GAM 

Ruthenium 106 13967-48-1 U 0.7 Ul- GAM 

Cesium 134 13967-70-9 U 0'l T:;^, GAM 

Cesium 137 10045-97-3 U 0:09 0.05 U,7:, GAM 

Europium 152 14683-23-9 U. 0.1 0.1 U.i>- GAM 

Europium 154 15585-10-1 U. 0.08 0.1 U-': GAM 

Radium 226 13982-63-3 0:55 0.11 .. .. .. GAM 

Thorium 228 14274-82-9 1:0 0.12' GAN 

Thorium 232 7440-29-1 1.1 0.47 -- GAM 

Lab id TMAN 





Page 18 Report date 03/24/93 

U

SDG 7138 




Received 12/21 1 92 



TNA NORCAL 


DATA SHEET 

RESULT 

pCi/G 

B07QD9 


Contract MEH-SVV-069262 

Client sample id B070D9 

Matrix SOIL 



2a ERR 

(COUNT) 

!D)A 

pCi/G 

RDL 

pCi /G 

QUALI- 

FIERS TEST 

Gross Alpha Alpha 6.3 5 . 5 6-": 10 J,-- 80A 

Gross Beta Beta 8.9 3.7 5 c 10. J. 80B 

Uranium 233/234 - 0:42 0.19 0.1.. 0.3 U 

Uranium 235 15117-96-1 0.:: 0.044 0:'2', 0.3 U"''. U 

Uranium 238 7440 - 61-1 '0.40- 0.19 -061 0.3 ^- U 

Plutonium 238 13981-16-3 .:.0: :006 0.024 0:04 0.05 Ut'-:. PU 

Plutonium 239/240 0:: 006,.. 0.024 ' 0..04 0.05 U,, PU 

Americium 241 14596 -10-2 -0':004 0.020 0104 0.05 U., 

Strontium 90 10098-97 - 2 0'.:: 0.51 Oa 2 U:' Y 

Carbon 14 14762-75-5 -3.0. 8.3 -20,' 50 Ul C 

GAMMA SCAN ANALYTES - -- 

Potassium 40 13966-00-2 7:"7 0.85 GAM 

Iron 59 14596 - 12-4 U. 0.2' 0.05 U':' GAM 

Chromium 51 14392 -02-0 U 0.' S U':: GAM 

Cobalt 60 10198-40-0 U.. 0:05. 0.05 U'.'_ GAM 

Zinc 65 13982 -39-3 U.: 0:1 U'?' GAM 

Ruthenium 106 13967 -48-1 U 0': '3. U'. GAM 

Cesium 134 13967-70-9 U"'. -0.04 U. GAM 

Cesium 137 10045-97-3 U:. ..0.,04 0.05 U::. GAM 

Europium 152 14683-23-9 U:' 6 C'08" 0.1 U'1; GAM 

Europium 154 15585 - 10-1 .:-U 0':'05:-, 0.1 U:,, GAM 

Radium 226 13982-63-3 . 0.36 0.078 - -- GAM 

Thorium 228 14274-82-9 .. ' 0:60.. 0.069 - - -'._.. GAM 

Thorium 232 7440 -29-1 0 .41 0.15 - - - GAM 

Lab id TMAN 






TMA NORCAL 


N212078-07.' 807QPO 

DATA SHEET 


Contact Dinkar Kharkar Contract MBH-SVV-069262 -- 

Lab sample id N212078-07 Client sample id B070FO 


Received 12/21/92 Collected 12/17192 

moisture 1.9 Chain of custody id EFL-1062 


RESULT 

pCi/G 

2a ERR 

(COUNT) 

MDA 

pCi/G 

RDL 

pCi/G 

QUALI- 

PIERS TEST 

Gross Alpha Alpha 3.4 6.1 9 10 U:._' 80A 

Gross Beta Beta 8.9 - 4.2 6 10 Q."' -"^ 80B 

Uranium 233/234 0.48. 0.16 '0.1 0.3 "`'. - U 

Uranium 235 15117-96-1 '0.078 0.053 0.,1 0.3 U':;z,. U 

Uranium 238 7440-61-1 ..0'.33`. 0.13 0.'08 0.3 U 

Plutonium 238 13981-16-3 -0.003 0.024 0.05 0.05 U::',: PU 

Plutonium 239/240 0:012. 0.018 0.03 0.05 U, PU 

Americium 241 14596-10-2 --0:012' 0.023 0.05 0.05 U "' 

Strontium 90 10098-97-2 -0.'19 - 0.28 1.. 2 U'.-- - Y 

Carbon 14 14762-75-5 =552'" 8.7 20' 50 U.f.'" C 


Potassium 40 13966-00-2 --8'3, 0.73 - GAN 

Iron 59 14596-12-4 0..:. 0.2 0.05U:.'. ^^ GAN 

Chromium 51 14392-02-0 U'. 0.9 U..,,. .: GAM 

Cobalt 60 10198-40-0 U 0.04 0.05 U:B - GAM 

Zinc 65 13982-39-3 u:. 0.1 U;'.._ GAN 

Ruthenium 106 13967-48-1 U 0.3 - U GAM 

Cesium 134 13967-70-9 U 0.04 U, GAM 

Cesium 137 10045-97-3 U.: 0.03 0.05 U.,-.^- GAN 

Europium 152 14683-23-9 U;. 1 0:07 0.1 U?"._ GAM 

Europium 154 15585-10-1 U:: 0:05 0.1 U;at. GAM 

Radium 226 13982-63-3 - .0.31 0.068 GAM 

Thorium 228 14274-82-9 0.51_... 0.046 GAM 

Thorium 232 7440-29-1'0.47 -- 0.16, GAM 

Lab id TMAN 






Westinghouse 



Custody Form initiator )Q R= - &ES 

company contact WV SEWER Telephone 376-2413 

Project Designation/Sampling Locations 100-NR-1 

collection Date 1691 /G —9A 

Ice Chest No. .S*O L /47 Field Logbook No. EFL- /O-6J 

Bill ofJLading/AirbiU No. 4lgLl7 7 SC offsite Property No. /.Ug3—/J-D/7L 


Shipped to TMA/NORCAL 


241 

Sample Identification 

1,25âG:GLP;ICP/AA Metals,Hg,Cn 


1,950ml aG: CLP; Semi -VOA, PCB/PEST, Anions (F,SO4,NO2,NO3)PH 

1,1000ml G/P:Gross alpha/beta, Gamma Spec, Sr-90,C-14,U-235/238,Pu-239/240,Am- 

2) fL—'E" ^W8 1,250m1 aG:CLP;ICP/AA Metals,Hg,Cn 



1,1000ml G:Gross alpha/beta, Gamma Spec, Sr-90,C-14,U-235/238,Pu-239/240,Am-241 

1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 

G:CLP;VOA 

1,950ml 26 aG: R,S^mi-VOA,PCB/PEST,Anions (F,SO4,NO3) 

1,1000ml G:Gross 1pha e^ Gamma Spec,Sr-90,C-14,U-235/238,Pu-239/240,Am-241 

'/s 9L 

[) Field Transfer of Custody Chain of Possession (Sign and Print Names) 

Relinquished by: '^J' fferirs Recei by: n 

ReliPned b 

ey: 

(/ /l^Jy 

Date/Time: 

Received by: yam. N j , , Date/Time: 



o So 

Comments: * 9cce, veJ G I M4 /hiJA`C A l lr 'i GJ -`1 Z ; G)^P^+Jen1 12•'Ri -9^ ° K6 

A • 6000-407 (12/90) (EF) WEF061 - 052 

Chain of Custody

Westinghouse 

Hanford Company SAMPLE ANALYSIS REQUEST 

Collector Date ^7, •/9Z 

Company contact WV SETZER telephone (509)376-2413 

Sample Date Time - 

• NUi(?er and Type of Sample Containers/Analysis Required 

Number 

Collected Collected 

" 1-250ml aG CLP;ICP/AA Metals,Hg,Cn 

-0 -120ml aG CLP;VOA 

W 1-950ml aG CLP;Semi-VOA,PCB/PEST 

02:2D 7 I?•/%•4z 12s1, 300.0/353.2;Anions(F,SO4,NO3) 

" 1-1000ml G Gross alpha/beta,Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 

j^Q$ $ IAS3 

1y250ml aG CLP;ICP/AA Metals,Hg,Cn 

-1-120ml 

vr950ml 

aG CLP;VOA 

aG CLP;Semi-VOA,PCB/PEST 

S3 300.0/353.2;Anions(F,SO4,NO3) 

vl-1000ml G Gross alpha/beta,Gamma Spec,Sr-90,C-14 

U-235/238,PLI-239/240,Am-241 




300.0/353.2;Anions(F,SO4,NO3) 


U-235/238,Pu-239/240,Am-241 

1. 




300.0/353.2 ;Anions(F,SO4,NO3) 

1-1 ml G Gross alpha/beta,Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 

urs 

*Type of Sample A = Air L = Liquid SE = Sediment T = Tissue x = Other 

OL = Drum Liquids O = Oil SL = Sludge W ' = Water 

DS = Drum Solids S = Soil SO = Solid WI wipe 

field Information FROM 100 #4-f Drilling 



A-6000-406 (06/91) WEF060 

() 5 3

Westinghouse 


Custody Form initiator ^ :M /iDS 



Project Designation/Sampling Locations 100 - NR- 1 Collection Date - -9,9 

Ice Chest No. .qML /73 Field Logbook No. _ EFL- • _ 1=i7 ^: ^^ 

Bitt oAflading/AirbiLt No. 966 7ac7A? Offsite Property No. 'î /q.'^- •d FJ/ZL p 





1 By B.o 1,250m I aG:(; ; CP AA Metals,Hg,Cn 



1,1000ml G/P:Gross alpha/beta,Gamma Spec,Sr-90,C-14,U-235/238,Pu-239/240,Am- 

241 

2),8&7G1f-p 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 




3)4Ji^ 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 



i—ra^^ ' ^ Gre•ss a•1-phatbet^Gamma Spe.G c on r 14 U 235/238 PN-^'â/24n,^m-241 

Was yz •/S^•QL 

%^L307Q66 1 ImQ aG:C/-P;ICP/R /t Ale /'00r,NS,Cn 

/ /doln ,4 896: CAP KQA 

/ 9,t n t9 aG : CAP yen - dOA, /i l3^Fest/udz , A^/e ^s ^F, SOy,/io3^ 

f 1 Field Transfer of Custody Chain of Possession (Sign and Print Names) 

Relinquished/-) . 4L;Ev1;5 Receiv by: Date/Time: 

Reli hed y: Rec/eived by: / / ,^ k' (1i IJn 

4f OVIJ '/U m 

Date/Time: 



Discosition 

Comments: 'f Rece ;veal (P `Tme /vC^CA^ 12-19 9 o^C,vec/ !2.2/-92 

Q S 

0Ff00 

A-6000-407 (12/90) CEF) WEF061 C: 5 4 


'K,3

Westinghouse 



Collector /G Date /^•/^Y•9Z 

company Contact WV SETZER telephone (509)376.2413 




1 250m1 aG CLP;ICP/AA Metals,Hg,Cn 

`1 20ml aG CLP;VOA 


s %/7.97, 10 5?49 300.0/353.2;Anions(F,SO4,NO3) 

1-1000ml G Gross alpha/beta,Gamina Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Ain-241 

7 Blo S /3/3 

250ml aG CLP;ICP/AA Metals,Hg,Cn 

^'-120ml aG CLP;VOA 

-950inl aG CLP;Semi-VOA,PCB/PEST 

^ 300.0/353.2;Anions(F,SO4,NO3) 

`7-I000nil G Gross alpha/beta,Gamma Spec,Sr-90,C-14 

U-235/238, Pt1-239/240, Ant-241 

1-250n11 aG CLP;ICP/AA Metals,Hg,Cn 

I 20ml aG CLP;VOA 

-950ml aG CLP;Seini-VOA,PCB/PEST 

//J. S"5— 300.0/353.2;Anions(F,SO4,NO3) 

WJS 11 235 ,Q •t 8 

n.. osnt^.nn n Dn t 

1-120ml aG CLP;ICP/AA Metals,Ng,Cn 


•• 1 -950ml aG CLP;Senli-VOA,PCB/PEST 

300.0/353.2;Anions(F,SO4,NO3)-- 

GuvS 

/z •Fi•9r_ 

*Type of Sample A = Air L = Liquid SE = Sediment T tissue x-_= Omer 

DL = Drum Liquids 0 = Oil SL = Sludge W = -Water 

DS = Drum Solids S Soil SO = Solid WI = Wipe 

Field Information FROM 100 N4—f Drilling 



A•6000 . 406 (06/91) WEF060 

055

PAYMENT -, 

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Total TranWorlab'm, Charged - 

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®56

ivery 

Contractor 

Westinghouse Hanford OFF-SITE 

Company I PROPERTY CONTROL 

PART I-TO BE COMPLETED BY ORIGINATOR 

CONTROLNUMBER -' 

(To be obtained from PROPERTYMANAGEM£NT) 

Depa rtment Environmental Section Env Field Services Unit Env Charac-& Sampling 

The following items are to be shipped from Contractor q Vendor 

Routing Air n Contractor q Vendor 

Shipped to 

THA/NORCAL 

2030 Wright Ave. 

Off-site Custodian 

Delores Sanchez 


Full Title 

Project Coordinator 

Quantity Description (Include Serial and any Government Tag Numbers) Original Cost 

5Y>fa 1 73 pol y cooler. Contains soil samples that a re N/A 

76& 

double-bagged and packed in wet ice and vermiculite. 

Samples are nonhazardous. 

S'AMlole +^': /^p7(3/^-d [^7tyFU ^67 .9 9' .(s'L 

^ ^^. 

WestinghouseI 


Custody Form initiator 

161ZI S'E TTE/Z- 



Project Designation/sampling Locations 100-NR-1. Collection Date /^' 7.9L 

Ice Chest No. 'qM 4- /7 1 Field Logbook No. L EFL- 166 4- 

Bill ofrLading/Airbill No. ^Z 5 1 gD0 76 23 offsite Property No. /Z^ D?9lZ2 7 



Possible Sample Hazards /Remarks None detected with field instruments. Maintain at 4C. 

Sample identification 

1)^,9g3 1,250m aG:CLP;ICP Meta s,Hg, n 


1,950ml aG:CLP;Semi-V0A,PC6/PEST,Anions (F,SO4,NO2,NO3)PH ^^ ^^ -,^ 

g4T' W 3 6 /z• 7. qz 

3) 




11 . os ,1912 Pit-239/240TAm-21 

a33s /Z•7.4L 

L aG:CLP;ICP/AA Metals,Hg,Cn 

1,120m1 a vs 

1,950ml aG:CLP;Semi- V0F,SO4,NO3) 

1,1000m1 G:Gross alpha/beta,Gamma Spec,Sr- 

U-235/238,Pu-239/240, Am-24 


Reli uis d by 

Received by 

Dare/Time: 

Z 

Relinquished by: ZJ 

^,;,,:: 

RecAved by: 

.d ata 

!R -1y-92 

Date/Time: 

(%KOG 'k 



0 

Commenes:.: ^7CCeIVet^ /R-!z 92 %M 4l/VJicL A I ') SpCN e d 1'-1'f-9z it 13 

A-6000 . 407 (12/90) (EF) WEF061 O 

Chain of Custody - 8

Westinghouse 



Custody Form initiator leye) r 7-7FA? 


Project Designation/Sampling Locations 100-NR-1 _ collection Date 9.9Z 

Ice chest No. Ry'yli.- 171_ Field Logbook No. EFL- /Q( 

Bill oflLading/Airbill No. ea T-Z 966 `j j' A 3 offsite Property No. ^^93 O 0/ZZ ^..^ 





1),C3o.^^^ i,Zbuml au:LLV;1l.N/ AA McLals,tlg,un 



>14,6 

IA141-4 

Ni 


1,120ml aG:.CLP;VOA 


wry /2.g.yz 

3)a(G:CLP;ICP/AA Metals,Hg,Cn 

1,120m1 a : wvs 

1,950ml aG:CLP;Semi-VOA,P F SO4,NO3) 

1,1000ml G:Gross alpha/beta,Gamma Spec,Sr-90, , - 35/238,Pu-239/240,Am-24 

P Field Transfer of Custody Chain of Possession (Sign and Print Names) 

Relin uished by Rec /lived by- 

{9U 

M J /,' b1 4"1 . 

, 

Date/Ti: m 


Relinquished by: Received by: :Date/Time: 


Co mm ents: 

9 

1.2-11 .2 -1' - / 2- 81e00 

;C)2c e, ve,) /z-12-9 7 C 7MA^No2cAI oFe,led 12 1191 IKR 

A-6000-407 (12/90) (EF) WEF061 - 

Chain of Custody n ()

M 

Westinghouse 



Collector /,/ Date /2—/D • 9Z 

Company Cantact WV SETZER Telephone (509)376-2413 

Sample * Date Time 



1-250ml aG CLP;ICP/AA Metals,Hg,Cn 1 



egO7^93 S 1,2-7.9z O9/6 Anions(F,SO4,NO2,NO3)PH 

` 1o•^1Z7, ^^^/^â Pii 9'to/9dn e m_ •JA7 ' 

5 

1-250ml aG CLP;ICP/AA Metals,Hg,Cn I 



42 . 7-2 1,31s— Anions(F,SO4,N0,NO3)PH 

I tnnn l a r_,._ ._ .,^..--^-^. 2 r_, c„e,- c v._af1 r_td 





> 

/L 4 0,4 ^!L 



1-950m1 aG CLP;Semi-VOA,PCB/PEST 


wvs 

- 

us ' i 

*Type of Sample A = Air L = Liquid SE = Sediment T = Tissue X-.= Other 

DL = Drum Liquids O = Oil SL = Sludge W = Water 





A-6000-406 (06191) WEF060 

1 

060 

i

Westinghouse I 



Custody Form Initiator gzk/ ,5°e 7-Z6.t- — 

Company Contact WV SETHR Telephone 376-2.413 

Project Designation/Sampling Locations 100-NR-1 Collection Date 1.21 S^•9Z_ 

Ice Chest No. Srn I- ax3 Field Logbook No. EFL- •/ZeZ 

Bill o£tLading/AirbiLL No. _ aT/ 90D V 2 3 Offsite Property No. "-- 7 6-OnZZ qr-S 





1) 99^^ 250m] aG CLP;ICP/AA Metals,Hg,Cn 

^120ml aG:CLP;VOA 

v: 950ml aG:CLP;Semi-VOA,PCB/PEST,Anions (F,SO4,NO2,NO3)PH 

7 400 i G i aro_e _°i..u. i^^.., n_ê c c,- nn !• t n ilôa /94A o , ^ZO /94f1 

N-1• LUV5 / 2. a0 .5'Z 

2)&7 q6 ^4,250ml aG:CLP;ICP/AA Metals,Hg,Cn 

1d,120ml aG:CLP;VOA 

^-1 ,950ml aG:CLP;Semi-VOA,PCB/PEST,Anions (F,SO4,NO3) `— 

W05 fe-ed •RZ_• 

3&o;; 981,250ml aG:CLP;ICP/AA Metals,Hg,Cn 



tuu9 /z• /d •qZ 

() Field Transfer of Custody Chain of Possession - (Sign and Print Names) 

Relin wi shed Y Rec ived b Y. 7^ 

ERMa f ^^3M 

Relinquished by. Received by: Date/Time: 



Final Samp le Disposition 

Disposal Method: I Disposed by: i Date/Time: 

Comments: * received C@ 7M411V60ZA1 12 42 -92 

A-6000-407 (12/90) CEF) WEF061 


Date/Time: 

12 - 1H 9z ©Soo 

Ope'U C C) !z'1Y-92 

061

1 

Westinghouse 


Custody Form Initiator L/^!/. 11-^TZ Cam!?_ 

Company Contact WV SETZER 


Ice Chest No. -s mi— a3S 

Bill oftLading/Airbill No. 




Telephone 376-2413 

Collection Date IL•k'9 

Field Logbook No. - EFL- 16&, 

offsite Property No. //-?-(1 -6&Z 2^r,' 


1 Bo7^Q ,250m aG:CLP;IC AA Meta s, g,Cn 

7;,,,120ml aG:CLP;VOA 

^,950ml aG:CLP; Semi -VOA, PCB/PEST, An ions (F,SO4, 02,03)PH 

t t - - 

241 

wus iL.y.q z 

2)250ml aG:CLP;ICP/AA Metals,Hg,Cn 

1,1 G:CLP;VOA 

1,950m1 aG: ni-VOAPCB/PEST,Anions (F,SO4,NO3) 

1,1000ml G:Gross a p a Gamma Spec,Sr-90,C-14,U-235/238,Pu-239/240,Am-241 

W VS 

3) 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 


1,950ml aG:CLP;Semi-VOA,PCB/PEST,Anions (F,SO4,NO3 

I,1000ml G:Gross alpha/beta,Gamma Spec,Sr-90,C-14,U-235 Pu-239/240,Am-241 

() Field Transfer of Custody Chain of Possession - 

Rail uished by¢ Received by: xen M , •f 'S/UM Date/Time: 




Disposal Method: Disposed by: Date/Time: -- 

(Sign and Print Names) 

Comments; i-- Rec eived C `-TmA 19ojZCA/ 1^'l?.-^^ ; ^"pe.ved ;z-^`/-92 • kI3 - 

A-6000 . 407 (12/90) (EF) WEF061 - ^^ 6 2 

Chain of Custody

Westinghouse 


I 


Collector___WW &45 7-Z Date 1/17 •/O.9Z 


Sample 

Number 

* Date 

Collected 

Time 

Collected 





ÔTQ95 6 za g .9z 68410 Anions(F,SO4,NO2,NO3)PH 

, 

aus^^•.o •^z, 

O p^ S 

^ 9p ^ ' 




/o/S Anions(F,SO4,NO2,NO3)PH 

1 1990m; G Gross- beta,Gawa Spar Sr-90 C-14 

WOS 12• 1O •q z- 




7^ 9A S ^^•8.4a /^ o Anions(F,SO4,NO2,NO3)PH 

2 s 

W 35 /L•/a•rtL 




l^ 9 9z 1^4^ Anions(F,SO4,NO2,NO3)PH 

t2•/o.yz 

*Type of Sample A = Air L = Liquid SE = Sediment T = Tissue X-= Other 






A-6000-406 (06/91) WEF060 

v 

m -

1 

WestinghouseI 


Custody Form Initiator cig Hge, 

e! G 

I 


Company Contact WV SETZER Telephone 376 - _2413 

^ 11 


collection Date /52'10-9a 

Ice Chest No. .5m /- - / 

^1 // - 99-1( 

Bill of-tLading/Airbill No. P'7 I q00 /10X ^/ n 

- 1 

Field Logbook No. EFL- l 

offsite Property No. f/J 3 -0- 0,;r • 





1,z!)umI au:LLV;1Li'/AA metials,ng,Ln 



JV,L - lY,V'LJ J/GJV,I U-LJ'/.TV,. uu 

2) 6^LO'7^'1 s,6-5 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 



3) aG:CLP;ICP/AA Metals,Hg,Cn 

I,12 n - P;VOA 

1,950m1 aG-CLP. PCB/PEST,Anions (F,SO4,NO3) 

1,1000ml G:Gross alpha/be a,Gamma—Sp c Sr-90,C-14,U-235/238,Pu-239/240,Am-24 

fl Field Transfer of custody Chain of Possession (Sign and Print Names) 

Re hed by :,yRR ^?e Ve S 

-^ ^ y6 

Received by: kekmi"f-BI 3.M 

fS 

Date/Time: 




Disposition 

^ - - 2 c95Sc, o 

Disposat Method: I Disposed by: I Date/Time: 

Comments: * Rece, ved 12-12-9Z L `&41Nonca 1 ; ©peived 12-/d-92 ' Ke 

A-6000-407 (12/90) (EF) WEF061 " v 4 

Chain of Custody

Westinghouse 



Collector .l2 k?t/8C Date l /fJ=q 


Sample 

Number 

Date 

Collected 

Time 

Collected 


9^ 

AP-/O- 

O 4 

_7 



1-950m1 aG CLP;SVOA , /mi- PCB/PE(T) pH 

300.0 353.2 ;Anions. ^ IC F,SO4,NO3, NO2 

A) S !a ./n_ 9Q 133 


I -120ml aG CLP;VOA 


300.0/353.2;Anions (IC) F,SO4,NO3,NO2 

oanioen nM_241 

V LJ J/ LJf 






U-235/238,Pu-239/240,Am-241 


^li,q 120ml aG CLP;VOA 

â' 1-9 1 aG CLP;Semi-VOA,PCB/PEST & pH 


1-1000ml ross alpha/beta,Gamma Spec,Sr-90,C-14 

- 35/238,Pu-239/240,Am-241 



DS = Drum Solids a = Soil SO = Solid WI = Wipe 

Field Information FROM 100-0-1 Drilling 



A-6000-406 (06/91) WEF060 

()6a'

Westinghouse 


Custody Form Initiator t—y)g R ELF—(/^S 



Project Designation/sampling Locations 100-NR-1- Collection Date /9-09-9:21/I^ 

ice Chest No. SM L 17.R Field logbook No. EFL- /t^leiJ 

Bill ofOLading/Airbiil No. lull 900 7(. ;2 3 Offsite Property No. /d/ ^3 I 041/ Z Z t'T ? 





I ) &;'7Q58 i,c5umi aG:CLN;it.F/AA metals,Hg,Cn 


1,950ml aG:CLP; Semi -VOA, PCB/PEST,Anions (F,SO4,NO2,NO3)PH 

1,1000ml G/P:Gross alpha/beta, Gamma Spec, Sr-90,C-14,U-235/238,Pu-239/240,Am- 

241 . 

2),0r1-QBq 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 



1,1000ml G:Gross alpha/beta, Gamma Spec, Sr-90,C-14,U-235/238,Pu-239/240, Am- 241 

3)BO'Melo 1,250m] aG:CLP;ICP/AA Metals,Hg,Cn 




I Field Transfer of Custody Chain of Possession (Sign and Print Names) 

Relinquished by:dfl 6 -S Received by: Date/Time: 

>^ ff 1,2 J9 .12-, ¢ Lz^ Gam• pl^ / -/D Z /41 6 e) 

Relinq • shed Received by: Ke/tM i(' f3JUM Date/Time: 

Z7 3 ( w 1)-) 4--97 0?00 



Final Samp le Di 

Disposal Method: I Disposed by: I Date/Time: 

Co mm ents: ^ 

'k 1\ec e-: •vec) J ^- -JR•9 ;Z. @ 7i-1 4 / N00,c.o( , ,DPCNed 1) , -1y-9 2 K13 

A • 6000 .407 (12/90) CEF) WEF061 

Chain of Custody n66

I 

Westinghouse 

Hanford Company SAMPLE ANALYSIS REQUEST - 

Collector ET? Date /Z•/o 9r 


Sample 

Number 

^ ,^^ Q^ 

CU 

Date 

Collected 

Time 

Collected 

S ^•î 4L Oal r7 

S 

S 


-250ml aG CLP;ICP/AA Metal s, Hg,Cn 


4-950ml aG CLP;Semi -VOA, PCB/PEST 


d 1000ml G Gross alpha/beta, Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 

-250m1 aG CLP;ICP/AA Metal s, Hg,Cn 



LET o^^ a Anions(F,SO4,NO2,NO3)PH 

!' :5^ 2 Gird 


U-235/238,Pu-239/240,Am-241 

-250ml aG CLP;ICP/AA Metals,Hg-rGn. 

1 120ml aG CLP;VOA 

\I-950ml aG CLP;Semi-VOA,PCB/PEST 


-1000ml G Gross alpha/beta, Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 

1-120m1 aG CLP;ICP/AA Metals,Hg,Cn 


1-950ml aG CLP;Semi-VOA,PCS/PEST 



U-235/238,Pu-239/240,Am-241 

w3$ 

*Type of Sample A = Air L = Liquid SE = Sediment T = Tissue XJ= Other 






A-6000-406 (06/91) WEF060 

('67

fib' orb 

FORM OF PAYMENT SERVICES" INTERNATION, 

. 

UNITED =ES / CAMDA 

El 

0 

El S 

"N 

q tZ. co=m) El s--ftd m- El B=l Dper 

F1 C^ 

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il Wwy shw^KJ 

--Els-wDay 

L VON Cat 

Car A Im" 

6-666r 

Inlu D RMNT "WtNe0ov d4o 

ICHLAND 

BLDG- 1163 

.4300 c^"nti"s PG3J'WP=0-0KZ#351 9:?352 

w bf 

L YCOOLEt' 

'1 1 ^vtl 

!6 

I I 1 1`1 

SOIL $WÊ& 

IN 

Ship 

Farr 1 L iments SWt.^ within Shlq. 'rite 

5 

h4lUthV 

b. o :dt^bn' Ô oh^k kl^. 

kTURDAY DrMVIRY this . an v nF 

. 

th.t'th. Zip Sh'5 

[ }1 I d. 

3wes 

=% the nqlh4 appti. 

wrA.J 

"W""OeVy E;d. 

F,m;o mbwy Z( [ET 

Id P" i4vng 

fm'-'o 

^twwmr* 

TR 

'Consignee's Account Number 

-n^ 

CARna 

FOR INFORMATION OR RATES 

CALL 1-80 0 44 EMERY 

(I-BOQ-44 3-637 2 

I r 

s -'^ ^ - 

-" 'l 50 

2 5 1 9 0 G 76 8`4 

1. 

Mark' 4ak Emery 

Inteinnational Gus !omsyalue Inlenw t' tionat fnsu^ce,.t 

Total Trans;"tafion Charges 

Pa 

T 

s O'n, 

Back 

$ 

^sccept,' r 

check with all 

being assualae, 

Shipper, indluc 

but not limItec 

non-paym?nt^. 

and miSrapras( 

Declared Vt 

n68

4) ML t7( 

Overni ht Deliver 

Contractor 

Westinghouse Hanford 

OFF-SITE 

Company PROPERTY CONTROL 

Depa rtment Environmental I 

PART I - TO BE COMPLETED BY ORIGINATOR 

CONTROL NUMBER 

(TO be obtained from PROPERTY MANAGEMENT) 

3 o , ./2 36 0 q -e 

Section Env Field Services Unit Env Charae k Sampling 

The following items are to be shipped from KI-Contractor q Vendor 

Routing Air ® Contractor q Vendor 

Shipped to Off-site Custodian 

TNA/NORCAL Delores Sanchez 

2030 Wright Ave. Full Title 



Quantity Description (Include Serialandany Government Tag Numbe rs ) Originai Cost 

S 

^3 . 

3P?4-I 'll poly cooler. Contains soil samples that are N/A 



5i9n 11ft.F 'S (1070 14 ,u"t d4 '6 

gT) I 1_ ^1 3:Qofy CoCIEF:.i:urJT'ri {n.S tt.11 'sno , l)E5 +ko,+Al i E f 

Tt.U&1E I ;P G^64 A"T> FACt4ED IN Oar ICE ANt^ IiEIZW%C11d&. 

FPM + IE< Pr,` J i,N - H p^Zn (uu5. 

Samplre 

f G76 /sr /,,, ley le, HG?!^ 7'P I i-G 

q Class ified [2 Unclassified I] Shipped UnderOOE Co ntract q Shipped Under Co tractor's Use Permit Contract 

Necessity for the Off-Site Use of this Prope rty 

To support drilling and sampling at the 100 Areas 

Bill of Lading 2, 3 

1. 

CERTIFICATION OF THE RADIAL GN MONITORING RELEASE MUST BE SECURED THE SAME DAY THATMATERIAL IS DELIVERED TO SHIPPING. 

RM Clearance for Pub 'c Release RM Survey No Date 

Location of Prope rty (Area & Bldg.) 

100 Area 

Conta ct 

W. V. Setzer 

i 

N/A 

Phone 

376-2413 

Date Ready for Shipment Cost Code to be Charged Approximate Date This 

/q. 16 PG3BF 84300 Property will be Returned N/A 

Originated ey , 

/.^„ 

Relinquished by: r, cu 

it •r 

o'n 

r.'r 

Date 

G -°L 

Authond z By 

.'t. i, ,/^.'i. •, i 

Date 

/S,j . Y(^, . `/:. 

Signature and Nameof Prope rty Control Custodian Date Property Managgment /A 

pproval/ Date 

PART I I - TO BE COMPLETED BY SHIPPING 

Signature of Recipient ^ Return Order No. Date Issued Purchase Order No. Date Issued 

Date 

By O rig inator 

DISTRIBUTION 

Shipping Operation- Sion all Couiesand Forward to: 

'+vv 

White, Green, Yellow, Pink- Prope rt y Management 

Goldenrod - Reta in 

White-Property Management Green-Prope rty Control Custodian(Issuing Office) 

Yellow-Retain Pink -Originator 

i 

.. onnn e+necoma

Delivery. 

. :1?; :1.. 

Contractor I CONTROLNUMBER 

OFF-SITE, 

(To be obtained from PROPERTYMANAGEMENT) 

Westinghouse Hanford _ _ 

:_,._,._._; _.__ .._^ -, _. ^_^_ - ..... _ .. 

Company PROPERTY CONTROL J ^bs 

7Nrk3="^ M^'O ^ly cooler. Contains soil samples that N/A 

are double-bagged and packed in wet ice and vermiculite. 


Sample III: 

q Classified ® Unclassified 0 Shipped Under DOE Contra ct q Shipped Under Contractor's Use Permit Contract 

Necessity for the Off-Site Use of this Prope rty 

To support drilling and sampling at the 100 Areas. 

gill of Lading: 

CERTIFICATION OF THE RADIATION MONITORING RELEASE MUST BE SECURED THE SAME, DAY THAT MATERIAL IS DELIVERED Td.SHIPPING, 

RM Clearancefor Public Release_ . -` `•-` "' ""-""'"" - •MSUrve o--r.•-,-.--- 

Location of Property (Area & Bldg.) 

1 .00 Area 

Contact 

W. V. Setzer 

Date Ready for Shipment 'r ;CostCode to be Charged 

i _P-8$45- ,u(,.UQ. - '^' _ 

Date This 

Prope rty will be Returned 

Phone„ 076-2413 

Origôared By n t pate Authonzed By Date 

Signature and NameiSf Prope rty Control Custodian Date Propert.:Nt ,ErAent^WPp~fâ l-,_ Date 

PART I I -TO BE COMPLETED BY SHIPPING 

Signature of Recipient Return Order No. Date Issued Purchase Order No. Date Issued 

Date + ? I' . C(1 

DISTRIBUTION 

By Originator- Shipping Operation- Sian all Copies and Forward to: 

r• 

it (,v 

White, Green, Yellow, Pink. Prope rty Management 

Goldenrod-Retain 

White- Pr6pe rty Management Green-Prope rty Control Custodian (issuing Office) 

Yellow-R&tam Pinlc I Originator 

. ' - ""' - •• , - .. _._ . 54 3000-47910989) 

N/A 

i.

Overnight Delivery 

Contra ctor 

Westinghouse Hanford 

Company 

OFF-SITE 

PROPERTY CONTROL 

PART '1-TO BE COMPLETED BY ORIGINATOR 

Department Environmental Section Env Field Service "'t 

Y. 

CONTROLNUMBER 

(robe obtained from PROPERTYMANAGEMEii 

CI3^Q^ 

W 012 2 W%349. 

The following items are to be shipped from [Contractor q Vendor - 

Routing Ai r ® Contractor 0 Vendor 

Shipped 

tO MA/NDRCAL 

Off-site Custodian 

2030 Wright Ave. 


Delores Sanchez 

Full Title 


Quantity Description,- •,(lnclude Serial andany Government Tag Numbers) Original Cost 

S.4rIE-1 7b poly cooler. Contains soil samples that a re N/A 



Sample 1!': %^li7l^/^'^ f-G7^.h •>^ F^07'îl:G^ n 

wvs /^•ya.yz 

r^-r'r^ 

q Classified ® Unclassified q Shipped under DOE Contra ct q Shipped Under Contra ctors Use Permit Contract 

Necess it y for the Off-Site Use of this Prope rty 

To support drilling and sampling at the 100 Areas 

Bill of Ladin 91 ^7 - 

CERTIFICATION OF THE RADIATION MONITORING RELEASE MUST BE SECURED THE SAME DAY THAT MATERIAL IS DELIVERED TO SHIPPING. 

RM Clearance fo Public Release 

RMSurvey No 

/^ 1 -'-., Z ^/ 7 //I-- v - 

Conta ct 

Pho 

W. V. Setzer 

r 76-2413 

Location of Prope rty (Area & Bldg.) 

100 Area 

Date Ready for Shipment 

^•/U • 

Cost Code, to be Charged 

PG^38F 84300 

Date 

Approximate Date This 

P lopertywill be Returned N/A 

Origmated By* KV i nquT sheiT y: r. «Ar Date Authorized By Date 

Signature and Name of droperty Control Custodian Date Property Management Approval Date 

Signature of Recipient 

i 

Date 

PART I I -TO BE COMPLETED BY SHIPPING 

Return Order No. Date Issued Purchase Order No. Date Issued 

DISTRIBUTION 

By O riginator Sh ipping Operation -Sign all Copies and Forward to: 

White, Green, Yellow, Pink-Propert y Management White-Prope rty Management Green-.P.roperty Control Custodian(Issuing Office) 

Goldenrod - Reta inYellow-Retain Pink-Originator 

i 

I 

S430011.474I0WR01 

I

LABORATORY : TMA/ARLI 

CASE : 12-074 


CONTRACT ID : WESTINGHOUSE HANFORD COMPANY 

SDG RECEIPT DATE : December 21, 1992 

1.0 DESCRIPTION OF CASE : 

Six soil samples 

Semivolatiles and 

Laboratory Program 

Revision OLMOI.S. 

2.0 SAMPLE LIST : 

WESTINGHOUSE ID 

9070D7 

B07QD7 MS 

B07QD7 MSD 

B07QD7 

B070D7 MS 

B070D7 MSD 

B070DS 

B070DS 

B07QDB MS 

9070DS MSD 

B07QD9 

8070D9 

B070FO 

B070FO 

B07QB5 

B07QB5 

B07086 

B07QB6 

3.0 COMMENTS : 

3.1 SHIPPING AND DOCUMENTATION : 

P61 9q^6- 

^0/2Q93--Tm,g-'39^ 

000002 

were analyzed for TCL Organics- Volatiles, 

Pesticide/PCBs according to the USEPA Contract 

(CLP) Statement of Work for Organic Analysis, 

ANALYSIS 

LAB ID REQUESTED MATRIX 

A2-12-074-0 1A V SOIL 

A2-12-074-0 1B V SOIL 

A2-12-074-0 1C V SOIL 

A2-12-074-0 1D SV & P SOIL 

A2-12-074-0 1E SV SOIL 

A2-12-074-0 1F SV SOIL 

A2-12-074-02A V SOIL 

A2-12-074-02B SV & P SOIL 

A2-12-074-02C P SOIL 

A2-12-074-02D P SOIL 

A2-12-074-03A V SOIL 

A2-12-074-03B SV & P SOIL 

A2-12-074-04A V SOIL 

A2-12-074-04B SV & P SOIL 

A2-12-074-05A V SOIL 

A2-12-074-058 SV & P SOIL 

A2-12-074-06A V SOIL 

A2-12-074-06B SV & P SOIL 

All of the samples were received and properly documented. A 

950mL bottle was received at TMA/ARLI unlabeled. Per TMA/NORCAL 

and the process of elimination, the sample was determined to be 

B07QF0.

3.2 ANALYSIS 

3.2.1 VOLATILE ANALYSI$_ ;COMMENTS : 


000003 

The samples were analyzed by heated purge within the CLP SOW 

holding times. 

All of the CC results were within the limits specified by 

the EPA CLP SOW. 

TUNES : 

All of the BFB tunes are injected directly into the GC/MS 

instrument. 

3.2.2 SEMIVOLATILE ANALYSIS COMMENTS : 


The samples were extracted and analyzed within the CLP SOW 

holding times. 

All of the CC results were within the limits specified by 

the EPA CLP SOW. 

3.2.3 PESTICIDE/PCB ANALYSIS COMMENTS : 

SEQUENCE NOTES : 

The sequence was started on 01/05/93 and analyzed in 

accordance with the EPA CLP SOW. The sequence was analyzed 

by single injection into a dual column system. The sequence 

met all the CC criteria specified in the CLP SOW. 

The Chromatograms are presented in the manner consistent 

with the capabilities of the Nelson 2700 Turbochrome Data 

System which normalizes the largest peak to scale. 

SAMPLE NOTES: 


The samples were extracted and analyzed within the CLP SOW 

holding times. Sample BO70DSMS had a percent difference 

between the two GC columns for all of the spiking compounds 

and surrogates greater than 20%. The high percent 

difference appears to be due to unequal amounts of the 

sample injected into both columns. The percent difference 

for Dieldrin and 4,4'-DDT were greater than 25%. Therefore, 

Dieldrin and 4,4'-DDT have been "P" qualified.

000004 

All of the other OC results were within the limits specified 

by the EPA CLP SOW. 

We certify that this data package is in compliance with the terms and 

conditions of the contract, both technically and for completeness, for 

other than the conditions detailed above. Release of the data in this 

hardcopy data package and in the computer-readable data submitted on 

diskette is authorized by the Laboratory Manager or his designee, as 

verified by the following signatures. 

Nicole Roth Wida Ang 

CLP Program Manager Organics Supervisor

00P005 

1A 

VOLATILE ORGANICS ANALYSIS DATA SBEET 

EPA salaw NO. 

Lab Name: TMA/ARLI Contract: NBC 

1 

I B07QB5 

I 

I 

) 

i 




Level: (low/med) IOW 





Lab File ID: 21223RII 

Date Received:.}j21/92 



Soil Aliquot Volumes (UL) 



i I 


1 it IU 

74-83-9 --------- Bromomethans 1 11 III 

75-01-4---------Vinyl Chloride I it IV 


75-09-2---------Methylene Chloride 2 1J 

67-64-1---------Acetone I 9, I&7 

75-15-0---------Carbon Disulfide 1 11 III 

75-35-4 --------- 1,1-Dichloroethene ( 11 III 

75-34-3 --------- 1,1-Dichloroethane I li III 

540-59- 0 -------- 1,2-Dichloroethene (total)_I it III 

67-66-3---------Chloroform 1 11 IV 

107-06-2 -------- 1,2-Dichlorcethane 1 11 1v 

78-93-3 --------- 2-Butanone 1 it IU" 

71-55-6 --------- 1,1,1-Trichloroethane 1 li IV 

56-23-5---------Carbon Tetrachloride I li 1U 

75-27-4 --------- Bromodichloromethans 1 it III 

78-87-5 --------- 1,2-Dichloropropane 1 11 IV 

10061-01-5 ------ cis-1,3-Dichloropropene 1 11 IV 

79-01-6 --------- Trichloroethene 1 11 IV 

124-48-1 -------- Dibromochloromethans 1 it IV 

79-00-5 --------- 1,1,2-Trichloroethane 1 11 III 

71-43-2---------Benzene 1 11 III 

10061-02-6 ------ trans-1,3-D chloropropene 1 11 

IV 

75-25-2 --------- Bromoform 1 11 III 

108-10-1 -------- 4-Methyl-2-Pentanone I 11 III 

591-78-6 -------- 2-Hexanons I 11 III 

127-18-4 -------- Tetrachloroethene 11 III 

79-34-5 --------- 1,1,2,2-Tetrachloroethane 1 11 IV 

108-88-3--------Toluene i 4- IJ 

108-90-7 -------- Chlorobenzene 1 11 IV 

100-41- 4 -------- Ethylbenzene 1 11 III 

100-42-5--------Styrene i 11 III 

1330-20-7 ------- Xylene (total) i 11 III 

I---- 

FORM I VOA 

3/90

Lab Nacre: 

lE 



Lab Code: THALA Case No.: 12074 



Level: (low/med) lg^ 

i' Moisture: not dec. _ 9 




Contract: WHC 

00110('G 


I- B07QB5 



S^ Lab Pilo ID: 21223R11 

Date Received: '12121/92 



Soil Aliquot Volume: _(UL) 

CONCENTRATION UNITSS 


CAS NUMBER COMPOUND NAME ( RT EST. CONC. Q I 

ssass:asssssz^ I ssss I sasyso I `ssa^ss 


3/90

000007 

lx EPA SAMPLE NO. 


I I 

I B07QB6 I 

Lab Name: =/ARLI Contract: NHC I I 

Lab Code: TMALA Cass No.: 12074 SAS No.: NA SDG No.: Imo_ 



Level: (low/Red) JAF- 

% Moisture: not doe. _3 




I 

74-87-3 --------- Chloromethans 1 



Date Received:- 12/21/92 



Soil Aliquot Volumes (uL) 


(uq/L or uq/Kq) UG/XG Q 

10 I V 

74-83-9 --------- Bromomethane 1 10 I v 1 

75-01-4---------Vinyl Chloride 1 10 III 1 

75-00-3 --------- Chlorosthans 1 10 III 1 

75-09-2---------Methylene Chloride i 2 IZT 1 

67- 64-1---------Acetone i 12 IB 1 

75-15-0---------Carbon D sulf de I 10 III 1 

75-35-4 --------- 1,1-Dichloroethene I 10 III 1 

75-34-3 --------- 1,1-Dichloroethane 1 10 III 1 

540-59- 0 -------- 1,2-Dichlorosthene (total)_[ 10 IV 1 

67-66-3---------Chloroform [ 10 IV 1 

107-06-2 -------- 1,2-Dichloroethans i 10 I V1 

78-93- 3 --------- 2-Butanons 1 10 III 1 

71-55-6 --------- 1,1,1-Trichloroethans I 10 IU 1 

56-23-5---------Carbon Tetrachloride i 10 I V1 

75-27-4 --------- Bromodichloromethans7- 1 10 I V1 

78-87-5 --------- 1,2-Dichloropropens 1 10 I V1 

10061-01-5 ------ cis-1,3-Dichloropropens 1 10 IV 1 

79-01-6 --------- Trichloroethene I 10 I V1 

124-48-1 -------- Dibromochloromsthane 


71-43-2---------Benzene 


75-25-2 --------- Bromoform 

108-10-1 -------- 4-Methyl-2-Pentanone 

591-78-6 -------- 2-Hexanons 

127-18- 4 -------- Tetrachloroothens 


108-88-3--------Toluene 


100-41-4 -------- Ethylbenzene 

100-42-5--------Styrene 

1330-20-7 ------- Xylene (total) 

1 

1 

1 

1 

1 

I 

1 

1 

I 

i 

I 

10 1u1 

1II_ 

10 

1 

10 IV 1 

10 IV 1 

10 Iv I 

10 IV 1 

10 III 1 

10 I U1 

10 III 1 

11 1 I 

10 III 1 

10 III 1 

10 IV 1 

I I 

FORM I VOA 

3/90 

1 

1 

1

Lab Name: 

000008 

la EPA SAIQ+LE NO. 

VOLATILE ORGANICS ANALYSIS DATA SHF= 


Lab Code: ZK&L&_ Case No.: 12074 


Sample wt/vol: 5.0 (g/AL) 

Level: ( low/med) jam_ 

4; Moisture: not dec. _3 




Contract: NHC 

I 807496 

SAS No.: NA SDG No.: g&! 


St__ Lab File ID: 21223R12 






(ug/L or ug/Kg) VG/KG 

CAS NUMBER I COMPOUND NAME I RT I EST. CONC. 1 4 1 

mama.:aa^sa:ate I aasaa:aoaâ^saa^vaaaâs I C I ^wrvoô I aso I 

I i I I I 

FORK I VOA-TIC 3/90

1A. 

VOLATILE ORGANICS ANALYSIS DATA SBSBT 

Lab Name: TMK/ARLI Contract: WHC I 

11 

11 

11 

11 2. 

12 

it 

11 

11 

11 

11 

11 

112 

11 

11 

it 

11 

11 

11 

11 

11 

11 

11 

11 

11 

11 

it 

11 

11 

it 

11 

11 

000009 


I I 

B07QD7 

Lab Code: THALA . Case No.: 12074 SAS No.: NA SDG No.: NA 

Y_ 


Lab Sample ID: A212074-01h 

Sample wt/vol: 5.0 (9/mL) Q 

Level: ( low/Red) UN 

8 Moisture: not dec. _ _6 





74-83-9 --------- Bromomethane 


75-00-3 -------- -Chloroethane 

75-09-2---------Methylene Chloe, 

67-64-1---------Acetone 

75-15-0---------Carbon DD su^da 



540-59-0 -------- 1.2-Dichloroethene 

107-06-2 -------- 1,2 -Dichloroethane 

78-93-3 --------- 2-Butanone 



75-27 -4 --------- Bromodichloromethane 


10061-01-5 ------ cis-1 , 3-Dichloropropene 


79-00-5 --------- 1,1,2-Trichloroethana, 

71-43-2-------- -Benzene 

10061-02-6 ------ trans-1,3-D chloropro 

591-78-6 -------- 2-Nexanone 

127-18-4 -------- Tetrachlorne 

79-34-5 --------- 1,1,2,2-Tetr. 

108-88-3--------Toluene 

108-90-7 -------- Chlorobenzen 

100-41-4 -------- Ethylbenzene 

100-42-5--------Styrene 

1330-20-7 ------- Xylene (tots 

FORM I VOA 

Lab Pilo ID: 21223R05 

Date Received:- 12121/92 




III 

iU 

IU 

III 

IJ 

IB 

III 

I V 

IU 

III 

III 

ID 

ID 

Ii 

III 

III 

III 

U UU 

U U 

1.0 


(uq/L or u9/R9) UG/RG a 

(UL) 

3/90

Lab Name: 

Lab Code: THALA 

. 13 

V0LATILE ORGANICS ANALYSIS DATA SHEET 



Case No.: 12074 

Sample wt/vol: 5.0 (q/NL) G 

Level: (low/med) Uff_ 




Contract: WHC 

000CILO 


I B07QD7 

SAS No.: NA SDG No.t 

Lab Sample ID: A212074-OIA 


Date Received:-- 12121/92 




Number TICS found: _Q (uq/L or uq/Kg) UG/KG 


CAS NUMBER COMPOUND NAME RT EST. CONC. I Q 

FORM I VOA-TIC 3/90

Lab Name: TMA/ARLI -- 

lA 


Lab Code: TMAIA Case No.: 12074 


Sample wt/vol: 5.0 (g/RL) Q,_ 

Level: (low/Red) ID _ 

4; Moisture: not dec. _ 4 

GC Column: PACK ID: 2.00 (mR) 

Contract: NBC 


nonoi1 

EPA SAMM NO. 

1 I 

1 B07QDG I 

I I 


Lab File ID: 21223ROS 






CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 

74-87-3 --------- Chloromethane 1 10 III 



75-00-3 --------- Chloroethane I 10 jU 

75-09-2---------Methylene Chlor de I 2 IJ 

67-64-1---------Acetone j 14 IS 

75-15-0---------Carbon Disulfide j 10 IU 

75-35-4 --------- 1,1-Dichloroethens 1 10 jU 

75-34- 3 --------- 1,1-Dichloroethane I 10 JU 

540-59-0 -------- 1,2-Dichloroethene (total)_] 10 III 

67-66-3---------Chloroform j 10 jU 

107-06-2 -------- 1,2-Dichloroethans j 10 III 

78-93-3 --------- 2-Butanone j 10 jU 

71-55-6 --------- 1,1,1-Trichloroethane j 10 IV 

56-23-5---------Carbon Tetrachloride j 10 III 

75-27-4 --------- Bromodichloromethane 1 10 jU" 

78-87-5 --------- 1,2-Dichloropropane 1 10 jU 

10061-01-5 ------ cis-1,3-Dichloropropene j 10 jU 

79-01-6 --------- Trichloroethene ( 10 III 

124-48-1 -------- Dibromochloromethane i 10 1 t 

79-00-5 --------- 1,1,2-Trichloroethane j 10 Ju - 

71-43-2 --------- Benzene j 10 jU 

10061-02-6 ------ trans-1,3-D chloropropene I 10 IU 

75-25-2 --------- Bromoform j 10 1U 

108-10-1 -------- 4-Methyl-2-Pentanone j 10 jU 

591-78-6 -------- 2-Hexanone ( 10 jU 

127-18-4 -------- Tetrachloroethene I 10 jU 

79-34-5 --------- 1,1,2,2-Tetrachloroethane I 10 jU 

108-88-3--------Toluene 1 1- IJ 

108-90-7 --------- 1 10 

IU. 

100-41-4 -------- Ethylbenzene 1 10 jU 

100-42-5--------Styrene 1 10 IU 

1330-20-7 ------(total) 1 10 IU 

FORM I VOA 

I 

0 

3/90

la 



Contract: Lab Name: WHC 1 

SAS Lab Code: TMALANo.: Case No.: 12074 NA_ SDG No.: NA 

Matrix: (Soil/water) SOIL 

Sample wt/vol: 5.0 (9/mL) 

Level: (low/ned) LOW 




DATA SHEET 

000012 


CONFOUNDS 1 I 

1 B07QDB I 


_ Lab Pilo ID: 21223R08 




.ONCENTRATION UNITS: 

Number TICS found: _ 0 (u9/L or uq/K9) UG/KG 


1 1 I I 1 

CAS NUMBER 1 COMPOUND NAME I RT I EST. CONC. I Q 

1 I I I I 

FORM I VOA-TIC 3/90

Lab Name: 

1A 


Lab Coda: TMALA Casa No.: 12074_ 



Leval: ( low/med) I8N 





I 


74-83-9 --------- Bromomethane 


75-00-3---------Chloroethane 

75-09-2---------Methylene Chloride_ 

67-64-1---------Acetone 



75-34-3---------1,1-Dichloroethana^— 

540-59-0 -------- 1,2-Dichloroethene ( 

67-66-3---------Chloroform 

107-06-2 -------- 1,2-Dichloroethane_ 

78 -93-3 --------- 2-Butanone 

71-55-6 --------- 1,1,1-Trichloroethan 


i 75-27-4 --------- Bromodichloromethans 

78-87-5 --------- 1,2-Dichloropropana_ 

110061-01-5 ------ cis-1.3-DichloroPLOA 

124-48-1 -------- Dibr 

79-00-5---------1,1, 

10061-02-6------trans-1, 

108- 

108-88- 

1,2, 

100-41-4 -------- Ethylbenzene 

1330-20-7 

Contract: WC 

SAS No.: NA 

000013 


B07QD9 

SDG No.: NA 


Q__ Lab File ID: 21223R09 

FORM I VOA 


Data Analyzed: 12/23/92 


Soil Aliquot Volume: (uQ 



10 

10 

10 

10 

10 

12 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

30 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 t 

3/90


1E 



Lab Code: rya_ Case No.: 12074 


Sample wt/vol: s.0 (g/mL) S^ 

Level: ( low/mod) LQK- 




000014 


B07QD9 

Contract: vuu I 

SAS No.: NA SDG No.: NL-- 







Number TICS found: _Q (ug/L or ug/Kg) UG/KG 

soil Aliquot Volume: (uL) 

I I I I I 

CAS NUMBER I COMPOUND NAME I RT I EST. CONC. I Q 

Iammsssasasss I amâssaaaasa^âaâm=: I sssâa I â.ass:::::o I mss 

I I I 1 I 


3/90

2A 


000015 


I I 

I B07QF0 1 


Lab Code: TMALi ► Case No.: 12094 SAS No.: NA SDG No.: N_ 

Matrix: (soil/water) ^Z,QIL Lab Sample ID: A212074-04A 

Sample wt/vol: 5:0 (g/mL) G_ 


= Moisture: not dec. 2 



Lab Pilo ID: 21223810 

Data Received:- 12/21/92 





CAS NO. COMPOUND (ug/L or ug/Kg) VG/KG Q 

74-87-3 --------- Chloromethane i 

I 

I 

10 III 



75-00-3 ----- ----Chloroethane I 10 III 

75-09-2---------Methylene Chloride I 10 III 

67-64-1---------Acetone I 13 IB 

75-15-0---------Carbon Disulfide 1 10 IV 

75-35-4 --------- 1,1-Dichloroethene I 10 IV 

75-34-3 --------- l,l-Dichloroethane I 10 IV 

540-59-0 -------- 1,2-Dichloroethene (total) _I 10 III 


107-06-2 -------- 1,2-Dichloroethane 1 10 III 

78-93-3 --------- 2-BUtanone I 10 III 

71-55-6 --------- 1,1,1-Trichloroethans 1 10 III 

56-23-5---------Carbon Tetrachloride I 10 III 

75-27- 4 --------- Bromodichloromethane 1 10 IU 

78-87-5 ----- ----1,2-Dichloropropans I 10 III 

10061-01-5------cis-1,3-Dichloropropens 1 10 IV 

79-01-6 --------- Trichloroethene I 10 III 

124-48-1 -------- Dibromochloromethane I 10 III 

79-00-5 --------- 1,1,2-Trichloroethane I 10 IV 

71-43-2---------Benzene i 10 III 

10061-02-6 ------ trans-1,3-D chloropropens I 10 III 

75-25-2 --------- Bromoform i 10 IV 

108-10-1 -------- 4-Methyl-2-Pentanone I 10 IV 

591-78-6 -------- 2-Hexanone I 10 III 

127-18-4 -------- Tetrachloroethene I 10 IV 

79-34-5 ------ ---1,1,2,2-Tetrachloroethane I 10 IV 

108-88-3--------Toluene I 10 III 

108-90-7 -------- Chlorobenzene 1 10 IU 

100-41- 4 -------- Ethylbenzens I 10 III 

100-42-5--------Styrene I 10 IU 

1330-20-7 ------(total) I 10 III 

FORM I VOA 3/90

(Q^VIG 

IN EPA SAMPLE RD. 



S07QF0 


Lab Cod*: THALA Case No.: 12074 SAS No.: NA SDG No.: NA 

_ 



Sample wt/vol: 5.0 (g/mL) G_ Lab File ID: 21223RIO 

Level: (low/sod) I&#— Date Received: 12/21/92 

t Moisture: not doe. _2 Date Analyzed: 12/23192 

GC Column: PACK ID: 2.00 (ms) Dilution Factor: 1.0 




CAS NUMBER COMPOUND NAME RT i EST. CONC. 

I I I 

FORM I VOA-TIC 3/90

000017 

ID EPA amts NO. 


Lab Name: Told/ARLI Contract: NHC 

B07QB5 

Lab Code. TMALA Case No.: 12074 SAS No.: NA SDG No.: NA 

Matrix: (soil/water) 60IL Lab Sample ID: A212074-05B 

Sample wt/vol: 30.1 (g/NL) G 


! Moisture: _9 decanted: (Y/N) N 






Date Receivedr 12/1/92 






108-95-2--------Phenol 360 IU 

111-44-4 -------- bis(2-Chloroethyl)Ether 360 III 

360 IU 

541-73-1 -------- 1,3-Dichlorobenzene 360 III 

106-46-7 -------- 1,4-Dichlorobenzene 360 IU 

95-50-1 --------- 1,2-Dichlorobenzene 360 III 

95-48-7 --------- 2-Methylphanol 360 IU 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_ 360 IU 

106-44-5 -------- 4-Methylphanol 360 IU 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne_ 360 III 

67-72-1 --------- Hexachloroethans 360 III 

360 III 

78-59-1 --------- Isophorone 360 III 

88-75-5 ---------- 2-Nitrophenol 360 III 

105-67-9 -------- 2,4-Dimethylphenol 360 III 

111-91-1 -------- bis(2-Chloroethoxy)Methane 360 III 

120-83-2 -------- 2,4-Dichlorophenol 360 IU 

120-82-1 -------- 1,2,4-Trichlorobenzene 360 III 

91-20-3---------Naphthalene 360 III 

106-47-8 -------- 4-Chloroanil ne 360 III 

87-68-3 --------- Hexachlorobutad ena 360 III 

59-50-7 --------- 4-Chloro-3-Methylphanol 360 III 

91-57-6 --------- 2-Methylnaphthalene 360 III 

77-47-4---------Hexachlorocyclopentad ene 360 III 

88-06-2 --------- 2,4,6-Trichlorophenol 360 III 

95-95-4 --------- 2,4,5-Trichlorophenol 880 III 

91-58-7 --------- 2-Chloronaphthalene 360 III 

88-74-4 --------- 2-Nitroaniline 880 III 

360 III 

360 III 

99-09-2---------3-N 880 IU 

83-32-9---------Ace 360 III 

51-28-5---------2,4 880 III 

FORM I SV-1 3/90

1C 



100-02-7--------4-Ni 

121-14-2 -------- 2,4-Dinitrotolue 

606-20-2 -------- 2,6-Dinitrotolue 


000018 

EPA SANPLE NO. 

I B07QB5 



Sample wt/vol: 30.1 (9/mL) Sz- Lab File ID: 30125507 

Level: (low/med) Date Received:- 12121192 

t Moisture: _9 decanted: (Y/N) N 



GPC Cleanup: (YIN) Y— 


pH: 8.9 

86-73-7 --------- Fluorene 

100-01-6 -------- 4-Nitroan 1 ne 

534-52-1 -------- 4,6-Dinitro-2-methylphenol_ 

86-30-6 --------- N-Nitrosodiphenylamine (1)_ 




85-01-8 --------- Phenanthrene 

120-12-7 -------- Anthracene 

86-74-8 --------- Carbazole 

84-74-2 --------- Di-n-Butylphthalate 

206-44-0 -------- Fluoranthene 


91-94-1 --------- 3,3'-Dichlorobenzidine 


117-81-7 -------- bis(2-Ethylhexyl)Phthalate 

218-01-9 -------- Chrysene 

117-84-0 -------- Di-n-Octyl Phthalate 



50-32-8 --------- Benzo(a)Pyrene 

193-39-5 -------- Indeno(1,2,3-cd)PyrenO 

53-70-3 --------- Dibenz(a,h)Anthracens 






(uq/L or uq/Rq) yG/RG Q 

880 

360 

360 

360 

360 

360 

360 

880 

880 

360 

360 

360 

880 

360 

360 

360 

130 I W 

360 IU 

360 IU` 

360 IU 

360 IU 

360 IU 

360 IV 

360 IU 

360 IU 

360 IU 

360 IU 

360 (U 

360 (U 

360 IU 

360 IU 

I_ 

FORM I SV-2 3/90

0000.19 

1! EPA SAMPL8 No. 

SEMXVOLATILE ORGANICS ANALYSIS DATA SHEET 


I B07QBS I 

Lab Name: TMA/ARLI Contract: WKC I I 

Lab Code: TNALA Case No.: 12074 SAS No.: KA SDO No.: NA_ 

matrix: ( soil/water) Lab Sample ID: A212074-05B 

Sample wt/vol: 30.1 (g/NL) S_ Lab File ID: 30125507 

Level: ( low/med) Loy Date Received:-" 12/21/92 

t moisture: ^9 decanted: (Y/N) N Date Extracted: 12/23192 



Injection Volume: _ 2.0 (uL) Dilution Factor: 1.0 

GPC Cleanup: (YIN) Y PH: 8.9 


Number TICS found: _-} (ug/L or ug/Xg) UG/KG 

I 2. 

i 3. 

1 

CAS NUMBER 

4. 

s. 

6. 

7. 

i 8. 

9. 

1 10. 

i 11. 

I 

COMPOUND NAM 



IUNXNOWN HYDROCARBON 




IUNKNOWN HYDROCARBON 

1PROPANOIC ACID ISOMER 

IUNKNOWN CARBOXYLIC ACID ESTE 

(UNKNOWN ALKANE 

(UNKNOWN ALRANE 

RT I EST. CONC. 1 Q 

5.25 I 470 IX I 

5.85 i 1900 1 I 

5.90 I 580 IJ I 

1 6.00 ( 1600 1w I 

6.55 1 98000 1 w I 

7.73 I 1900 1 I 

9.05 I 260 I W 

18.35 i 220 IJ 

21.42 ( 110 Ia7 

28.37 I 73 IJ 

30.48 I 

I 

150 1J I 

.1-1 

FORM I SV-TIC 3/90

000020 

is EPA SAWLE NO. 


I B07QB6 1 

Lab Nana: =/ARLI Contract: WHC I I 

Lab Code: TKWA Case No.: 12074 SAS No.: NA SDG No.: X& 

_ 



Sample wt/vol: 31.0 (g/AL) G Lab File ID: 30125so8 

Level: (low/mad) jam_ Data Received: 12121/92 

t Moisture: _ 3 decanted: (Y/N) N Data Extracted: 12/23/92 



GPC Cleanup: (Y/N) Y_ pH: 8.7 


CAS NO. COMPOUND (ug/L or ug/Rg) UGZKG Q 

1 108-95-2--------Phenol I 330 I II I 

1 111-44-4 -------- bis(2-Chloroethyl)Ether I 330 I U I 

195-57-8 --------- 2-Chlorophenol I 330 III I 

1 541-73-1 -------- 1,3-Dichlorobenzene i 330 I U I 

1 106-46-7 -------- 1,4-Dichlorobenzens I 330 I V I 

195-50-1 --------- 1,2-Dichlorobenzene I 330 IV I 

195-48-7 --------- 2-Methylphencl I 330 III I 

1 108-60- 1 -------- 2,2'-oxybis(1-Chloropropane)_I 330 III I 

106-44-5 -------- 4-Methylphenol I 330 III I 

i 621- 64-7 -------- N-Nitroso-Di-n-Propylam e_I 330 IU 

167-72-1 --------- Hexachloroethane I 330 IV I 

98-95-3---------Nitrobenzene I 330 III I 

178-59-1 ------- --Isophorons ( 330 I UI 

188-75-5 ---------2-Nitrophenol I 330 III I 

1 105-67- 9 -------- 2,4-Dimethylphenol ( 330 I U I 

1 111-91-1 -------- bis(2-Chlorosthoxy)Methane I 330 III I 

1 120-83-2 -------- 2,4-Dichlorophanol 1 330 I VI 

1 120-82-1 -------- 1,2,4-Trichlorobanzene I 330 I UI 

91-20-3---------Naphthalene I 330 1 i 

1 106-47- 8 -------- 4-Chloroanil ne I 330 III I 

187-68-3 --------- Hexachlorobutad one I 330 III I 

159-50-7 --------- 4-Chloro-3-Methylphenol I 330 III I 

191-57-6 --------- 2-Methylnaphthalene ( 330 III I 

77-47-4 --------- Hexachlorocyclopentad ene I 330 I II I 

188-06-2 --------- 2,4,6 -Trichlorophanol I 330 III I 

195-95- 4 --------- 2,4,5-Trichlorophanol I 800 III I 

191-58-7 -------- 2-Chloronaphthalene I 330 III I 

188-74-4 --------- 2-Mitroaniline i 800 I VI 

1131-11-3 -------- Dimethylphthalate I 330 IV I 

1208-96- 8 -------- Acenaphthylene I 330 III I 

199-09-2 --------- 3-Nitroaniline I 800 III I 

183-32-9 --------- Acenaphthene 1 330 III I 

i 51-28-5 --------- 2,4-Dinitrophenol 

I 

800 III I 

I 

I 

I I

1C 


00n022 

EPA SAMPLE No. 

I B07QBG 

Lab Name: TMA/ARLI Contract: WHC i 

Lab Code: TMALA Casa No.: 12074 SAS No.: NA SDG No.: Imo__ 

Matrix: (soil/water) 492E Lab Sample ID: A212074-06B 

Sample wt/vol: 31.0 (g/RL) Q_. 

Level: (low/Red) LOW 

t Moisture: _ 3 decanted: (Y/N) W 



Lab File ID: 

30125508 

Data Racaived:- 12/21/92 

Data Extracted: 12./23/92 



GPC Cleanup: (YIN) X-- pH: 8.7 


CAS NO. COMPOUND (ug/L or uq/Rq) UG/RG Q 

100-02-7 -------- 4-Nitrophenol I 800 III 

132-64-9 -------- Dibenzoturan I 330 III 

121-14-2 -------- 2,4-Dinitrotoluene i 330 IV 

606-20-2 -------- 2,6-Dinitrotoluene I 330 IU 

84-66-2 --------- Diethylphthalate ( 330 IU 

7005-72-3 ------- 4-Chlorophenyl-phenylether_I 330 IU 

86-73-7 --------- Fluorene ( 330 IU 

100-01- 6 -------- 4-Nitroan 1 e I 800 JU 

534-52-1 -------- 4,6-Dinitro-2-mothylphenol I 800 III 

86-30-6 --------- N-Nitrosodiphenylamine (1)_I 330 III 

101-55-3 -------- 4-Bromophenyl-phenylether 1 330 IU 

118-74-1 -------- Hexachlorobenzene I 330 IU 

87-86-5 --------- Pentachlorophenol I 800 IU 

85-01-8 --------- Phenanthrene I 330 IU 

120-12-7 -------- Anthracene I 330 IU 

86-74-8 --------- Carbazole ( 330 IV 

84-74-2 --------- Di-n-BUtylphthalato I 150 1 

206-44-0 -------- Fluoranthene I 330 III 

129-00-0 -------- Pyrene I 330 IV 

85-68-7---------BUtyl.benzylphthalata I 330 III 

91-94- 1 --------- 3,3'-Dichlorobenzidine I 330 IU 

56-55-3 --------- Benzo(a)Anthracene I 330 III 

117-81-7 -------- bis(2-Ethylhexyl)Phthalata_I 55 

218-01-9 ---- ----Chrysene 

117-84-0--------Di-n-OCtyl Phthalate 


207-08-9 -------- Benzc(k)Fluoranthene 

50-32-8 --------- Benzo(a)Pyrene 

193-39-5 -------- Indeno(1,2,3-cd)Pyrsna 


191-24-2 -------- Benzo(g,h,i)Perylens 

I 

I 

I 

I 

I 

330 

330 

330 

330 

330 

330 

330 

330 

IJ_ 

IU 

IU 

IV 

IV 

III 

IU 

IV 

III 

I - rannnt ha aannrmtnA 4'"MM ninhwnvlainina 

FORM I SV-2 

1.0 

3/90

Lab Name: 

IF 



Contract: WHC 

0000)2 


( I 

I B070BG I 

I I 

Lab Code: THALA Case No.: 12074 SAS No.: NA SDG No.: NA—_ 


Lab Sample ID: A2 12074-06B 



S^ Lab Pilo ID: 30125508 


t Moisture: _3 decanted: (YIN) N Date Extracted: 12 /23/92 





Number TICS found: U (ug/L or uq/Kg) UG/KG 

i 

1 

1 

1 

i 

I 

I 

I 

CAS NUMBER 

1. 

2. 

3. 

4. 

5. 

6. 

7. 

8. 

9. 

1 10. 

1 11. 

12. 

COMPOUND NAME I RT I EST. CONC. I Q I 

UNKNOWN HYDROCARBON 5.85 830 IJ I 

INNKNOWN HYDROCARBON I 5.90 I 800 I J I 

(UNKNOWN HYDROCARBON 1 6.02 1 1500 iW I 

(UNKNOWN HYDROCARBON 1 6.57 1 84000 I BJ I 

(UNKNOWN HYDROCARBON i 7.15 I 130 I BT I 

(UNKNOWN HYDROCARBON I 7.33 I 67 IJ I 

1UNKNOWN KETONE 1 7.73 1 1800 1 B I 

(UNKNOWN HYDROCARBON I 9.05 1 270 1 W I 

(UNKNOWN CARBOXYLIC ACID ESTEI 21.42 1 100 1 B I 

(UNKNOWN ALKANE 1 26.73 ( 130 IJ I 

(UNKNOWN ALKANE 1 28.38 1 100 IJ I 

(UNKNOWN ALKANE 1 30.48 1 130 IX I 

1 

FORM I SV-TIC 

1-1 

1-1 

3/90

13 



GPC Cleanup: (Y/N) y PH: _2:.2 


CAS NO. COMPOUND (uq/L or uq/Kq) UG/KG E 

108-95-2--------Phenol ( 350 

111-44-4 -------- bis(2-Chloroethyl)Ether ( 350 

95-57-8 --------- 2-Chlorophenol ( 350 

541-73-1 -------- 1,3-Dichlorobenzens I 350 

106-46-7 -------- 1,4-Dichlorobenzene ( 350 

95-50-1 --------- 1,2-Dichlorobenzene ( 350 

95-48-7 --------- 2-Methylphenol ( 350 

108-60-1 -------- 2,2'-oxybis ( 1-Chloropropane)_( 350 

106-44 -5 -------- 4-Methylphenol ( 350 

621-64 -7 -------- N-Nitroso-Di-n-Propylam e_I 350 

67-72-1 --------- Hexachloroethane ( 350 

98-95-3---------Nitrobenzene ( 350 

78-59-1 --------- Isophorone ( 350 

88-75-5 --------- 2-Nitrophenol ( 350 

105-67-9 -------- 2,4-Dimethylphenol ( 350 

111-91-1 -------- bis ( 2-Chloroethoxy ) Methane_I 350 

120-83-2 -------- 2,4 -Dichlorophenol ( 350 

120-82-1 -------- 1,2,4-Trichlorobenzene ( 350 

91-20 -3---------Naphthalene ( 350 

106-47 -8 -------- 4-Chlorcanil ne ( 350 

87-68-3 --------- Hexachlorobutad i -u ( 350 

59-50-7 --------- 4-Chloro-3 -Methylphenol I 350 

91-57 -6 --------- 2-Methylnaphthalene I 350 

77-47-4---------Hexachlorocyclopentad Man I 350 


95-95-4 --------- 2,4 , 5-Trichlorophenol I 840 

91-58 -7 --------- 2-Chloronaphthalene 350 

I 

88-74-4 --------- 2-Nitroaniline 840 

I 

131-11-3 -------- Dimethyiphthalate I 350 

208-96-8 -------- Acenaphthylene ( 350 

99-09-2 --------- 3-Nitroaniline I 840 

83-32-9 ------ ---ACenaphthene ( 350 

51-28-5 ---------2,4-Dinitrophenol ( 840 

FORM I SV-1 

I 

000023 


I H07QD7 

Lab Code: ZMLL— Case No.: 12074 SAS No.: NA SDG No.: NA 


Sample wt/vol: 30.4 (9/]LL) 0_ 

Level: (low/med) I&N-- 

4 Moisture: 6 decanted: (Y/N) 1^ 






Date Extracted: 12123/92 



III I 

IL i 

III 

I Q I 

I M I 

III i 

III I 

III I 

III I 

III I 

I II I 

III I 

1u I 

III I 

IQ I 

Iv I 

III I 

IQ I 

III I 

I U I 

I II I 

III I 

I II i 

IU i 

I u i 

I II I 

I II 

I U 

III 

III 1 

I II I 

3/90 

I 

I 

{

0000 2 4 

1C EPA SAMPLE NO. 


I I 

I B07QD7 I 


Lab Code: TMALa _ Case No.: 12074 


Sample wt/vol: 30.4 (q/mL) rg_ 

I I 

SAS No.: NA SDG No.: IA 

Lab Sample ID: A212074-OID 


Laval: (low/mad) Date Received: 12/21/92 

Moisture: _ 6 decanted: (Y/N) N Date Extracted: 12/23/92 

Concentrated Extract Volume: 500.0 (UL) Data Analyzed: 01/25/93 


GPC Cleanup: (YIN) Y pH. 9.3 


CAS NO. COMPOUND (ug/L or ug/Rg) UQ/KG Q 

100-02-7 -------- 4-Nitrophenol 1 840 1 U 

I 

I 

1 

132-64-9 -------- Dibenzofuran i 350 IU 1 

121-14-2 -------- 2,4-Dinitrotoluena I 350 I U 1 

606-20-2 -------- 2,6-Dinitrotoluene 1 350 III 1 

84-66-2 --------- Diethylphthalate 1 350 III 1 

7005-72-3 ------- 4-Chlorophanyi-phenylether 1 350 IU 1 

86-73-7 --------- Fluorene I 350 I U 1 

100-01-6 -------- 4-Nitroan 1 ne i 840 III 1 

534-52- 1 -------- 4,6-Dinitrc- 2-methylphenol 1 840 IU 1 

86-30-6 --------- N-Nitroeodiphenylamine (1) =1 350 IU 1 

101-55-3 -------- 4-Bromophenyl-phanylether 1 350 III 1 

118-74-1 -------- Hexachlorobenzene 1 350 IU 1 


85-01-8 --------- Phenanthrene I 350 I U I 

120-12-7 -------- Anthracene I 350 IU 1 

86-74-8 --------- Carbazole 1 350 IV 1 

84-74-2 --------- Di-n-Butylphthalate 1 130 1W 1 

206-44-0 ----- ---Fluoranthene 1 350 IU 1 

129-00-0 ------- -Pyrene I 350 I U 1 

85-68-7 -------- -Butylbenzylphthalate 1 350 III 1 

91-94-1 --------- 3,3'-Dichlorobanzidine I 350 IU 1 

56-55-3 --------- Benzo(a)Anthracene 1 350 I U 1 

117-81-7 -------- bis(2-Ethylhexyl)Phthalate_I 350 I U 1 

218-01-9 -------- Chrysone 1 350 1U 1 

117-84-0 -------- Di-n-Octyl Phthalate I 350 III 1 

205-99-2 -------- Benzo(b)Fluoranthene I 350 1V 1 

207-08-9 -------- Benzo(k)Fluoranthene I 350 IU 1 

50-32-8 --------- Benzo(a)Pyrene 1 350 1 U 1 

193-39-5 -------- Indeno(1,2,3-cd)Pyrene 1 350 IU 1 

53-70-3 --------- Dibenz(a,h)Anthracene i 350 III 1 

191-24-2 -------- Benzo(q,h,i)Perylene 1 350 IU I 

;1) - Cannot be separated from Diphenylamine 

I 

FORM I SV-2 3/90

UU0025 

IF sPA SAMPLE NO. 

SEMIVOLATILE ORGANICS ANALYSIS DATA SKEET 

TENTATIVELY IDENTIFIED COM 20UNDS I 

I B07QD7 i 


Lab Code: MJ&JA_ Case No.: 12074 SAS No.: NA SDG No.: ga_ 

Matrix: ( soil/eater) SOIL Lab Sample ID: A212074-01D 

Sample wt/vol: 30.4 (VRL) G File ID: 30125S03 


i Moisture: _6 decanted: (YIN) N 

Date Extracted: ]^ 23/92 



GPC Cleanup: (YIN) Y p8: 9.3 



(uq/L or uq/Xq) UG/KG 

I i I I I I 

I CAS NUMBER I COMPOUND NAME ( RT 1 EST. CONC. I Q 

1 ^^ I =° I ^ I :I-1 

I 1. 1 UNKNOWN HYDROCARBON 1 5.80 ( 1000 1 I 

i 2. ( UNKNOWN HYDROCARBON 1 5.87 1 980 I J I 

I 3. 1 UNKNOWN HYDROCARBON 1 6.00 1 1300 1 BJ I 

I 4. (UNKNOWN HYDROCARBON 1 6.53 1 97000 1 BJ I 

I 5. 1 UNKNOWN KETONE 1 7.72 1 2000 1 I 

I 6. (UNKNOWN HYDROCARBON I 9.03 I 350 IBJ I 

I 7. IPROPANOIC ACID ISOMER I 18.33 ( 210 IJ I 

8. 1 UNKNOWN CARBOXYLIC ACID ESTEI 21.37 1 100 1 BJ I 

9. JHEXANEDIOIC ACID ISOMER 1 25.88 1 140 iJ 

FORM I SV-TIC 3/90

18 


UUUVZb 

EPA SAMPLE MO. 

I 1 

I B07QM I 

Lab Name: TMA/ARLI Contract: WHC __ I I 

Lab Code: JKAJA Case No.: 12074 SAS No.: NA SDG No.: I_ 

Matrix: (soil/vater) ,ROIL 



t Moisture: _ 4 decanted: (Y/N) N_ 


Injection Volume: 2,O(UL) 




Date Extracted:,/23/92 





CAS NO. COMPOUND (uq/L or uq/Rq) UG/RG 0 

108-95-2--------Phenol I 330 1V 

111-44-4 -------- bis(2-Chloroethyl)Ether I 330 IU 

95-57-8 --------- 2-Chlorophenol I 330 IV 

541-73-1 -------- 1,3-Dichlorobenzene 1 330 IV 


95-50-1 --------- 1,2-Dichlorobenzene I 330 III 

95-48-7 --------- 2-Methylphenol I 330 IV 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_I 330 IU 

106-44-5 -------- 4-Methylphenol 1 330 IV 

621-64-7 -------- N-Nitroso-Di-n-Propylam e_I 330 III 

67-72-1 --------- Hexachloroethane 1 330 III 

98-95-3---------Nitrobenzene 1 330 IU 

78-59-1 --------- Isophorone I 330 III 

88-75-5 --------- 2-Nitrophenol I 330 III 

105-67-9 -------- 2,4-Dimethylphenol I 330 III 

111-91-1 -------- bis(2-Chloroethoxy)Methane I 330 III 

120-83-2 -------- 2,4-Dichlorophenol ii 330 III 

120-82-1 -------- 1,2,4-Trichlorobenzane I 330 IU 

91-20-3---------Naphthalene I 330 III 

106-47-8 -------- 4-Chlorcanil e I 330 III 

87-68-3 --------- Hexachlorobutad ene 1 330 III 

59-50-7 --------- 4-Chloro-3-Hethylphenol I 330 III IU 


77-47- 4 --------- Nexachlorocyclopentadio e I 330 IU 

88-06-2 ---------- 2,4,6-Trichlorophenol I 330 III 

95-95- 4 --------- 2,4,5-Trichlorophenol I 810 III 

91-58-7 --------- 2-Chloronaphthalene I 330 III 

88-74- 4 --------- 2-Nitroaniline I 810 III 

131-11-3 -------- Dimethylphthalate I 330 III 

208-96-8 -------- Acenaphthylene I 330 III 

99-09-2 --------- 3-Nitroaniline i 810 III 

83-32-9 --------- ACenaphthene I 330 III 

51-28-5 --------- 2,4-Dinitrophenol I 810 III 

FORM I SV-1

1C 


000027 

EPA SAJUTA NO. 

1 I 

1 B07QDS i 

Lab Name: TMA/ARLI contract: NHC I 1 

Lab Code: TMALA Case No.: 12074 SAS No.: NA SDG No.: )^^ 

Matrix: ( soil/water) SOIL ye Lab Sample ID: A2 12074-02B 

Sample wt/vol: 30.8 (9/ RL) Sz_ Lab File ID: 30122521 

Level: ( low/med) Date Received: 12/21/92 

t Moisture: _ 4 decanted: (Y/N) N_ Date Extracted: x,/23/92 


Injection volume: 2.0(uL) Dilution Factor: 1.0 

GPC Cleanup: ( Y/N) Y pH: 8.2 


CAS NO. COMPOUND (uq/L or ug/Rg) UG/1CG Q 

I 

100-02-7 -------- 4-Nitrophenol J 

810 III 1 

132-64 -9 -------- Dibenzofuran i 330 JU 1 

121-14-2 -------- 2,4-Dinitrotoluene J 330 JU 1 

606-20-2 -------- 2 , 6-Dinitrotoluene J 330 JU 1 

84-66-2 --------- Diethylphthalate J 330 JU 1 

7005-72-3 ------- 4-Chlorophenyl-phenylether 1 330 JU 1 

86-73-7 --------- Fluorene 330 JU 1 

1 

100-01-6 -------- 4 -Nitroan 1 ne i 810 JU 1 

534-52 -1 -------- 4,6-Dinitro -2-methylphenol I 810 I V 1 

86-30-6 --------- N-Nitrosodiphenylamine ( 1 )_i 330 1U 1 

101-55-3 -------- 4-Bromophenyl -phenylether I 330 JU 1 

118-74-1 -------- Hexachlorobenzene J 330 J U 1 

87-86-5 --------- Pentachlorophenol I 810 1U 1 

85-01-8 --------- Phenanthrene J 330 J U 1 

120-12-7 -------- Anthracene ( 330 1U I 

86-74-8 --------- Carbazole J 330 III 1 

84-74-2 --------- Di-n-BUtylphtha ate J 130 1 W 1 

206-44 -0 -------- Fluoranthene J 330 JU 1 

129-00-0 -------- Pyrene 1 330 J U 1 

85-68-7 --------- BUtylbenzylphthalate J 330 JU I 

91-94 -1 --------- 3,3'-Dichlorobenzidine 330 JU J 

J 

56-55 -3 --------- Benzo (a)Anthracens J 330 JU 1 

117-81-7 -------- bis ( 2-Ethylhexyl ) Phthalate_ J 330 JU I 

218-01-9 -------- Chrysene 330 JU 1 

J 

117-84 -0 -------- Di-n-Octyl Phthalate 330 1U J 1 

205-99-2 -------- Benzo (b)Fluoranthene J 330 1 U 1 

207-08-9 -------- Benzo (k)Fluoranthene J 330 JU 1 

50-32-8 --------- Benzo ( a)Pyrene J 330 JU 1 

193-39-5 -------- Indeno ( 1,2,3-cd)Pyrens J 330 JU 1 

53-70 -3 --------- Dibenz(a,h)Anthracens ( 330 JU 1 

191-24-2 -------- Benzo ( g,h,i)Perylene J 330 JU I 

(1) - Cannot be separated from Diphenylamins 


I 

I

I 1. 

I 2• 

1 3. 

1 

1 

1 

I 

1 

CAS NUMBER 

4. 

5. 

6. 

7. 

8. 

I 9. 

1 10. 

1 11. 

1 12. 

1 13. 

000028 

iF 


SEXIVOLATILE ORGANICS ANALYSIS DATA SHEET 


I B07QDB I 

Lab Name: TMA/ARLI Contract: WHC 1 1 

Lab Code: THALA Case No.: 12074 SAS No.: NA SDG No.: Mme_ 

Matrix: ( soil/water) $AIL Lab Sample ID: A212074-02B 

Sample wt/vol: 30.8 (q/RL) G_ Lab File ID: 30122921 

Level: ( low/mod) UN Date Received: 12/21/92 1/92 

t Moisture: 4 decanted: (YIN) N Date Extracted: 12/23/92 3/92 

Concentrated Extract Volume: 500.0 (UL) Date Analyzed: 0 1/23/93 


GPC Cleanup: ( Y/N) ,g _ pH: 9.2 


Number TICS found: (ug/L or uq/Kq) UG/KG 

COMPOUND NAME I RT 1 

via aâaaaaa I^ I 

UNKNOWN HYDROCARBON i 5.25 I 

UNKNOWN HYDROCARBON 1 5.85 

UNKNOWN ALKANE ( 5.90 I 

UNKNOWN HYDROCARBON i 6.02 1 

UNKNOWN HYDROCARBON 1 6.57 1 

SUBSTITUTED BENZENE 1 6.73 1 

UNKNOWN HYDROCARBON 1 7.15 

/UNKNOWN HYDROCARBON i 7.32 1 

I I 

EST. CONC. 1 4 I 

---^° 1---'° 1 

850 I J I 

1.000 1 W 1 

780 i1,T 1 

1500 1 BJ 

1 

100000 1BJ 1 

140 11 1 

140 11 

100 11 I 

/UNKNOWN KETONE i 7.73 1 

1800 1 I 

UNKNOWN HYDROCARBON 1 7.83 68 IJ 1 

1 

/UNKNOWN HYDROCARBON 9.03 

140 1 1 

1 1 

1PROPANOIC ACID ISOMER 1 18.35 

200 IJ 1 I 

UUNKNOWN CARBOXYLIC ACID ESTE1 21.40 1 

100 1 I 

1 

1-1 

I I 

FORM I SV-TIC 

3/90

Matrix: ( soil/water) SOIL Lab Sample ID: A212074-038 

Sample wt/vol: 30.0 (VAL ) Sc_ 




t Moisture: _3 

000049 

is sPA sAXPTX NO. 


I 1 

1 s07QD9 i 

Lab Name: TMA/ABET Contract: WHC i I 

Lab Code: M%LA Case No.: 12074 SAS No.: NA _ SDG No.: Imo_ 

decanted: (Y/N) jam_ 



Data Extracted: ^,/23/92 

Data Analyzed: 01/2 3/93 


GPC Cleanup: (Y/N) Y_ PH: 9.5 


CAS NO. COMPOUND (uq/L or uq/Rq) UG/RG Q 

108-95-2--------Phenol 1 

I 

340 III 

111-44-4 -------- bis(2-Chloroethyl ) Ether I 340 III 1 

95-57 -8 --------- 2-Chlorophenol I 340 III 1 

541-73-1 -------- 1,3-Dichlorobanzene I 340 IV 1 

106-46-7 -------- 1,4-Dichlorobenzena I 340 IU 1 

95-50-1 --------- 1,2-Dichlorobenzens 1 340 III 1 

95-48-7 --------- 2-Nsthylphonol I 340 I V 1 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_I 340 IV 1 

106-44-5 ------ --4-Methylphanol 1 340 IV I 

621 - 64 -7 ------ --N-Nitroso-Di-n-Propylam ne_I 340 1 U 1 

67-72-1 --------- Hexachloroethane I 340 IV 1 

98-95-3---------Nitrobenzene 1 340 IV 1 

78-59-1 --------- Isophorone I 340 IV 1 

88-75-5 --------- 2-Nitrophenol I 340 IV 

105-67-9 -------- 2,4-Dimethylphenol i 340 IV 1 

111-91-1 -------- bis(2-Chloroothoxy ) Mathane_ I 340 III 1 

120-83-2 -------- 2,4-Dichlorophenol 1 340 IV 1 

120-82-1 ----- -- -1,2,4-Trichlorobenzans I 340 IV 1 

91-20-3---------Naphthalene I 340 IV 1 

106-47-8 -------- 4-Chloroani e I 340 IU' 1 

87-68-3 --------- Hexachlorobutad ens I 340 IV I 

59-50-7 --------- 4-Chloro-3-Mathylphenol I 340 I U 1 

91-57-6 --------- 2-Nothylnaphthalsns j 340 IV I 

77-47-4 --------- Hexachlorocyclopentad —ne e 

340 IV I 

88-06-2 --------- 2,4,6-Trichlorophenol I 340 IV I 

95-95-4 --------- 2,4,5-Trichlorophenol I 820 III 1 

91-58-7 ------- --2-Chloronaphthalens I 340 IU 1 

88-74 -4 ------- --2-Nitroaniline j 820 IV _ 

1 


I 340 IV 1 

208-96-8 -------- Acenaphthylene I 340 IU 1 

99-09-2 --------- 3-Nitroaniline I 820 IV 

83-32-9 --------- Acenaphthene I 340 IV 1 

51-28 -5 --------- 2,4-Dinitrophenol I 820 I U I 

FORM I SV-1 

I I 3/90 

1 

1 

1

Lab Naas: TMA/ARLI 

t1O iNrl0 



Lab Cods: TMALA Cass No.: 12074 



Level: (low/med) SO_ 




GPC Cleanup: (Y/N) Y_ 


pH: 9.5 

B07QD9 

Contract: W C ) 









(uq/L or uq/Rg) UG/RG Q 

100-02-7 -------- 4-Nitrophenol 820 JU 

1 

132-64-9 -------- Dibenzoluran 340 J U 

121-14 -2 -------- 2,4-Dinitrotoluene 340 JU 

606-20 -2 -------- 2,6-Dinitrotoluens 340 JU 

84-66-2 --------- Diethylphthalate 340 JU 

7005-72-3 ------- 4-Chlorophenyl -phanylether 340 JU 

86-73-7 --------- Fluoreno 340 JU 

100-01-6 -------- 4-Nitroan 1 ne 820 JU 

534-52-1 -------- 4,6-Dinitro-2-mothylphanol 820 JU 

86-30-6 --------- N-Nitrosodiphenylamine (1)_ 340 1U 

I 

101-55-3 -------- 4-Bromophanyl-phenylether 1 340 JU 

118-74-1 -------- Hexachlorobenzene 1 340 JU 

87-86-5 --------- Pentachlorophenol ( 820 JU 

85-01-8 --------- Phenanthrene 1 340 JU 

120-12 -7 -------- Anthracsne 1 340 JU 

86-74-8 --------- Carbazols 1 340 JU 

84-74-2 --------- Di-n -BUtylphthalate l 110 1 W 

206-44 -0 -------- Flucranthene 340 IV 

129-00-0 -------- Pyrene 340 (U 

85-68-7 -------- -BUtylbenzylphthalata 340 I V 

91-94 -1 -------- -3,3 1 -Dichlorobenzidine 340 JU 

56-55-3 --------- Benzo ( a)Anthracene 1 340 J U 

117-81-7 -------- bis ( 2-Ethylhexyl ) Phthalats_ I 340 J U 

218-01-9 -------- Chrysens I 

117-84-0 -------- Di-n-Octyl Phthalate 340 j U 

205-99-2 -------- Benzo(b)Fluoranthens 340 JU 

207-08-9 -------- Benzo(k)Fluoranthens 340 IV 

50-32-8 --------- Benzo(a)Pyrene 1 340 JU 

193-39-5 -------- Indeno(1,2,3-cd)Pyrens 340 1U 

53-70-3 --------- Dibenz ( a,h)Anthracene 340 IV 

191-24-2 -------- Benzo (q,h,i)Perylens 1 340 J U 

1 - CAT1nn* hA aa"A. A*MA }rnw T^r.h nnvl. 


t

IF 

000051 




I B07QD9 I 

Lab Name: T!!A/ABET — Contract: WHC I 

Lab Code: TMALA_ Case No.: 12074 SAS No.: NA SDG No.: N_ 

Matrix: (soil/water) SOIL y Lab Sample ID: A212074-03B 

Sample wt/vol: 30.0 (q/mL) G File ID: 30122522 

Level: (low/med) LOM Date Received: 12/21/92 

t Moisture: !3 decanted: (YIN) N 






Number TICs found: _ U (uq/L or uq/Rq) UG/RG 

I CAS NUMBER I COMPOUND NAME I RT I EST. CONC. I Q 

I 1. (UNXNOWN HYDROCARBON ( 5.27 ( 650 11 1 

I 2. IUNENOWN HYDROCARBON I 5.85 1 960 11 1 

I 3. (UNKNOWN HYDROCARBON I 5.90 I 790 IJ I 

I 4. 1UNIWOWN HYDROCARBON I 6.00 I 1200 IBS I 

i 5. IUNXNOWN HYDROCARBON I 6.55 I 95000 1BJ 1 

I 6. ISUBSTITUTED BENZENE I 6.73 I 69 IJ 1 

1 7. IUNXNOWN HYDROCARBON I 7.15 i 140 1W I 

I 8. IUMWOWN HYDROCARBON 1 7.32 1 69 IJ I 

I 9. IUNXNOWN XETONE I 7.73 1 1700 (BJ 1 

1 10. IUN10OWN HYDROCARBON I 9.03 1 140 IBJ I 

1 11. IPROPANOIC ACID ISOMER I 18.35 1 170 IJ I 

112. 

IUNINOWN CARBOXYLIC ACID ESTEI 21.40 1 

69 IBJ I 

i 

1 

1-1 .1-1 

FORM I SV-TIC 3/90


is 



Matrix: (soil/water) SOZL 


000032 

sPA SAMPLE NO. 

I I 

I B07QFO I 


SAS No.: NA SDG No.: N&_ 




3 Moisture: 2 decanted: (Y/N) )i_ Date Extracted: 12/23/92 



GPC Cleanup: (YIN) y,_ pH: 9.5 


CAS NO. COMPOUND (uq/L or uq/Rq) UG/RG 0 

108-95-2--------Phenol I 

111-44-4 -------- bis(2-Chloroethyl)Ether I 340 

95-57-8 --------- 2-Chlorophenol i 340 

541-73-1 -------- 1,3-Dichlorobenzens I 340 

106-46-7 -------- 1,4-Dichlorobenzene i 340 

95-50-1 --------- 1,2-Dichlorobenzens I 340 

95-48-7 --------- 2-Methylphenol I 340 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_I 340 

106-44-5 -------- 4-Methylphenol 1 340 

621-64-7 -------- N-Nitroso-Di-n-Propylam ns_1 340 

67-72-1 --------- Hexachloroethans I 340 

98-95-3 --------- Nitrobenzens I 340 

78-59-1 ----------- I 340 

88-75-5 --------- 2-Nitrophenol I 340 

105-67-9 -------- 2,4-Dimethylphenol i 340 

111-91-1 -------- bis(2-Chlorosthoxy)Methans_I 340 

120-83-2 -------- 2,4-Dichlorophenol 1 340 

120-82-1 -------- 1,2,4-Trichlorobenzene I 340 

91-20-3---------Naphthalene I 340 

106-47-8--------4-Chlorcanil e I 340 

87-68-3 --------- Hexachlorobutad ene I 340 

59-50-7 --------- 4-Chloro-3-Methylphenol I 340 

91-57-6 --------- 2-Methylnaphthalens 

77-47- 4 --------- Hsxachlorocyclopentad rns e 

340 


95-95- 4 --------- 2,4,5-Trichlorophenol I 810 

91-58-7 --------- 2-Chloronaphthalene I 340 

88-74-4 --------- 2-Nitroanilins I 810 

131-11-3 -------- Dimethylphthalate ( 340 

208-96-8 -------- Acenaphthylene I 340 

99-09-2 --------- 3-Nitroanilins i 810 

83-32-9 ---------- cenaphthene I 340 

51-28-5 --------- 2,4-Dinitrophenol I 810 

FORM I SV-1 

i 

340

lC 

SEMIVOLATILE ORGANICS ANALYSIS DATA SHIM 

UOUO33 

XPA SAMPLE NO. 

1 I 

1 B07QFO ) 

Lab Naas: TMA/ARLI Contract: WHC I l 

Lab Cods: TMALA Cass No.: 12074 SAS No.: NA SDG No.: Nom_ 

Matrix: (soil/water) SOIL r Lab Sample ID: A212074-04B 

Sample wt/vol: 30.1 (9/ML) Q_ Lab File ID: 30125506 

Level: (low/mod) 

t Moisture: 2 decanted: (Y/N) N 


Injection volume: 2.0(uL) 

GPC Cleanup: (YIN ) Y_ 


pH: 9.5 

I 

100-02-7 -------- 4-Nitrophenol 1 






(ug/L or uq/Rg) UG/XG Q 

132-64-9 -------- Dibenzofuran I 340 III 

121-14-2 -------- 2,4-Dinitrotoluene 1 340 III 

606-20-2 -------- 2,6-Dinitrotoluene I 340 IV 

84-66-2 --------- Diethylphthalate I 50 Ii 

7005-72-3 ------- 4- Chlorophenyl-phenylether_I 340 III 

86-73-7 --------- Fluorens 1 340 IU 

100-01-6 -------- 4-Nitroan 1 ne 

I 810 IU 

534-52- 1 -------- 4,6-Dinitro-2-methylphenol i 810 III 

86-30-6 --------- N-Nitroeodiphenylanine (1),I 340 IV 

101-55-3 -------- 4-Bromophenyl-phenylether I 340 IV 

118-74-1 -------- Hexachlorobenzene I 340 III 


85-01-8 --------- Phenanthrene 1 340 IU 

120-12-7 -------- Anthracens 1 340 1U 

86-74-8 --------- Carbazole I 340 IV- 

84-74-2 --------- Di-n-Butylphthalate I 120 IW 

206-44-0 -------- Fluoranthene I 340 III 

129-00-0 -------- Pyrene I 340 III 


JU 

91-94-1 --------- 3,3'-Dichlorobenzidine I 340 III 

56-55-3 --------- Benzo(a)Anthracene 1 340 III 

117-61-7 -------- bis(2-Ethylhexyl)Phthalate— I 340 IV 

218-01-9 -------- Chrysene I 340 IU 

117-84-0 -------- Di-n-Octyl Phthalats I 340 IV 

205-99-2 -------- Benzo(b)Fluoranthene I 340 IU 

207-08-9 -------- Benzo(k)Fluoranthene 1 340 III 

50-32-8 --------- Benzo(a)Pyrene 1 340 

IU. 

193-39-5 ------- -Indeno(1,2,3-cd)Pyrene 1 340 IU 

53-70-3 -------- -Dibenz(a,h)Anthracene I 340 IU III 


830 

I 

III 

FORM I SV-2 3/90

000034 

1FEPA SAMPLE E0. 

SEMIVOLATILS ORGANICS ANALYSIS DATA SHEET 


I B07QF0 


Lab Code: TMALA_ Case No.: 12074 SAS No.: NA SDG No.: N_ 

Matrix: (soil/water) SAIL Lab Sample ID: A212074-04B 

Sample wt/vol: 30.1 (q/mL) G Lab File ID: 30125506 

Level: (low/med) ;Qf-- Date Received: 12/21/92 

t Moisture: ,2 decanted: (Y/N) W Date Extracted: 12/23/92 


Injection Volume: 2,O(UL) Dilution Factor: 1.0 

GPC Cleanup: (Y/N) Y _ pH: 9.5 


Number TICS found: _ a (uq/L or uq/Rq) UG/KG 

I 

I CAS NUMBER 

I 

I COMPOUND NAME 

I 

I 

I RT I EST. CONC. 

I I 

1 1. (UNKNOWN HYDROCARBON 1 5.43 1 300 IBJ I 

1 2. 1UNKNOWN HYDROCARBON 1 5.88 1 1700 IJ I 

I 3. (UNKNOWN HYDROCARBON 1 6.00 i 1500 18J I 

1 4. (UNKNOWN HYDROCARBON 1 6.55 ( 95000 I BJ I 

1 5. (UNKNOWN HYDROCARBON 1 7.15 1 140 1BJ I 

1 6. (UNKNOWN KETONE 1 7.73 1 1900 iW I 

1 7. (UNKNOWN HYDROCARBON 1 9.03 1 300 1BJ I 

I 8. 

(UNKNOWN CARBOXYLIC ACID ESTEI 21.40 1 

100 1BJ I 

I 

1 

1-1 

I Q 

.1-1 

FORM I SV-TIC 3/90

ID 

PESTICIDE ORGANICS ANALYSIS DATA SBEET 

SPA oua^ 

1 I 

I B07Q35 I 


Lab Code: TMALA Case No.: 12074 SAS No.: NA 8DG No.: NA 


Sample wt/vol: 30.0 (q/mL) Q_ Lab Pilo ID: 


k Moisture: 9 decanted: (Y/N) 1i_ Date Received: 12/21/92 

3xtraction: (SepF/font/Sonc) SONC Date Extracted: 12/24/92 

;oncentrated Extract Volume: 5000 (uL) Date Analyzed: 01/07/93 

Injection volume: 1.00 (UL) Dilution Factor: 1.00 

3PC Cleanup: (YIN) Y pH: 8.9 Sulfur Cleanup: (Y/N) N 



(uq/L or uq/Rg) UG/RG Q. 

i 1.91U 

I 

i 

i 319-84-6 -------- alpha-BHC i 

319-85-7 -------- beta-BHC I 1.91U 

1 319-86 -8 -------- delta-BHC 1 1.91U 

1 58-89-9 --------- gamma -BHC (L ndane) 1 1.91U 

1 76-44-8---------Heptachlor ( 1.91U 

1 309-00-2 -------- Aldrin 1 1.91 U 

1 1024-57 - 3-------Heptachlor spox de 1 1.91U 

1 959-98-8 -------- Endosulfan I 1 1.91U 

1 60-57-1 --------- Dieldrin 1 3.61U 

1 72-55-9 -------- -4,4'-DDE 1 3.61U 

1 72-20-8 -------- -Endrin 1 3.61U 

i 33213-65-9 ------ Endosulfan II 1 3.61U 

1 72-54-8 --------- 4,4'-DDD I 3.61U 


1 50-29-3---------4,4'-DDT I 3.61U 

1 72-43-5 --------- Methoxychlor I 19 1U 

i 53494-70-5 ------ Endrin ketone I 3.61U 

i 7421-36-3 ------- Endrin aldehyde 1 3.61U 



1 8001-35-2 ------- Toxaphene 1 190 IV 

1 12674-11-2 ------ Aroclor-1016 i 36 IU 

1 11104-28-2 ------ Aroclor-1221 i 74 III 

1 11141-16-5 ------ Aroclor-1232 1 36 III 

i 53469-21-9 ------ Aroclor-1242 I 36 IU 

1 12672-29-6 ------ Aroclor-1248 1 36 III 

11097-69-1 ------ Aroclor-1254 36 IV 

1 

1 11096-82-5 ------ Aroclor-1260 1 36 III 

FORM I PEST 

3/90

1D 


000036 

EPA SA1@LE 110. 

i 1 

1 D07086 1 

Lab Name: THA/ARLI Contract: 11HC 1 1 

Lab Code: g'KALK _ Case No.: 12074 SAS No.: NA SDG No.: NA 

Matrix: (soil/eater) SOIL 

Sample wt/vol: 30.1 (q/mL) G_ Lab File ID: 

Lab Sample ID: A212074 -068 

t Moisture: 3 decanted: (YIN) H—Date Received: 12/21/92 


Concentrated Extract Volume: 5000 (UL) Date Analyzed: 01/08/93 



CAS NO. 

7 

1 76-44-8---------Heptachlor 

i 309-00-2 -------- Aldrin 

1 1024-57-3-------Heptachlor spox de 

1 959-98-8 -------- Endosulfan I 

1 60-57-1 --------- Dieldrin 

1 72-55-9 --------- 4,41-DDE 

i72-20-8 --------- Endrin 

1 33213-65-9 ------ Endosulfan II 

1 72-54-8---------414'-DOD 

1 1031-07-8 ------- Endosulfan sulfate 

1 50-29-3---------4,4$-DDT 

53494-70-5 ------ Endrin 

7421-36-3 ------- Endrin 

1 8001-35-2 ------- TOxaphene_ 

i 12674-11-2 ------ Aroclor-101 

1 11104-28-2 ------ Aroclor-122 

1 11141-16-5 ------ Aroclor-123 

1 53469-21-9 ------ Aroclor-124 

1 12672-29-6 ------ Aroclor-124 

i 11097-69-1 ------ Aroclor-125 

1 11096-82-5 ------ Aroclor-126 

I 

FORM I PEST 


1.00 

Sulfur Cleanup: (YIN) N 

ANCENTRATION UNITS: 

(uq/L or uq/Kq) UG/KG 4 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71V 

1.71U 

1.71U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

17 1U 

3.41U 

3.41U 

1.71U 

1.71U 

170 1U 

34 1U 

69 IU 

34 1U 

34 1U 

34 (U 

34 III 

34 1U I- 

3/90

1D 


000037 

SPA sumal 110. 

1 ( 

1 B07QD7 I 

Lab Name: THAIARLI Contract: NBC 1 1 

Lab Code: TMALA Case No.: 12074 SAS No.: NA SDG No.: MA 

latrix: (soil/water) SOIL Lab Sample ID: A212074-OID 

iample wt/vol: 29.7 (Cl/ML) Q_ Lab File ID: 

t Moisture: 6 decanted: (YIN) N Date Received: 12/21/92 

3xtraction: (SepF/font/Sonc) SONC Date Extracted: 12/24/92 

:Oncentrated Extract Volute: 5000 (uL) Date Analyzed: 01/06/93 


3PC Cleanup: (YIN) Y— pH: 9.3 Sulfur Cleanup: (Y/N) X 


CAS NO. COMPOUND (uq/L or uq/Kq) UG/KG Q 

I 1 

319-84-6 -------- alpha-BHC I 1.8 

319-85-7--------beta-BBC I 1.8 

319-86-8 -------- delta-BHC I 1.8 

158-89-9 --------- gamma-BHC ( ndane) I 1.8 

76-44-8---------Heptachlor I 1.8 

309-00-2 -------- Aldrin I 1.8 

1 1024-57-3-------Heptachlor epoxide I 1.8 

959-98-8 -------- Endosulfan I I 1.8 

60-57-1 --------- Dieldrin I 3.5 

72-55-9---------4,4'-DDS I 3.5 

72-20-8 --------- Endrin i 3.5 

33213-65-9 ------ Endosulfan II ( 3.5 

72-54-8 --------- 4,4 1 -DDD I 3.5 

1031-07-8 ------- Endosulfan sulfate I 3.5 

50-29-3---------4,4'-DDT I 3.5 

72-43-5 --------- Methoxychlor I 16 

53494-70-5 ------ Endrin ketone I 3.5 

i 7421-36-3 ------- Endrin aldehyde I 3.5 

5103-71-9-------alpha-Chlordane I 1.8 

i 5103-74-2-------gamma-Chlordane I 1.8 

8001-35-2 ------- Toxaphene I 180 

i 12674-11-2 ------ Aroclor-1016 I 35 

11104-28-2 ------ Aroclor-1221 I 72 

11141-16-5 ------ Aroclor-1232 1 35 

53469-21-9 ------ Aroclor-1242 I 35 

1 12672-29- 6 ------ Aroclor-1248 I 35 

11097-69-1 ------ Aroclor-1254 I 35 

11096-82-5 ------ Aroclor-1260 

I 35 

I 

I 

FORM I PEST 3/90

ID 

PESTICIDE ORGANICS ANALYSIS DATA SHSET 

Lab Name: TMA/ARLI Contract: NHC I 

000038 

EPA SAM1gA N0. 

I BO7QDB 

'.gab Code. TMALA Case No.: 12074 SAS No.: NA SDG No.: NA 

tatrix: (soil/eater) SOIL 11s Lab Sample IDs A212074-02B 

Sample et/vol: 30.6 (9/AL) Q_ Lab File ID: 

k Moisture: 4 decanted: (Y/N) N Date Received: 12/21/92 

:xtraction: (Sapp/Copt/Sonc) SONC Date Extracted: 12/24/92 

7oncentrated Extract Volume: 5000 UL) Date Analyzed: 01/07/93 


;PC Cleanup: (YIN) Y p8: 8.2 Sulfur Cleanup: (Y/N) N 


CAS NO. COMPOUND (ug/L or ug/Rg) UG/RG Q 

J 

J 319-85-7 -------- beta-BHC 1 1.71U I 

J 319-86-8 -------- delta-BHC I 1.71U I 

J 58-89-9 --------- gamma-BHC ( ndane) I 1.71U I 

176-44-8---------Heptachlor J 1.71U I 

J 309-00-2 -------- Aldrin I 1.71U I 

i 1024-57-3-------Heptachlor spox de I 1.71U I 

1959-98- 8 ------- -Endosulfan I I 1.71U I 

1 60-57-1 -------- -Dieldrin I 3.41U I 

172-55-9 -------- -4 # 4 0 -DDE J 3.41U 

J 72-20-8 -------- -Endrin i 3.41U I 

I I 

1 319- 84-6 -------- alpha-BHC i 1.71U 

1 33213-65-9 ------ Endosulfan II I 3.4IU I 

172-54-8 --------- 4,4'-DDD J 3.41U I 

J 1031-07-8 ------- Endosulfan sulfate I 3.41V 1 

J 50-29-3---------414'-DDT J 3.41U 

172-43-5---------Methoxychlor I 17 III I 

1 53494-70-5 ------ Endrin ketone I 3.41U I 

1 7421-36- 3 ------- Endrin aldehyde J 3.41U I 

J 5103-71-9-------alpha-Chlordane J 1.71U I 

1 5103-74-2-------gamma-Chlordane I 1.71U I 

1 8001-35- 2 ------- Toxaphene I 170 JU I 

12674-11-2 ------ Aroclor-1016 I 34 JU I 

1 11104-28-2 ------ Aroclor-1221 J 68 I U I 

111141-16- 5 ------ Aroclor-1232 J 34 IV I 

i 53469-21-9 ------ Aroclor-1242 I 34 JU I 

J 12672-29-6 ------ Aroclor-1248 J 34 JU I 

111097-69- 1 ------ Aroclor-1254 J 34 JU I 

J 11096-82-5 ------ Aroclor-1260 

I 

34 JU I 

I 

I 

I I 


I

ID 

PESTICIDE ORGANICS ANALYSIS DATA SMEET 

000039 

SPA SAMPLE NO. 

I I 

I 807QD9 I 

Lab Name: TMA/ARLI Contract: NMC I I 

Lab Code: M21A_ Case No.: 12074 SAS No.: NA SDG No.: NA 

Matrix: (soil/water) SOIL -.- Lab Sample ID: A212074-03B 


V Moisture: 3 decanted: (YIN) N Date Received: ya/21/9z 

Extraction: (SepF/font/SOnc) SONC Date Extracted: 12/24/92 

Concentrated Extract Volume: 5000 (uL) Date Analyzed: O1/07/93 

injection Volume: 1.00 (uL) Dilution Factor: 1.00 

+PC Cleanup: (Y/N) Y_ pH: 9.5 Sulfur Cleanup: (Y/N) TL 



319-84-6 -------- alpha-BHC 

319-85-7 -------- beta-BHC 

319-86-8--------delta-BHC 

58-89-9 --------- aamma-BHC 

309-00-2 

1024-57- 

959-98-8 

72-55-9 --------- 4,4'-DDE 

72-20-8 --------- Endrin 

33213-65-9 ------ Endosulfan II 

72-54-8 --------- 4,4'-DDD 

1031-07-8 ------- Endosulfan sulfate 

50-29-3---------4,4'-DDT 

53494-70-5 ------ Endrin 

7421-36-3 ------- Endrin 

5103 

11141-16-5 ------ Aroclor- 

12 

11096-82-5 ------ Aroclor-12 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

3:41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

17 1U 

3.41U 

3.41U 

1.71U 

1.71U 

170 1U 

34 1U 

68 1U 

34 1U 1U_ 

34 

34 IU 

34 1U 

34 1U 

FORM I PEST 3/90

Lab Name: TNA/ARLI 

1D 

PESTICIDE ORGANICS ANALYSIS DATA SHSET 

Gab Code: TMALA Case No.: 12074 


sample wt/vol: 30.4 (g/mL) G 

t moisture: 2 decanted: (Y/N) K-- 

3xtraction: (SepF/Copt/Sonc) SONC 

:oncentrated Extract Volume: 5000 (UL) 


3PC Cleanup: (Y/N) Y_ pH: 9.5 

000040 

EPA gains, E NO. 

I 1 

I B07QFD ) 


SAS No.: NA SDG No.: MA 

._ Lab Sample ID: A212074-04B 

Lab File ID: 

Date Received: 12j21/92 

Date Extracted: ~12/24/92 



Sulfur Cleanup: (Y/N) Ii_ 



319-84-6 -------- alpha-BHC 1 1.71U 1 

319-85-7 -------- beta-BHC I 1.71U 1 

319-86-8 -------- delta-BHC 1 1.71U 1 

58-89-9 --------- gamma-BHC (L dane) I 1.71U 1 

76-44-8---------Heptachlor I 1.71U 1 

309-00-2 -------- Aldrin 1 1.71U 1 

1024-57-3-------Heptachlor epoxide I 1.71V 1 

959-98-8 -------- Endoeulfan I 1 1.71U 1 

60-57-1 --------- Dieldrin 1 3.31U 1 

72-55-9 --------- 4,4'-DDE 1 3.31U 1 

72-20-8 --------- Endrin I 3.31U 1 

33213-65-9 ------ Endosulfan II I 3.31U 1 

72-54-8 ------- --4,4'-DDD I 3.31U 1 

1031-07-8 ----- --Endosulfan sulfate I 3.310 1 

50-29-3---------404'-DDT 1 3.31U 1 

----------Nothoxychlor or 1 17 IV 1 

53494-70-5 ------ Endrin ketone I 3.31U 1 

7421-36-3 ------- Endrin aldehyde 1 3.31U 1 

5103-71-9-------alpha-Chlordane I 1.71U 1 

5103-74-2-------gamma-Chlordane 1 1.71V 1 

8001-35-2 ------- Toxaphene I 170 III 1 

12674-11-2 ------ Aroclor-1016 1 33 III 1 

11104-28-2 ------ Aroclor-1221 1 67 I U 1 

11141-16-5 ------ Aroclor-1232 1 33 I II 1 

53469-21-9 ------ Aroclor-1242 1 33 III 1 

12672-29-6 ------ Aroclor-1248 1 33 III 1 

11097-69-1 ------ Aroclor-1254 I 33 I II 1 

11096-82-5 ------ Aroclor-1260 i 33 

I 

IV I 

I I 

FORM I PEST 3/90

Westinghouse 


Custody Form initiator IJIQ Reayk'* 


Company contact WV SETZER Telephone 376-2413 

Project Designation/Somplfng Locations 100-NR-1 CoLlection Date /q /l0-9A 

Ice Chest No. .Sm- L- 197 Field Logbook No. EFL-/06,1 

g ill offLading/Airbill No. A--y 6n 7 Q' Offaite Property No. 



Possible Sampte Hazards/Remarks None detected with field instruments. Maintain at 4C. 


X907 ,250m aG: P; CP AA eta s, g,Cn 



1,1000ml G/ P:Gross alpha/beta,Gamma Spec,Sr -90,C-14,U -235/238,Pu - 239/240,Am- 

241 

2) 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 



1,1000ml G : Gross alpha/beta, Gamma Spec, Sr-90,C-14 , U-235/238,Pu-239/240,Am-241 

3) 1,250m] aG:CLP;ICP/AA Metals,Hg,Cn 

G:CLP;VOA 

1,950ml 

1,1000ml 

aG: • mi-VOA,PCB/PEST,Anions (F,SO4,NO3) 

G:Gross a prate a,Gamma Spec,Sr-90,C-14,U-235/238,Pu-239 /-240,Am-241 

u 

Field Transfer of Custody Chain of Possession (sign and Print Names) 

Relinquished by: Reeei by: 

(e/!_ 

Reli ed by Received by: 9 13 1 u. •+ 

. î 

yL 

Date/Time: 


Relinquished by: Received by: Date/Tine: 

Disposal Method: i Disposed by: i Date/Time: 

Comments: * 11 

RCC e: %PeU e MA MO 0 tCA 

/ 

A • 6000-407 (12/90) CEF) WEF061 


o Sa 

Date/Time: 

/2'2l-9z OSt 

/2-19-92 ; &P&Ned /^' -z/-9Z -K6

Westinghouse 


ICHAIN OF CUSTODY 

Custody Form Initiator :VQ RE6VE; 3 


Project Designation/Somplin g locations 100-NR-1 Collection Date 129 1d.-9A 

Ice Chest No. . ls'm L /R 7 Field Logbook No. EFL- 1063 

Bill c0LadirWAirbill No. 7R 57 offsite Property No. /U9, 'd /Tx 




Semple identification 

1 &7 907 1,250m aG: ; C AA Meta s, g, n 



1,1000ml G/P:Gross alpha / beta, Gamma Spec, Sr-90 , C-14,U-235/238,Pu - 239/240,Am- 

241 

2) $ 1,250ml aG:CLP;ICP/AA Metals,Hg,Cn 




3) 1,250m1 aG:CLP;ICP/AA Metals,Hg,Cn 

G•CLP;VOA 

1,950ml aG: . mi-VOA,PCB/PEST,Anions (F,SO4,NO3) 

1,1000ml G:Gross a p a Gamma Spec, Sr-90,C-14,U-235/238,Pu-239/240,Am-241 

^ ra vs 

Field Transfer of Custody Chain of Possession (sign and Print Names) 

Reli,puished by: J Rexvi•5 Recei ' bY: 

(/e/ 

Rat1ed by: p 

Date/Time: 

Received by: ^(. J3l u^"^ Date/Time: 

O SO' 

)1C,J/ 

/^-z^-9z Oe6 

Relinquished by: Received by. Date/Time: 

Relinquished by: Received by: Date/Time- 

Final 

Disoosat Method: I Disoosed bv: I Date/Time: 

Comments: * (ZGce; v,-j G 7M.4 /iifo/ZCA / /1-19-94 ap ^J 12 zf -9z < K6 

A-6000-407 (12/90) (EF)-WEF061 

Chain of Custody

Westinghouse 


collector Date ^2' •/p 4z 

company contact WV SETZER tetephone (509)376-2413 

Cr wlbIb^T7 


Nunber and Type of Sample Containers/Analysis Required 

Runber Collected Collected 


120m1 aG CLP;VOA 

1-950m1 aG CLP;Semi-VOA,PCB/PEST 

_^,^ 300.0/353.2 ;Anions(F,SO4,NO3) 


U-235/238,Pu-239/240,Am-241 

1 Oml aG CLP;ICP/AA Metals,Hg,Cn 


,^J9Ql^R S iz•^G 9^ S3 

''950ml 

aG CLP;Semi-VOA,PCB/PEST 

300.0/353.2;Anions(F,SO4,NO3) 

v(-1000ml G Gross alpha/beta, Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 




300.0/353.2;Anions(F,SO4,NO3) 

1-1000ml G Gross alpha/beta, Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 




300.0/353.2;Anions(F,SO4,NO3) 

1-1 ml G Gross alpha/beta, Gamma Spec,Sr-90,C-14 

U-235/238,Pu-239/240,Am-241 

Dos 

*Type of Sample A = Air L = Liquid SE = Sediment T = Tissue x = other 

OL = Drum Liquids O = Oil SL = Sludge W = Water 

OS Drum ,Solids S = Soil SO = Solid WI Wipe 

Field information FROM 100 . #9-1 Drilling - 


Possible Sampte Hazards NA 

A-6000-406 (06/91) WEFO60

Westinghouse 


Custody Form Initiator Riewmr5 _. 


Company Contact WV SMER Tetephone 376-2413 

Project Deal gnat ioNeampLing Locations 100-NR-1 Collection Date î2-17-9%C 

Ice Chest No. .4ML _/7s Field Logbook No. _EFL- ,/ -/9ros /L 

Bill of*Lading/Airbill No. ;gS/42)6 offsite Property No. L4 4-9, T=d ' ^ /2L.T 


shipped to TMA/NORCAL 


1 8x apq 

241 

Sample identification 

1,2 m aG:CLP;ICPIAA Metals,Hg,Cn 

1, 120ml aG : CLP;VOA 

1,950ml aG : CLP;Semi-VOA,PCB/PEST,Anions ( F,SO4,NO2,NO3)PH 

1,1000ml G/P:Gross alpha/beta,Gamma Spec , Sr-90,C - 14,U-235/238,Pu-239/240,Am- 

2)80%Vf-V 1, 250ml aG:CLP ; ICP/AA Metals,Hg,Cn 

1,120ml aG:CLP;VOA. 

1,950ml aG:CLP ; Semi - VOA,PCB/PEST , Anions ( F,SO4 , NO3) "--' 

1,1000ml G : Gross alpha / beta, Gamma Spec, Sr - 90,C-14,U - 235/238 , Pu-239/240,Am-24] 

3)40705 1,250ml aG:CLP ; ICP/AA Metals,Hg,Cn 

1,120ml aG : CLP;VOA 

1,950m] aG:CLP; Semi -VOA, PCB/PEST, Anions (F,SO4,NO3)' 

°? r1969m',^G.: ,r-cs^—al efiafve#a.•Gamma Sae^Sr-90.0-1 4 a-235/ 't8 P I- -UL24D,A&--24'. 

60.Of. /Z -/7 -TG - - 

y^B07G186 / oZ27n4 aG:C^P%/CP/AA Mef^s,N9,Cn 

/ /X'0'9 aG : Gl.P YOA 

/ 9 (Za1,e aG : CLP vie rn- 3OA, /^Q/ sfrr ale, 1q/711ers 


Relinquished :J(^./{^5jReceiv by: Date/Time: 

D If 

Reli 'had I /^ Rec ived by.{(, 13 (,IH Date/Time: 

Sd fitrwf ^c 12-21-92- Ofsoo 

Relf ished hy: Received by: Date/Time: 

Relinquished by: Received by: Date/Tine: 

Final Sample Disposition 

Disposal Method: Disposed by: Date/Tine:_ 

Comments: * 

7M 4 1 NoQCAl I z 19 -92. -, oPe,ved !2 2/ •92 

A-6000-407 (12/90) CEF) WEF061 

chain of Custody 

S 

K/j

Westinghouse 


Collector . Dote /Z /cY• 9Z 

company contact WV SETZER telephone (509)376-24 .13 

sample Date Time 

Number Collected collected 

^^ny^ 

S .G2GZ^ eYa49 




P-950m1 

aG CLP;Semi-VOA,PCB/P, F 

300.0/353.2;Anions( (FSO4,NO3) 


U-235/238,Pu-239/240,Am-241 




^t^ S /Z/7.4 /nZ,A 300.0/353.2;Anions(F,SO4,NO3) 

-1000ml G Gross alpha/beta,Gamma Spec,Sr-90,C-14 

U-235/238,PLI-239/240,Am-241 

7 6/ S ( /3/ 


-0 20m] aG CLP;VOA 


300.0/353.2;Anions(F,SO4,NO3) 

WJs U-ZZ494944^^, Am 

24 1 



'-'1-950ml aG CLP;Semi-VOA,PCB/PEST 

300.0/353.2;Anions(F,SO4,NO3) 

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*Type of Sample A = Air L = Liquid SE = Sediment T = Ti ssue X = Other 

OL Drum Liquids 0 = Oil SL - Sludge V = Dater 

OS = Drum Solids S Soil SO = Solid VI - wipe 

Field Information FROM 100^Ng—/ brilling 



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Date -:? 22 XC _COMPANY 

Surveyor's Name 

RADIATION DOSE RATE SURVEY FORM 

C 

000006 

OTHER ORD / 4 , 0 3 7-S 

Model No. HP-21T I FSP-1 Model No. AC-S-7 / ESP-1 

Serial Nos. 710M 02619 Serial Nos. Oa619 

Calibr ation Date I ^1G` ^^ Calbration Date 

Instrument Calibration Factor n, Instrument Calbratioo Factor O 

©© w mm 

OK V 

reef: MLI aA-01 

ft v-06 

^^^_nnrten_^.^_ 

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01,13,

GENERAL CHEMISTRY RESULTS 

CASE N0. 12-074 

Soil Sample #: 

B07QD7 B07QDB B07QD9 

B07QFO B07QB5 B07QB6 


The holding times for the pH and Anions analysis 

was exceeded. Careful review of the QC analysis 

indicate the data is reliable. 

No other problems were encountered during sample 

analysis. All QC results were acceptable. 

00000'7

Received: 12122192 

000010 

IRA Inc. REPORT 

Rfwtts by Swpte 

York Order i A2-12-874 

SAMPLE ID R07OD7 FRACTION 9jk TEST CODE YCCLPS NAME Anions in Sotido - YN232 

Date S Time Collected I?i16192 

Category 

x 



Fluoride 300.0 1.0 so/K g 0.2 

pN 9045 9.3 pH 0.1 

Sulfate 300.0 10 Ng/Kg 2.0 

FORM I


000011 

TPA Inc. REPORT 

Results by Sauple 

York Order t AZ-12-074 

SAMPLE ID n 07gDS FRACTION 021_ TEST CODE VCCLPS NAME Anions in Solids - VR232 

Date L Time Collected 12116/92 

Category 



fluoride 300.0 1.3 mg /K g 0.2 

pN 9045 0.2 pN 0.1 

Sulfate 300.0 2040 no/K g 200 

FORM I

000012 

TMA Inc. REPORT Work Order 0 A2-12-674 


SAMPLE ID S07aD9 FRACTION Qom, TEST CODE VCCLPS NAME Anions in Solids - VN232 

Date i Time Collected 12117192 Category 

— i- 

ANIONS AND NET CHEMISTRY . SOLIDS 


Fluoride 300.0 0.9 me/K9 0.2 

pN 9045 9.5 pN 0.1 

Sulfate 300.0 40 eg/Ko 2.0 

FORM I

000013 

IRA Inc. REPORT Wort Order t A2-12-974 


SAMPLE ID 9070FO FRACTI0N 049 TEST CODE WCCL ► S NAME Anions in Solids - WN232 

Date 4 Time Collected 12117/92 Category 


ANALYSIS METH00 RESULT UNITS LIMIT 


PH 9045 9.5 PH 0.1 

Sulfate 300.0 40 m0/Kg 2.0 

FORM I

000014 

TNA Inc. REPORT York Order 0 A2-12-974 

Received: 12/22192 Resultte by triple 

SAMPLE ID 907095 FRACTION UA TEST CODE YCCLPS NAME Anions in Solids - VN232 

Date i Tiee Collected 12/17/92 Category 

0 


ANALYSIS METHOD RESULT UNITS LI IT 

Fluoride 300.0 2.4 mg/KO 0.2 

PH 9045 3.9 PH 0.1 

Sulfate 300.0 9 m g/Kg 2.0 

FORM 1

000015 

TMA Inc. REPORT York Order • A2-12-074 

Received: 12/22/92 Results by Sampte 

SAMPLE 10 107g96 FRACTION 069 TEST CODE WCCLPS NAME Anions in Solids - 09232 

Date i Time Collected 12/17/92 Category 

t- 

ANIONS AND WET CHEMISTRY • SOLIDS 


Fluoride 300.0 1.6 m g /K g 0.2 

PH 9045 8.7 PH 0.1 

Sulfate 300.0 33 mg/Kg 2.0 

FORM I

JQ 

oCf1C?C3. '^//6^9? 

Pape 1 Skinner&Sherman REPORT Work Order t S2-12-330 

Received: 12/22/92 01/25/93 16:37:14 

REPORT TMA/NORCAL PREPARED TMA / Skinner & Sherman Labs. 

TO 2030 Wright Avenue i BY 300 Second Avenue 

Richmond, CA 94804 P,O, Box 521 

Waltham. MA 02254 CERTIFIED BY 

ATTEN Dan Steurmer ATTEN Went Services 

PHONE (617) 890-7200 CONTACT DP 

CLIENT HANFORD NOR SAMPLES 7 

COMPANY TMA/NORCAL Hanford 

FACILITY Richmond, CA 

WORK ID N2-12-113 

TAKEN BY CLIENT 

TRANS FED EX 

TYPE SOIL 

P.O. p N2-12-113 

INVOICE Wrier separate cover 

SAMPLE IDENTIFICATION TEST CODES and NAMES used an this wrkorder 

2 1 007OD7 NITR S Nitrate/Nitrite in Soils 

237 607008 

of Bonn 

24 Bo7GFO 

2£ 007085 

PA 607086 

2k 007086 OWL 

06 007086 SPIKE 

07 LCSS

Pam 2 SkimrrLsherrh REPORT Work Order ! S2-12-350 

Received: 12/22/92 Results by Semple 

7hemmAnalydad inc 

SAMPLE ID 607007 SAMPLE Y 01 FRACTIONS: A 

,Qate i Time Collected 12116/92 Category SOIL 

NITR S

A 4A 

Pape 3 Skimertshenm REPORT Work Order # SZ-iZ-370 


SAMPLE ID 207066 SPIKE SAMPLE k 06 FRACTIONS: C 

Datti Time Collected 72/17'/92 Category SOIL 

YITR S 35.0 

no N/kg 

SAMPLE ID LCSS SAMPLE # 07 FRACTIONS: A 

YITR S 1.57 

as N/L 

Data i Time Collected not aeecifi:ed Category SOIL 

000003 

Tbuwpon iattMna:f upon JI d NefGlowinBOdatlnian Skimv! 51m^ 1..banoriri.InC rtuuwornaahipol^hG rtponuW a+amatd wbiaiend wrxe u 

} [upar^mmae^vlcnvlWlbeavnilabkurmnluna

evp—eo.l 

Page 4 SkinnerLshermn REPORT York order 0 S2-12-330 

Received: 12/22/92 01/25/93 16:37:14 

TMA/NORCAL Hanford 

QUALITY CONTROL 

MATRIX SPIKE 

Sample ID Sample Resuit Spike Added Spike Result % Recovery 

S212330-D6 16.2 mg/kg 19.9 mg/kg 35.0 mg/kg 94.5 

DUPLICATE Relative 

Sample ID Sample Result Duplicate Result % Difference 

5212330-06 16.2 mg/kg 12.8 mg/kg 23.5 

QUALITY CONTROL SAMPLES 

Sample ID True Value Farad Value % Recovery 

LCS 2.00 mg/L 1.67 mg/L 93.5 

Blank (1/20) --

Pape 5 Skinnergshernan REPORT Work order t S2-12-330 

Received: 72/22/92 Tat Methodology 

TEST CODE RITR S NAME Nitrate/Nitrite in Soils 

The sample was extracted with deionized water and analyzed in accordance with 

Method for Chemical Analysis of Water and Wastes EPA-600/4-79-020, March 1979, 

Method 353.2 (modified) 

000OCs

00(,'O.3S 

TMA/Skinner & Sherman Labs SAMPLE LOG-IN 

WORKORDERCLIENT No. SAMPLES: 

PROTCL ^. ^; TURNARND S J^^_; s ^._ 

COOLER TEMP: 3 oC, or NA (Soil) (Water) (Specify Other) 

CUSTODIAN h. SDG/BATCH ti' A- 

CUSTODY SEAL:PRESENT/ASSENT/II$TACT/NOT CLIENT CASE 

v ^CZ 3 

SHIPER & $ oA l'. ^= K PO/CONTRACT,# u 

TAGS: PRESENT/ABSENT/4A/SEE COC CONTACT ^•SR,vc.izz 

CHAIN OF CUSTODY: $RE -SENT/ABSENT/NA,$ tilt- COMMENTS: vc1^` 

SAMPLE CONTAINERS- gA 

T CT/BROKEN COMMENTS 

SAMPLE LABELS AGREE WITH CHAIN OF CUSTODY INF °!LES / NO (COMME 

CLIENT PAPERWORK AGREES WITH SAMPLES & COC? YES) /NO (COMMENT) 

LIST ANY DATE WITH 

CLIENT ID MATRIX RECEIVED PH* TEST(S) & QC HOLD TIME UI 

N» Q h 

C2 T3 0a C>. 1 f- 

3 `?3 L^-iQnR 

4 7ônQ 'F L^ 

5 V-1c)1 cZ 6{ 

L6 bmQ 8U 

7 89 

10 

12 

13 

14 

15 

16 

17 

18 

19 

20 

21 

22 

23 

Sol 1 12-L2112 , j I A. fJO,Ûz 

- 

24 

25 

26 

27 

samples are from site known to have Rad- Contamination: YESN J O 

samples have detectable amounts of Radioactive Material:YES_NO 

SUBCONTRACT: YE INO, TO: D^ 

REVIEWED iZ'Z'^^C^^ 

* EPA/CLP required -- Rev 1:6 - PAGE:- 1- 

Z-

Thenno Analytical Inc 

Skinner & Sherman Labs., Ina 

Post Office Box 521 1 

FAX (61 7) 890-3883 

January 25, 1993 

TMA/NORCAL 

2030 Wright Avenue 


Attention: Dan Stuermer 

Ouality Control Narrative 

^^r 

Scone 

Six (6) soil samples were submitted to TMA/Skinner & Sherman 

Laboratories, Inc. on December 22, 1992 from TMA/Norcal. The 

samples were analyzed for the USEPA CLP Target Analyte List 

metals and cyanide. The analysis were performed under 

TMA/Skinner and Sherman work order 5212327. 

Met od loay 

The samples were prepared, analyzed and reported in accordance 

with the USEPA Contract Laboratory Program Statement of Work 

ILMO2. 

Discussion 

All quality control requirements were met for the samples with 

the following exceptions; 

The antimony, and selenium digestion spike recovery exceeded the 

control limit requirements. 

The ICP serial dilution for zinc exceeded the control limit 

requirements. 

The chromium laboratory duplicates exceeded the control limit 

requirements. 

Please feel free to call if there are any questions concerning 

this package. 

Respectfully submitted, 

TMA/SKINNER & SHERMAN LABORATORIES, INC. 

David N. Peterson 

Assistant Laboratory Manager 

a^ 

001


COVER PAGE - INORGANIC ANALYSES DATA PACKAGE' 

Lab Name: SKINNER & SHERMAN LABS. ,- Contract: 68-DO-0108 

Lab Code: SKINER Case No.. N2-12-1,13 SAS No.: SDG No.: S070B5 

SOW No.: ILMO2.1 

SAMPLE NUMBER: Lab Sam p le ID. 

B07OB5 12327-053 

B07OB6 12327-06S 

B07056D 12327-06S2 - 

6070B6S 12327-06DS 

6070D7 12327-01S 

B070DS 12327-02S 

6070D9 12327-0.3S 

6070FO 12327-04.S 

Were '1 CP inter • element corrections applied? 

Were TCP bac:!•. round ac,r_,ii.=d? 

If Yes .-were raw datzy vnerated before= 

a pp lication of backgrol_irri 'rorr•^r L' Lon s'? 

Comments: 

ês/No YES 

Yc •^'No 'iE° 

Ye es/No NO 

I certif y that this data oac!


1 


rs ,- 

Lab Name: SKINNER & SHERMAN LASS. Contract: 68-DO-0108 


B070B5 

Lab Code: SKINER Case No.: N2-12-11 .35AS No.: SDG No.: B07QB5 

Matrix (soil/water): SOIL Lab Samp le ID: 12327-055 


Solids: 91.5 

Concentration Units (u g /L or rn q /)< .; dr y weight): MG/KG 

1 I 

:CAS No. Analyte :Concentration!C: Q :M 

i 

;7429-90-5 !Aluminum 8200 !P~: - 

:7440-36-0 !Antimon y 3.7 IU: N :P7 

:7440-38-2 :Arsenic 2.. S :F" - 

:7440-39-3 :Barium ._.. :P 

;7440-41-7 :Ber y llium; 0.35:6: P. 

7440-43-9 :Cadmium 2).7-^:U: :P--• 

7440--70-2 :Calcium _500 :P-.• 

:7440-47-3 

17440-48-4 

,7440-50-8 

:7439-89-6 

!Chromium 

!Cobalt 

:Copp er 

:Iron 

i0.i 

'-'' -'-.:• 

-.._ 

20000 

* IP 

IP' 

:P, 

'P,.• 

:7439-92-1 ; Lead 

7439-95-4 :Ma gnesium: 

;7439-96-5 :Mang anes_: 

,7439-97-6 :Mercur y 

'7440-02-0 :Nick--1 

17440-09-7 ;Potassium: 

'7782-49-2 :Selenium 

;7440-22-4 :Silver 

:7440-23-5 :Sodium I 

:7440-28-0 :Thallium 

. 4.40-62-2 :Vanadium 

:7440-66-6 :Zinc 

!C y anide 

a3-ZrA• 

_-- 

0.05:U: 

.0._ 

1320 : 

0.6/i:U: WN 

.._ :BI 

212 ,B: 

0.54:U: W 

15.,? 

4°.7 E 

0.52!U: 

tP - 

:P... 

:CV: 

:P- 

:P: 

F. 

:P 

:P 

:F- 

:F 

:P- 

:CA: - 

::oior Before: BROWN Clarity B?tore: Text ure: .MEDIUM 

Color After: BROWN Clarity After: Artifact! YE° 

ST4ME_ 

:=9RM 1 - TN 

?LMO2.1

Color Before: BROWN 

Color, After"- BROWN 

r „rnm^r: if •_. 

STONES 


1 


Lab Name: SKINNER & SHERMAN LABS. s Contract: 68-DO-0103 


607CS6 

Lab Code: SKINER Case No.: N2--12-113SAS No.- SDG No.: 807055 

Matrix (soil/water): SOIL 

Lab Sam p le ID: 12327-06S 



Concentration Units (u g /L or m9/Kg dr y weight): MG/KG 

;CAS No. , Anal y te ;Concentration;C; O ;M 

;7429-90-5 ;Aluminum ; 9010 ;P 

:7..40-36-0 ;Antimon y 7 ;U; N :P 

17440-38-2 ;Arseni•_ 2.4 ;F . 

; 7440- .'•9-3 : L?ar, iLIM 5o. S 

;7440-al-7 ;3 ._:^v11lum; 0.34;E; 

7440-43 -^ . •=sdmium 7. -•2 ; U ; 

:7440-70-2 :C_- lciuffl 7130 

;7440-47-3 .Chromium 1 13.7 

;744.0-4°--:_ ;Cobalt 10.4 - 

, 7e4-0 - 50 - 8 - oocer i9.9 ' P 

;7439-89-6 ,=ron 19500 ; ;P 

'7439-92-1 ;Load 5.`.' ; 

;7439-95-4 ;Magnesium; 4390 

7439-96-`_• :Manganese: _90 

7439-97-6 : Mercury 0.05W; ; C'v : 

;7440-02-0 ;Nickel 11.9 IF - 

;7440-09-7 ;Potassium; 1110 ;r^- 

;7782-49--? :Selenium 0.60; U; WN ;F 

;7440-2 2 -4 ;Silver 1.3 ;B; ;P - 

:7440-23-5 :Sodium 254 ;3; ;P 

;7440-2'S-0 : Thallium 0.50;U; :F - 

t7440- 6 2-2 :Vanadium 43.2 ;P - 

; 74.40-66-- 6 :Zinc i51 . S - ; p 

:C y anide 0.49:U: :CAC - 

Clarity Before: 

Clarit y After: 

FORM 1 - IN 

Texture: -FINE 

Ar•tifact^c .YES 

QID3 

ILt10_.

Color , Before: BROWN 

Color After: BROWN 

^'. 010117?':t S: 

sTnNE:. 


1 


Clarity Before: 

Clarit y .After: 


isz 607OD7 

Lab Name: SKINNER & SHERMAN LABS. Contract: 63-D0-0108 

Lab Code: SKINER Case No.: N2-12--113SA.S No.: SDG No.: BO7OSS 



Solids: 

Concentration Units (u g /L or mg /Kg dr y weight): MG/KG 

I 

:CAS No. Analvte :Concentration:C; Q :M 

I _ 

;7429-90-5 Aluminum 5470 

17440-36-0 :Antimon y 3.6 ;U; :1\1 :P 

;7440-38-2 .Arsenic 2.0 S :F 

:7440-39-3 ;Barium 44.0 .P .. 

;7440-41-7 1Sar y lli um: 0.21;2; :? 

:7440-43-9 Cadmium 0.31:U: 

7440-70-2 ;Calcium 10700 . : 

:7440-47-3 :Chromium •3..: 

:7440-4£-4 :Cobalt 3.£ :B: .r . 

:7440-50-3 ;Copp er X6.0 :P 

:7439-89-6 ;Iron L69OO :P , 

7439-92-1 :Lead '3.7 :F 

:7439-95-G. :Magnesium: 3980 :F 

:7439-96-5 :Mangan•.:.,_ 257 :P 

;7439-97-6 :Mercur y O.OS;U: :CV.: 

. 440 -02 -0 : Nickel 9.6 : : .F 

;7440-09-7 :Potassium: 769 ;B; :P 

;7782-49-2 :Selenium t O.6O:U: WN 'F 

:7440-22-4 ;Silver 1.1 :B: :P: 

;7440-23-5 :Sodium 201 ;B: :P . 

;7440-2£-0 :Thallium O.5O:U: :F.: 

:7440-62-2 :Vanadium 36.2 , .. , 

:7440-66-6 :-.inc 37.0 E .; 

:C y anide O.52:U: :CA: 

FORM 1 — Ira 

Texture: -M ED I':"' 

._ 


ILMrd_^.


1 

INORG,,ANIC ANALYSIS DATA SHEET 

Lab Name: SKINNER 8 SHERMAN LABS. Contract: 68-DO-0108 


B070DS 

Lab Code: 'SKINER Case No.: N2-12-113SAS No.: SDG No.: 607055 

Matrix (soil/water): SOIL Lab Samp le I'D: 12327-025 



Concentration Units (ug/L or mg/Kg dr y wei ght): MG/KG - 

:CAS No. Analyte :Concentration :C1 

, 

17429-90-5 :Aluminum 1 4.220 

17440-36-0 ;Antimon y 3.5 :U: 

17440-38-2 :Arsenic 1.5 :B: 

'7440-•.39-; ;Barium 34.'+ 

7440-41-7 :Ber y llium; 0.20;6; 

,7440-43-7 ;Cadmium 0.71:U: 

' 74.40-•70--_ : Calf_ ium 5610 

'7440-47-3 ;Chromium 6.Z 

:7440-48-4 :Cobalt 10. 1-1 

:7440-50-8 ;Corp er "0.5 

:7439-89-6 ;Iron 1800 

:7439- U2-1 : 1-ead 2.7 

:7439-95- r.. :Magnesium: 3750 

:7439-96-5 :Manganese: -Z , 

:7439-97-6 :Mercur y 0.05: 111 : 

:7440-02-0 :Nick.eI 3.L , 

:7440-09-7 ;Potassium: 749 :8: 

:7782-49-2 Selenium : 0.63:U: 

:7440-22-4 :Silver : 1.1 :B: 

:7440-23-5 ;Sodium 355 :B: 

:7440-28-0 :Thallium 0.53:U: 

:7440--62-2 :Vanarium i i3.5 

:7440-66-6 Nino 36.0 

: Cy:anide 0.51:U: 

, 

Color GREY Clarity oefors: 

Color .After: GREY Clarity .After: 

f.Jll pp F: i'I ': 'S 

_.TONE= 

FORM _ - i1\1 

O :M i 

:P 

N ;P 

W 

N 

E 

:P 

n, 

;C»; 

•o 

:P 

^c 

:P - 

: F, 

:GA: 

%:xLure: MEDIUM 

Artifacts. YES 

r 

.._ 

- CLMLzJ— I

WESTINGHOUSZ/HANFORD 

1 


INORGANIC ANALYSIS DATA SHEET - 

.^ 

607009 

Lab Name: SKINNER, & SHERMAN LABS. Contract: 63-DO-0105 

Lab Code: JKINER Case No.: N2-12-113SAS No.: '_DG No.: 6070B5 


Lab Samp le ID: 12327-03S 


Solids: 96.1 - 

Color Before: -,REY 

Co1•.;r After: GREY 

;^mm, 

Concentration Units (ug/L or m9/Kg dr y weight): MGJKG 

:CAS No. Analyte :Concentration:C: 0 :M. 

: 

:7429-90-5 :Aluminum 3430 -- 

;7440-36-0 ;Antimon y :.7 :U1 N :P. 

;7440-33-2 :Arsenic 1.0 :6: W :F 

:7440- -39-3 1Barium 65. 3 :P _. 

17440-41-7 ;ber y llium; 0.3161 :P•• 

, 744.0-d3--, :Cadmium 0.32:U: :P , 

1 7440-70-2 :Calcium 5560 

: 1 440-47-5 ;Chromium 1.4 ,• 

:74.40-•12-a :Cobalt 11. 8 :F- 

.7440-50-3 :Copp er' 20.6 :P 

'7439-39- 6 :Iron 2 2300 : I tP - 

: 7 439-?2-1 :Lead 2 .3 :F 

:7439-95-4 :Magnesium: 4030 'P 

:Manganese: 2S4 :P 

7439-?7-6 :Mercur y 0.05:U: ;C'•r: _ 

:74 4. 0-02-0 :Nickel ^.0 :3: :P , 

:7440-09-7 :Potassium: 562 :6: :P -: - 

:7752-49-2 :Selenium : 0.63:U: WN :F - 

:7440-22-4 :Silver 1.3 :B: :P 

:7440-2=3-5 :Sodium 292 :b: :P 

:7440-2S-0 :Thallium 0.53:U: :F : - 

,7440--2-- ,Vanadium 46.0 :P 

:7440-6o-6 :Zino 37.1 E :P.: 

:C y anide 0.51:U: :CA: 

Clarity Sefor.e: Tts::tui-c: - 'NEDIUN 

Clarit y Afterl : =Artifacts: YE= 

FORM I - IN 

._-_i10'2 . 1


1 


I,- 


Lab Code: SKINER Case No.: N2-12-113SAS No.: 


B070FO 

SDG No.: B070B5 



Solids: 96.7 

Concentration Units (u g /L or mg/Kg dr y wei ght): MG/KG 

:CAS No. : Anal y te :ConcentrationlCl O IM I 

;7429-90-5 ;Aluminum 3050 ;? 

;7440-36-0 :Antimon y 3.7 :U; ?1 :P 

;7440-38-2 ;Arsenic 0.7618; W :F 

;7440-39- Z ;Barium 4?.4. :? 

17440-41--7 ;Ber y llium; 0.21;8; 1P 

' 7440- r4 ^-:< :Cadmium 0-32: I J , :P 

;7440-70-2 ;Calcium 5510 1? _- 

:7440- 47 -3 ;Chromium 3.9 ;P 

;7440- 4 - -4 ;Cobalt 11.9 ;? : 

;7440-50-3 'Copp er 16.5 ;P 

;7439-89-6 ;Iron 21700 ;? 

:7439-92-1 'Lad 1.3 

17439-95-4. ;Mag nesium; 3890 :P 1 

;7439-96-5 ;Manganese; 254 :P 

;7439-97-6 1Merour y 0.051U1 ICvI 

17440-02-0 ;Nickel 6.3 :B: :P -- 

;7440-09-7 ;Potassium; 420 ;8: :P 

;7782-49-2 ;Selenium 1 0.58;U; WN ;F I 

;7440-22-G. 'Silver 1.9 181 1P 

:7440-23-5 :Sodium 319 :8: :P 

;7440-2S-0 ;Thallium 1 0.49;U1 W :F 

:%40- % 2-2 :Vanadium ; 46.7 ;P 

:7440-66-6 ;Zinc : 36.7 : E :P 

:C y anide 0.49;U1 :CAI 

Color Before: GREY Clarity Before: Texture: i`1EDIUM 

Color After: GREY Clarit y After: Artifacts: YES 

òmm•=nt ^: 

3T,ONE5 

FORM I - IN 

ILMO2.1 

,

TMA NORCAL 


^*21Z078 OI B07 

DATA SHEET 

SDG 7138 

Contact Dinkar Rharkar 




i moisture 5.9 


Contract MER-SVV-069262 

Client sample id B070BS 

Matrix SOIL 



RESULT 2a ERR HDA RDL \,QyAyT+.J 

PARAMETER CAS NO pCi/G (COUNT) pCi/G pCi /G PIERS TEST 

Gross Alpha Alpha 3 1 >` . 3.9 ;5..'::-. 10 :}Q, ,.., 80A 

Grose Beta Beta 21Ci:. r 4.8 6, 10 "'. SOB 

Uranium 233/234 O 3T:,q, 0.14 '' 021 1-. 0.3 -. '., U 

Uranium 235 15117-96-1 0 D13 ;;i 0.027 0:. 1 :, 0.3 U 1 U 

Uranium 238 7440-61-1 0:35- :> 0.14 . U:08: 0.3: U 

Plutonium 238 13981-16-3 -0 006'` 0.022 0 :04:. 0.05 U PU 

Plutonium 239/240 O,00,6^1 0.011 }O_:03 0.05 .,U„ ..',^; PU - 

Americium 241 14596-10-2 O ' OO6r 0.015 `0 03r 0.05 U AM 

Strontium 90 10098-97-2 0.',7 0.84 0..8'.!,.,. 2 '.V Y 

Carbon 14 14762-75-5 4 ?',..'', 9.1 20 50 Vx C 

GAMMA SCAN ANALYSES ark^:; + ;;^, '2 s 

Potassium 40 13966-00-2 17 ,_ 1.2 GAM 

Iron 59 14596-12-4 U^Y,^..,; Pb'^ ',- 0.05Û GAN 

Chromium 51 14392-02-0 GAH 

Cobalt 60 10198-40-0 DJ098;;: 0.056 0.05 GAM 

Zinc 65 

Ruthenium 106 

Cesium 134 

Cesium 137 

13982-39-3 

13967-48-1 

13967-70-9 

10045-97-3 

U., 

U ,„ 

U 

V 

:,0'12:' 

:0:5:':,'-: 

0,.96.>. 

;0'.06 0.05 

^Û 

^V- 

V 

GAM 

GAM 

GAM 

GAM 

Europium 152 14683 -23-9 V ',0.1 0.1 

it. GAN 

Europium 154 15585-10-1 U s. ;

TMA NORCAL 

Lab sample id N212078-02 Client sample id R070B9 



t moisture 1.6 Chain of custody id EFL -1063 

RESULT 2a ERR NDA RDL 

PARAMETER CAS NO pCi/G (COUNT) pCi/G pCi/G FIERS TEST 

Gross Alpha Alpha 4.9 -. 5.9 7' 10 aH.' BOA 

Gross Beta Beta 38.:` 5.2 5`• 10 SOB 

Uranium 233/234 -_ 0:076.. 0.065 '0a -'' 0.3 U 

Uranium 235 15117-96-1 O.dn.'. 0.026 0:1 0.3 U"', 

Uranium 238 7440-61-1 :'' 0':22 i 0.089 '0:,08 0.3 T,s U 

Plutonium 238 13981 - 16-3 0 ' 016 0.027 0,06 0.05 U PU 

Plutonium 239/240 ... 0i`: . :'- 0.022 004 0.05 U PU 

Americium 241 14596 -10-2 O UO3'. 0.030 0.06 0.05 0 P. AM 

Strontium 90 10098-97-2 S.:10 0.64 0 '. 8 2 Y 

Carbon 14 14762-75-5 7.1, 9.1 20 50 Vy„ C 


,.rr+ 

Potassium 40 13966-00-2 >:4 6 9 1.6 e' z-`` GAM 

vt # 

Iron 59 14596-12 4 U , . 'O '6 _' 0.05 àge`, 

GAM 

Chromium 51 14392-02-0 U 3'::: „' B GAM 

Cobalt 60 10198-40-0 u "0:1'.- 0.05 'U: CAM 

Zinc 65 13982-39-3 U,^"' O'3' U GAN 

Ruthenium 106 13967 -48-1 U.;. - ' . i,.< 'U GAM 

Cesium 134 13967-70-9 U 0 1. : , U :, GAN 

Cesium 137 10045-97 3 U 0:1 0 05 UiA GAM 

Europium 152 14683-23-9 U y „ , 0:2 0.1 GAM 

Europium 154 15585-10-1 0.1 'Û'g''^,. : GAM 

Radium 226 13982-63-3 0a37 0.18 a,' GAM 

Thorium 228 14274-82-9 D 4T ': 0.19 GAN 

Thorium 232 7440-29-1 0'-149 ', 0.41 „

Lab sample id N212078-03 Client sample id B07000 


Received 12114/92 Collected 12/09/92 

E moisture 2.8 Chain of custody id EFL-1063 

PARAMETER Cas NO 

RESULT 

PCi/G 

2a ERR 

(COUNT) 

MM 

PCi/G 

RDL 

PCi/G 

5(2^ 

-QHBHI^ 

FIERS TEST 

Gross Alpha Alpha il'.. 6.1 6.:.: 10 80A 

Gross Beta Beta 9.1. 4.0 6 r;z `' 10 80B 

Uranium 233/234 0.29..: 0.13 r 0.'I ,f' 0.3 ':J U 

Uranium 235 15117 -96-1 0.019. 0.037 0.''1. 0.3 U.:" U 

Uranium 238 7440-61-1 O 29:> 0.13 OC1 . '" 0.3 J U 

Plutonium 238 13981-16-3 0 043 0.068 0 :2 ,,. 0.05 )M :. PU 

Plutonium 239/240 0 ;017 0.017 : OiOT Q ' ; 0.05 .c ... ^'' PU 

Americium 241 14596-10-2 70.006: 0.017 i0'04'

BUG 7138 Client Westinghouse Hanford 

Contact Dinkar Kharkar Contract MBH-SVV r069262 

Lab sample id N212078 -04 Client sample id BMW 


Received 12/21 / 92 Collected 12/16/92 

t moisture 10.2 Chain of custody id EFL-1063 

RESULT 2a ERR MDA RDL Qi--v--^ 

PARAMETER CAS NO pCi/G ( COUNT) PCi/G PCi/G FIERS TEST I 

Gross Alpha Alpha ', .3.4 .- 4.5 6..:, 10 !U' 3: BOA 

Grose Beta Beta 30 4.7 5?;: 30 80B 

Uranium 233/234 x. 0.39 0.19 ,:' ;01 0.3 - U I 

Uranium 235 15117 -96-1 0.043 0 . 044 0';2 0.3 II U ^1 

Uranium 238 7440-61- 1 :0.34.' 0.15 0 1.1 0 . 3 ^', 

Plutonium 238 13981 -16-3 0' 0.021 0304 0.05 V, PII 

Plutonium 239/240 O.IS.:. 0.042 0;04 0.05 xr,< PII 

Americium 241 14596-10-2 U:025, 0.019 0 :02 0.05 J AN 

Strontium 90 10098-97-2 ?:.. 0.24 .0'8 2 --Ur Y 

Carbon 14 14762-75-5 4.7"'` 8.3 20'::j, 50 Vy C 


Potassium 40 13966-00-2 13 2.3 GAM 

Iron 59 14596-12-4 II^r: 0.05'II K 

CAM 

Chromium 51 14392-02-0 GAH 

Cobalt 60 10198-40-0 a1::';;.,' 1.3 0.05 ? GAM 

Zinc 65 13982-39-3 U 2''; U GAM 

Ruthenium 106 13967-46-1 U...,,' 41 II 3 . GAM 

Cesium 134 13967-70-9 U-;I: Q:6U_ ^;'' GAM 

Cesium 137 10045-97-3 Q:61.,^. 0.37 :, '':''c'E3 

0.05 ^r'? GAM 

Europium 152 14683-23-9 U ; .',.. 0:'6 0.1 tj'^^ 1, GAN 

Europium 154 15585-10-1 - b :;' ' O ^ : 4 0.1 GAM 

Radium 226 13982-63-3 0':67'' 0.57 , GAM 

Thorium 228 14274-82-9 U 6 ttx^^ GAM 

Thorium 232 7440-29 - 1 U ; 3 Oaf;'; CAM 

Lab id THAN 






U 

I

TMA NORCAL 

REPORTING GROUP 7138 . r 

N212078 OS, 2070D8 

DATA SKEET 


Contact Dinkar Kharkar Contract MEH-SVV-069262 

Lab sample id N212078-05 client sample id B07ODS 



t moisture 4.1 Chain of custody id EFL-1063 

RESULT 2a ERR MDA RDL QUALI 

PARAMETER CAS NO pCi/G (COUNT) pCi/G PCi/G FIERS TEST 

Grose Alpha 

Gross Beta 

Uranium 233/234 

Uranium 235 

Uranium 238 

Plutonium 238 

Plutonium 239/240 

Americium 241 

Strontium 90 

Alpha 

Beta 

15117-96-1 

7440-61 - 1 

13981-16-3 

14596-10-2 

10098-97 -2 

: B.$.:" 

14 e > , ',. 

0 46,_. 

0:034:: 

0.59'? 

0:008; 

O'025 

-0'.008?' 

0002;', 

4.3 

2.8 

0.18 

0.068 

0.21 

0.022 

0.028 

0.022 

0.42 

4 ";'` 

- 01.,. 

0 1"' 

:", 005 

C:«05 

0':04' 

".0? 

10 

10 

0.3 

0.3 

0.3 

0.05 

0- . 05 

0.05 

2 

.;Z— 

': 

e 

.'.0 

^ .- 

U 

U 

U 

U 

80A 

80B 

U 

U 

U 

PII 

PII 

AN 

Y 

Carbon 14 


Potassium 40 

Iron 59 

Chromium 51 

Cobalt 60 

14762-75-5 

23966-00-2 

14596-12-4 

14392-02-0 

10198-40-0 

:^ 

-5 3..:.' 

16 x 

U :.^ ^' 

U 

4 3 .. 

8.7 

1.0 

0.17 

20';.`', 

O`c5.. 

2`r' 

50 

0.05 

0.05 

U 

°pU 

U 

-; 

-. 

C 

GAN 

GAM 

GAM 

GAM 

Zinc 65 

Ruthenium 106 

Cesium 134 

Cesium 137 

Europium 152 

Europium 154 

Radium 226 

Thorium 228 

Thorium 232 

13982-39-3 

13967-48-1 

13967-70-9 

10045-97-3 

14683-23-9 

15585-10-1 

13982-63-3 

14274-82-9 

7440-29-1 

"' 

U 

A 

U 

O s5^ 

1 0 ` 

1 Z ,, 

0.11 

0.12 

0.47 

..' 0 : 13:II".;:` GAH 

0.?3' ',U GAM 

01r' U GAN 

Oc'09. 0.05 -,V GAN 

01'`. 0.1 "V GAM 

0.1 U GAM 

GAN 

GAM 

GAM 

Lab id THAN 

Protocol WHC-HRIS 


Page 5 Form DM-DS 

SUN1MAAY DATA SECTION Version 2.23 

Page 18 Report date 03/24193 

•J / 

V

PARAMETER 

:K211078-;-06 

SDG 7138 





3 moisture 2.3 

Gross Alpha 

Gross Beta 


Uranium 235 

Uranium 238 

Plutonium 238 


Americium 241 

Strontium 90 

Carbon 14 


Potassium 40 

Iron 59 

Chromium 51 

Cobalt 60 

Zinc 65 

Ruthenium 106 

Cesium 134 

Cesium 137 

Europium 152 

Europium 154 

Radium 226 

Thorium 228 

Thorium 232 

RESULT 2a ERR 

CRS NO pCi/G (COUNT) 

Alpha 

Beta 

15117-96-1 

7440-61-1 

13981-16-3 

14596-10-2 

10098-97-2 

14762-75-5 

13966-00-2 

14596-12-4 

14392-02-0 

10198-40-0 

13982-39-3 

13967-48-1 

13967-70-9 

10045-97-3 

14683-23-9 

15585-10-1 

13982-63-3 

14274-82-9 

7440-29-1 

THA NORCAL 


DATA SHEET 

89 

0'^`d2 

O 

0006::,; 

-0 004' 

-370: 

7`7 

U.i 

Vi;' 

vy 

Ux 

II 

0 36s^' 

5.5 

3.7 

0.19 

0.044 

0.19 

0.024 

0.024 

0.020 

0.51 

8.3 

0.85 

0.078 

0.069 

0.15 

^^f a '^ z p 

L 

^ - B07QD9^ 

client Westinghouse Hanford 

Contract MBH-Syy-069262 

Client sample id BO7OD9 

Matrix SOIL 


Chain of custody id $PL-1062 

MM RDL 

pCi/G pCi/G 

6bs' ' 10 

10 

01; 0.3 

Oil- 

V.SO 

0.3 

0.3 

0.'04 ,- 0.05 

b'04 0.05 

0104> - 0.05 

2 

20 - so 

n , s 

0.05 

5: 0.05 

4

TMA NORCAL 

Lab sample id N212078-07 Client sample id B070FO 


Received 12121/92 _ Collected 12/17/92 

! moisture 1.9 Chain of custody id BFL-1062 

RESULT 2a ERR MDA RDL 

PARAMETER CAS No PCi/G (COUNT) PCi/G pCi/G 

Gross Alpha 

Gross Beta 


Uranium 235 

Uranium 238 

Plutonium 238 


Americium 241 

Strontium 90 

Carbon 14 


Potassium 40 

Iron 59 

Chromium 51 

Cobalt 60 

Zinc 65 

Ruthenium 106 

Cesium 134 

Cesium 137 

Europium 152 

Europium 154 

Radium 226 

Thorium 228 

Thorium 232 

Alpha 

Beta 

15117-96-1 

7440-61-1 

13981-16-3 

14596-10-2 

10098-97-2 

14762-75-5 

13966-00-2 

14596-12-4 

14392-02-0 

10198-40-0 

13982-39-3 

13967-48-1 

13967-70-9 

10045-97-3 

14683-23-9 

15585-10-1 

13982-63-3 

14274-82-9 

7440-29-1 

4 6.1 

04811..; 0.16 

:.,:110:078' - 0.053 

0.33,`x' 0.13 

:=Q`003' 0.024 

0:012:,. 0.018 

=0:012' 0.023 

-0 19 ,'`: 0.28 

8.7 

k: 

y k 

V. 

U: ?? 

U 

U 

0.73 

0.068 

0.046 

0.16 

{ 

9' .. 

0:3 

OY'' 

0::05 

0:;03' 

0'105' 

6r:9 ' .. 

r .'0.04 

0'1 , 

0:3. 

0.04 

O c 03 

0':07" 

;0:05 

10 

10 

0.3 

0.3 

0.3 

0.05 

0.05 

0.05 

2 

50 

0.05 

O.OS 

0.05 

0.1 

0.1 

80A 

80B 

U ^( 

U 

U 

PU 

PU 

AM 

Y 

C 

GAN 

GAN 

GAN 

GAN 

GAN . 

GAN 

GAN 

GAM 

GAN 

GAN i 

GAN I 

GAN 

Lab id TMAN 

Protocol WHC-HEIS 1 

DATA SHEETS Version y D 

Page 7 Form pw_ns t 

SUMMARY DATA SECTION Version 2,23 


F 

GAN f 

I

IA 


11 

11 

it 

11 

10 

42 

it 

li 

11 

11 

li 

11 

11 

11 

li 

11 

11 

11 

11 

li 

it 

11 

11 

11 

11 

it 

it 

11 

it 

li 

li 

11 

11 

000005 


I I 

I B07Q93 I 

Lab Name: TMA/ARLI Contract: NHC I I 

Lab Code: TM?aA_ Case No.: 12047 SAS No.: NA SDG No.: NA_ 


Sample wt/vol: 5.0 WML) G 

Level: (low/aed) LOW_ 

% Moisture: not doe. 6 


Soil Extract Volumes (UL) 



74-83-9 --------- Bromomethans 


75-00-3 --------- Chloroethane 


67-64-1---------Acetone 


75-35-4---------1,1-Dichloroethene 

75-34-3---------1,1-Dichloroethane 

540-59-0 -------- 1,2-Dichloroethene (total)_ 

67-66-3---------Chloroform 


78-93-3 --------- 2-Butanone 



75-27-4 --------- Bromodichloromethane 

78-87-5 --------- 1,2-Dichloropropans 

10061-01-5 ------ cis-1,3-Dichloropropens 

124-48-1 -------- Dibromochloromethans 


71-43-2---------Benzene 


75-25-2 --------- Bromoform 

108-10-1 -------- 4-Nethyl-2-Pentanons 

591-78- 6 -------- 2-Hexanone 

127-18-4 -------- Tetrachloroethens 

79-34-5 --------- 1,1,2,2-Tetrachloroethans 

108-88-3--------Toluene 


100-41-4 -------- Ethylbenzene 

133 

Lab Sample ID: A212047-OIA 

Lab Pilo ID: 


Date Analysed: 





U I 

U I 

U I 

U I 

U I l?b 

U I 

U U I 

U I 

U I 

U I 

U I 

U I 

U I 

U I 

U I 

FORK I VOA 3/90. 

U 

U 

U UUUUUU

lE 

EPA BMW 



I B07Q93 I 

Lab Name: TMA/ARLS Contract: WNC I 

Lab Code: TKALa_ Case No.: 12047 SAS No.: NA SDG No.: Imo_ 

Matrix: ( soil/eater) SOIL 

Lab Sample ID: A212041-0 1A 

Sample wt/vol: 5.0 (g/mL) Gc_ Lab File ID: 21221R03 

Level: ( low/mad) Imo_ 

i Moisture: not doe. _6 

GC Column: PACK iD: 2 2 00 (mm) 


Number TICS found: I 







i I i 

I CAS NUMBER I COMPOUND NAME I RT 

I 1. (UNKNOWN ALKA E i 16.53 

I I I 

FORM I-VOA-TIC 

EST. CONC. Q I 

^B 

6- 7 I 

I 

I 

3/90

lA EPA SSW j. 


Lab Names TNA/ARLS Contract: WHC I 

B07094 

Lab Code: TKAL& _ Case No.: 12047 SAS No.: NA SDG No.: NA 



Level: (low/med) TAW 

t Moisture: not dec. 4 


Lab Sample IDs 

Lab Pilo IDs 







I 

I 

74-87-3 --------- Chloromethans I 10 IU 

74-83-9 --------- Bromomethane 1 10 III 

75-01-4---------Vinyl Chloride 1 10 III 

75-00-3 --------- Chloroothane 1 10 IU 


67-64-1---------Acetone 1 41 WtA 

75-15-0---------Carbon D sulf de 1 10 III 

75-35-4 --------- 1,1-Dichloroethans i 10 III 

75-34-3 --------- 1,1-Dichloroethans I 10 III 

540-59-0 -------- 1,2-Dichloroethens (total)_I 10 III 

67-66-3---------Chloroform 1 10 IU 

107-06- 2 -------- 1,2-Dichloroethane 1 10 IV 

78-93-3 --------- 2-Butanone 1 10 IU 

71-55-6 --------- 1,1,1-Tri lor I 10 IU" 

56-23-5---------Carbon Tetrachloride 1 10 IV 

75-27-4 --------- Bromodichloromethans I 10 III 

78-87-5 --------- 1,2-Dichloropropane ( 10 1V 

10061-01-5 ------ cis-1,3-Dichloropropens 1 10 1U 

79-01-6 --------- Trichloroethene 1 10 III 

124-48-1 -------- Dibromochloromeans I 10 III 

79-00-5 --------- 1,1,2-Trichloroethane 1 10 1U 

71-43-2---------Benzene 1 10 III 

10061-02-6 ------ trans-1,3-D chloropropens 1 10 IV 

75-25-2 --------- Bromoform 1 10 IV 

1 108-10- 1 -------- 4-Methyl-2-Pentanons 1 10 III 

1 591-78-6 -------- 2-Hexanone 1 10 IV 

1 127-18-4 -------- Tatrachloroethens 1 10 1U 

1 79-34-5 --------- 1,1,2,2-Tetrachloroethane 1 10 1U 

1 108-88-3--------Toluene I 10 1U 

1 108-90-7 -------- Chlorobanzene 1 10 IV 

i 100-41-4 -------- Ethylbenzene 1 10 IU 

i 100-42-5--------Styrene ( 10 IU 

1330-20-7 ------- Xylone (tots ) i 10 IV - 

FORK I.VOA 3/90

1a aPQ QDef^Bxo. 



I B07Q94 

Lab Name: TMA/ARLI Contract: }HC I I 

Lab Code: ' HAL&_ Case No.: 12047 SAS No.: NA SDG No.: M_ 


Sample wt/vol: 5 . 0 (g/mL) Q_ Lab File ID: 21221804 

Le vel: (low/mad) Imo_ Date Received: 12/14/92 



GC Column: PACE ID: 2.00 (mm) Dilution Factor: 2.0 

Soil Extract Volume: (uL) Soil Aliquot Volumes (uL) 


Number TICS found: _l (ug/L or ug/Kg) UGZKQ 

ICAS NUMBER COMPOUND NAME RT I EST. CONC. I Q 

I!!!!!lffi!! S 1 8 !!i!!i!!!!!!!!i!!!liii!! I i^ I Biiiiiiiili0 I ea8i 

( UNKNOWN ALKANE I 16.58 I 5' IJ 

1 I I I I 

41 1 1^3 

FORM I VOA-TIC 3/90

IA 


Lab Naas: TMA/ARLI Contract: WHC I 

000009 






I 

I B07095 

Lab Coda: TMALN _ Cass No.: 12047 SAS No.: NA SDG No * : NA 


Sample wt/vol: 5.0 (g/aL) 0_ 

Level: (low/med) UHL- 

t Moisture: not doe. _5 

GC Column: PACK IDs 2.00 (ma) 



74-87-3 --------- Chloromethana 


75-00-3 --------- Chloroethane 

75-09-2---------Methylene Chlor a 

67-64-1---------Acetone 

75-15-0---------Carbon m D sud—e 

75-35-4 --------- 1,1-Dichloroethens 

75-34-3 --------- 1,1-Dichloroethani 

540-59-0 -------- 1,2-Dichloroethene 


78-93-3 --------- 2-Butanone 



75-27-4 --------- Bromodichloromethans 


10061-01-5 ------ cis-1,3-Dichloropropens 

79-00-5---------1,1, 

10061-02-6------trans-1, 

75-25-2 --------- Bromofor 

108-10-1--------4-Methyl 

591-78-6--------2-Hexane 

79-34-5---------1,1,2, 

108-88-3 -------- Toluer 

FORM 1. VOA 

Lab Sample IDs A212047-05A 

1.0 

Soil Aliquot Volumes _(UL) 


(ug/L or ug/Rg) UG /KG4 

11 IU 

li IU 

11 III 

11 IU 

24 IWok 

11 IU 

it IU 

]a IU 

11 IU 

11 IU 

11 IU 

11 IU 

li IU 

11 IU 

11 IU 

it IU 

li IU 

11 IU 

11 IU 

11 IU 

11 IU 

11 IU 

ll IU 

11 IU 

11 IU 

11 (U 

it IU 

11 IU 

11 IU 

11 IU 

11 IU 

11 IU 

3/90 

'\9 

4A/s

is 




i 

000010 


807Q9S 

Lab Code: TNAL&Case No.: 12047 SAS No.: NA SOO No.: Nom_ 

Matrix: ( soil/water) SOIL Y Lab Sample ID: A212047-05A 

Sample wt/vol: 5.0 (q/mL) G_ Lab File ID: 21221R09 





Number TICS found: . 0 




1.0 



(ug/L or ug/Kq) UG/KG 

CAS NUMBER COMPOUND NAME RT EST. CONC. Q 

^ 6 y/1 A? 

FORM I' 'VOA-TIC 3/90.

1A EPA ;0. 


I I 

I B07Q96 I 


Lab Code: TMALA Cass No . t 12047 SAS No.: NA SDG No.: H_ 


Sample wt/vol: 5.0 (g/sL) S^ 

Level: ( low/med) jgM 


GC Column: PACK IDS 2 . 00 (mm) 


Lab Sample ID: A212047-0SA 

Lab File ID: 

21221810 






CAS NO. COMPOUND (ug/L or ug/Rg) UG/XG Q 

74 -87-3 --------- 10 IV 1 

74-83-9 --------- Bromomethane 1 10 III 1 '''ttt 

75-01-4---------Vinyl Chlorides 1 10 III 1 y 

75-00-3 --------- Chloroethane 1 10 I `1 fff^^r 

III 

75-09-2---------Methylene Chlor do 1 3 IJ I 

67-64-1---------Acetone 1 19 IAA 

75-15-0---------Carbon Digulfide 1 10 I U 1 

75-35-4 --------- 1,1-Dichloroethens 1 10 III 1 

75-34 -3 --------- 1,1-Dichloroethans 1 10 III 1 

540-59 -0 -------- 1,2 -Dichiorosthene (total)_I 10 III 1 

67-66-3---------Chloroform 1 10 I V 1 

107-06-2 -------- 1 , 2-Dichloroethans 1 10 JU 1 

78-93-3 --------- 2-Butanone ( 10 IV 1 

71-55-6 --------- 1,1,1-Tric lorosthans 1 10 I II 1 

56-23-5---------Carbon Tetrachloride 1 10 III 1 

75-27-4 --------- Bromodichloromethans 1 10 I V 1 

78-87-5 --------- 1,2-Dichloropropans 1 10 III 1 

10061-01-5 ------ cis-1,3-Dichloropropene 1 10 ID III. 

1 

79-01-6 --------- Trichioroetheno 1 10 

1 

III_ 

124-48 -1 -------- Dibromochloromet ane 1 10 

1 

79-00-5 --------- 1,1,2-Trichloroethans i 10 I V 1 

71-43-2---------Benzene i 10 III 1 

------ -Dichloropropene 

c oropropene 1 10 I V 1 

75-25-2 --------- Bromoform 1 10 IU I 

108-10-1 -------- 4 -Methyl-2-Pentanone 1 10 IV 1 

591-78-6 -------- 2-Hexanons I 10 III 1 

127-18-4 -------- Tetrachloroe ene 1 10 IV 1 

79-34-5 --------- 1,1,2,2-Tatrachloroethane 1 10 I V 1 

108-88-3--------Toluene I 10 JU 1 

108-90-7 -------- Chlorobenzene 1 10 IV 1 

100-41-4 -------- Ethylbenzene i 10 III 1 

100-42-5--------Styrene 1 10 IV 1 

1330-20-7 ------- Xyiene (total) 1 10 I V I 

FORM I .VOA 3/90.

G 

Lab Name: TNA/ARLi 

lZ 

000012 


VOLi1TILE ORGANICS ANALYSIS DATA SHEET 


Lab Code: TKAId_ Case No.: 12047 


Sample wt/vol: --5 ,0 (9/ML) Q_ 

Level: ( low/med) LOW 

i Moisture: not dec. _ 4 




Contract: WHC i 

I B07Q96 

SAS No.: NA SDG No.: Imo_ 


Lab Pilo ID: 2122IR10 







CAS NUMBER COMPOUND NAME RT I EST. CONC. Q I 

ass:^:s::as^â I a^^^^smm^^^:ss I ^^saô I âoasâsss I sms I 

I I I I I 

Y102 

FORS I:VOA-TIC 3/90 

I 

I

lA 


000013 


I I 

I B07098 


Lab Code: TKALa_ Case NO.: 12047 SAS No.: NA SDG No.: Ike 







Lab File ID: 






GAS NO. COMPOUND (ug/L or ug/Kg) VG /KG 0 

I 

I 


10 IU 

74-83-9 --------- Bromomethane 1 10 IV 

75-01-4---------Vinyl Chloride 1 10 IU 

75-00-3 --------- Chloromthans ( 10 IV 

75-09-2---------Methylene Chloride 1 2- IJ 

67-64- 1---------Acetone i 17 

75-15-0---------Carbon Disulfide 1 10 U 

75-35-4 --------- 1,1-Dichlorosthens 1 10 III 

75-34-3 --------- 1,1-Dichloroethans I 10 IV 

540- 59-0 -------- 1,2-Dichloroethene (total)_I 10 III 

67-66-3---------Chloroform 1 10 1V 

107-06-2 -------- 1,2-Dichloroothane 1 10 1U 

78-93-3 --------- 2-Butanone 1 10 1V 

71-55-6 --------- 1,1,1-Trichloroethene 1 10 1U 

1 56-23-5---------Carbon Tetrachloride 1 10 1U 

175-27-4 --------- Bromodichloromethane 1 10 IU 

1 78-87-5 --------- 1,2-Dichloropropane 1 10 IU 

1 10061-01-5 ------ cis-1,3-Dichloropropene 1 10 1U 

1 79-01-6 --------- Trichloroethene 1 10 1U 

1 124-48-1 -------- Dibromochlorome ane 1 10 1U 

1 79-00-5 --------- 1,1,2-Trichloroethens 1. 10 III 

171-43-2--------- Benzene 1 10 IV 

10061-02-6 ------ trans-1,3 -D ch oropropene 1 10 IU 

1 75-25-2 --------- Bromoform 1 10 1U 

1 108-10-1 -------- 4-Methyl-2-Pentanons 1 10 1U 

1 591-78-6 -------- 2-Hexanone 1 10 1U 

1 127-18-4 -------- Tetrachloroethene 1 10 1U 

179-34-5 --------- 1,1,2,2-Tetrachloroethans 1 10 1U 

1 108-88-3--------Toluene 1 10 1U 

1 108-90-7 -------- Chlorobenzene 1 10 1U 

1 100-41-4 -------- Ethylbenzena 1 10 IV 

1 100-42-5--------Styrene 1 10 IV 

1 1330-20-7 -------Xylene (total) 1 10 IV 

1.0 

U 

4191 

FORM I VOA 3/90

000014 

lE EPA SAXPLE 110. 

VOLATILE ORGANICS ANALYSIS DATA SNSET 

TENTATIVELY IDENTIFIED COMPOUNDS I i 

i B07Q9i I 

Lab Name: TMA/ARLi Contract: WHC I I 

Lab Codes TMAJA Case No.: 12047 SAS No.: NA SDG No.: Nk 



Level: ( low/mad) LOW 

i Moisture: not dec. 4 



I 



Date Analyzed: 1,/21/92 




(ug/L or ug/Kg) UGIKG 

I CAS NUMBER COMPOUND NAME I RT I EST. CONC. I Q 

iiMMWWWi iiiii^ I î I iiiiiiiiiiiii I 

I 

FORM I VOA-TIC 3/90

000015 

lA EPA SAMPLE NO. 

VOLATILE ORGANICS ANALYSIS DATA SKEET 

I I 

I B07Q99 

Lab Name: TKA/ARLT Contract: WHC I I 

Lab Code: TMAja, Case No.: 12047 SAS No.: K& SDG No.: MA 



Level: ( low/sed) Ig_ 


GC Column: PACK ID: 2.00 (=) 

Soil Extract Volute: (uL) 


74-83-9 --------- Bromomethane 

75-01-4-------- -Vinyl Chloride 

75-00-3 --------- Chloroethane 

75-09-2---------Methylene chloride 

67-64-1---------Acetone 

75-15-0---------Carbon D Gulf de 


75-34 -3 --------- 1,1-Dichloroethane 

540-59-0 -------- 1,2 -Dichloroethene (total)_ 

67-66-3---------Chloroform 


78-93-3 --------- 2-Butanone 

71-55-6---------1,1,1 -Trick oroethane 






79-00-5 --------- 1,1,2 -Trichloroethans 

71-43-2-------- -Benzene 

10061 -02-6 ------ trans -1,3-D chloropropens 

75-25-2 --------- Bromoforx 

591-78-6-------- 

79-34 -5-- ------ 1,1,2,2-Tatrachloroethans 

108-88-3--------Toluene 


100-41-4 -------- Ethylbenzene 

100-42-5--------Styrene 

1330-20-7 ------ -Xylene (total) 





soil Aliquot Volumes (uL) 


(uq/L or ug/Rg) UG/KG Q 

I 

10 ,U 

10 ,U 

10 IU 

13 ^J 

27 )BAG( 

10 ,U 

10 IU 

10 III 

10 IU 

10 IU 

10 ,U 

10 ,U 

10 III 

10 IU 

10 IU 

10 IV 

10 III 

10 III 

10 ,U 

10 IU 

10 III 

10 IV 

10 IU 

10 (U 

10 IU 

10 III. 

10 IV 

10 IV 

10 IV 

10 IU 

10 IV 

10 IV 

q/y 

FORM I VOA 3/90

000016 

1E EPA SAMPLE NO. 



B07Q99 

Lab Naze: TMA/ARLI Contracts WHC 

Lab Code: TMALA_ Case No.: 12047 SAS No.: NA SDG No.: MA 


Sample wt/vol: 5.0 (VILL) G Lab File ID: 21221RIl 


% Moisture: not dec. _ 4 Date Analyzed: 12/21/92 

GC Column: PACK ID: 2.00 (UK) Dilution Factor: 1..0 

Soil Extract Volumes (uL) Soil Aliquot Volumes (UL) 


Number TICs found: _ 0 (uq/L or uq/Kq) UQ/KG 

CAS NUMBER I COMPOUND NAME RT EST. CONC. Q 

I ii iiiiiilil 

q /f #3 

FORK I VOA-TIC 3/90

1A 


000017 

EPA SAMPLE MO. 

I 

I 

Lab Name: TKA/ARLI Contract: WHC 

I B07QBO 

I 

I 

I 

Lab Code: TMAIA Casa No.: 12047 SAS No.: NA SDG No.: MR 


_ 


Sample wt/vol: 5.0 (9/AL) Q._ Lab File ID: 

Le vel: (low/mad) TOW Date Received: 

% Moisture: not doe. _3 Data Analyzed: 




CAS NO. COMPOUND (u9/L or u9/R9) UG/RG Q 


I 

I 

10 III 

74-83-9 --------- Bromomethane ( 10 IU 

75-01-4---------Vinyl Chloride 1 10 IU 



67-64-1---------Acetone 1 35 IXA 

75-15-0---------Carbon D sul! da 1 10 III 

75-35-4 --------- 1,1-Dichloroethene i 10 III 

75-34-3 --------- 1,1-Dichloroethane I 10 IU 

540-59-0 -------- 1,2-Dichloroethene (tota ` I 10 III 

67-66-3---------Chloroform 1 10 III 

107-06-2 -------- 1,2-Dichloroethana 1 10 IV 

78-93-3 --------- 2-Butanone 1 10 IV 

71-55-6---------1,1,1-Trick oroethans I 10 IV 

56-23-5---------Carbon Tetrachloride I 10 1V 

75-27- 4 --------- Bromodichloromethana I 10 1U 

78-87-5 --------- 1,2-Dichloropropane 1 10 III 

10061-01-5 ------ cis-1,3-Dichloropropene 1 10 III 

79-01-6 --------- Trichloroothene I 10 IU 

124-48-1 -------- Dibromochloromeane 1 10 III 

79-00-5 --------- 1,1,2-Trichloroethane 1 10 IV 

71-43-2---------Benzene 1 10 III 

10061-02-6 ------ trans-1,3-D chloropropens 1 10 IV 

75-25-2 --------- Bromoform 1 10 III 

108-10-1 -------- 4-Methyl-2-Pentanone i 10 1D 

591-78-6 -------- 2-Hexanone 1 10 IV 

127-18-4 -------- Tetrachloroethene 1 10 1u 

179-34-5 --------- 1,1,2,2-Tatrachloroethane 1 10 III 

1 108-88-3--------Toluene 1 10 ID 

1 108-90-7 -------- Chlorobenzene 1 10 Ju- 

1 100-41-4--------Ethylbenzene 1 10 IV 

1 100-42-5--------Styrene 1 10 III 

1 1330-20-7 ---- ---Xylene (total) 1 10 IV 

FORM I VOA 3/90 

0 ,4111

Lab Name: 

Lab Code: ^_ Case No.: 12047 


Sample wt/vol: 5:0 (9/ML) 


i Moisture: not doe. 3 

GC Column: PACK ID: 2.00 (IM) 


Number TICS found: I 

VVVV1O 

1E 



TENTATIVELY IDENTIFIED C014POUNDS 

I807Q80 I 

Contract: WHC I 1 



Q_ Lab File ID: 21221805 




Soil Aliquot Volumes (UL) 



CAS NUMBER COMPOUND NAME RT I EST. CONC. I Q 

I!!!ii!!!!alliii I iili!!!lilii!!!!i!i !!!!i I iliilOil iiiili!!!!!SI 0!i! 

I 1. (UNKNOWN ALKANE I 16.53 ( 5 IJ 

I I I I I 

FORK I VOA-TIC 3/90

1,^► 

VOLATILE ORGANICS ANALYSIS DATA SHEST 

EPA sA^P^.s 019 110. 

I B07QB1 

I 

I 


Lab Coda: TKALA Case No.: 12047 SAS No.: NA SDG No.: KA 


Sample wt/vol: 5.0 (VUL) G 



GC Column: PACK ID: 2.00 (sm) 



74-83-9 --------- Bromomethane 


75-00-3 --------- Chloroethane 

75-09-2---------Methylene Ch or e 

67 -64-1---------Acetone 


75-35-4 --------- 1,1-Dichioroethene 

75-34 -3 --------- 1,1-Dichloroethane 

540-59 -0 -------- 1,2-Dichloroethene (total)_ 

107-06-2 -------- 1,2-Dichlo 

78-93-3 --------- 2-Butanona 

71-55-6 --------- 1,1,1-Tric 

56-23-5---------Carbon Tat 

75-27-4 --------- Bromodichl 

79-00-5 --------- 1,1,2 -Trichloroethane 

10061-02-6------trans-1,3. 

75-25-2 --------- Bromolorm 

59 

-- - -------- 

79 -34-5---------1,1,2,2 

108-90 

100-41 

100-42 

1330-2 

FORK I VOA 






Soil Aliquot volumes (uL) 


(uq/L or uq/Kq) UG/KG Q 

10 III 

10 III 

10 III 

10 III 

10 IJ 

25 

10 U 

10 III 

10 IU 

10 III 

10 III 

10 III 

10 III 

10 IV 

10 III 

10 IV 

10 III 

10 III 

10 IV 

10 III 

10 IV 

10 IV 

10 IV- 

10 IV 

10 IV 

10 IV 

10 III 

10 III 

10 IV 

10 III 

10 III 

10 IV 

10 IV 

u IÂ 

g111, 

3/90 

t 

i

Lab Hama: TMA/ARLI 

lE 



Lab Code: 'ELK Case No.: 12047 


Sample wt/vol: 5.0 (g/nL) 






Contract: gHC 

0000__°0 


B07QB1 



s^ Lab File ID: 21221R0B 







CAS NUMBER COMPOUND NAME RT I EST. CONC. ( Q 

^sa^^^ss^:saw I :âamasâââs^âa: 

1. UNKNOWN ALKANE 16.58 6° j J 

FORM I.VOA-TIC 3/90

lA 


Lab Name: TMA/ LT Contract: WHC 

10 

10 

10 

10 4 

27 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

000021 


I B07QB2 

Lab Code: TKAIA_ Case Noes 12047 SAS Noes NA SDG No.: Nom_ 

a 

matrix: (soil/water) SOIL 


Sample wt/vol: 5.0 (g/aL) Q_ 


t Moisture: not doe. 4 





74-83-9 --------- Bromomethane 


75-00-3---------Chloroethane 

75-09-2---------methylene Chloride 

67-64-1---------Acetone 


75-35-4---------1,1-Dichloroethene 


540-59-0--------1,2-Dichloroethena (total)_ 

67-66-3---------Chloroform 


78-93-3 --------- 2-Butanone 




78-87-5---------1,2-Dichloropropane 


79-01-6 --------- Trichloroethene 

124-48-1 -------- Dibromochloromet ane 


10061-02-6------trans-1, 

Lab File ID: 

591-78-6 -------- 2-Hexanone 

127-18-4 ------- Tetrachloroethene 

79-34-5 --- -- ---- 1,1,2,2-Tetrachloroetha s 

108-88-3--------Toluene 

108-90-7 ------- Chlorobenzene 

100-41-4 ------- EthVibenzene 

FORM I VOA 







F UUUUUUUUUUUUUUUUUUU 

H 

A6 

W9/ 

3/90

Lab Name: 

is 



I 807QB2 


Lab Cods: Cass No.: 12047 


Sample wt/vol: 5.0 WUL) Q_ 

Laval: (low/mod) L40W 

t Moisture: not dec. _}, 




000022 



Lab Sample ID: A212647-OBA__ 


Data Received: 12/14/92 





(uq/L or uq/Kq) UG/KG 

I I I I 


^s^sss:isssssssslsss::sssssss:sss::asssss::ssl^ss:::asl (sssa 

I I I ^ 


r 

3/90

000023 

lk EPA SAMPLE NO. 


I I 

I B07QB3 I 

Lab Name: TMA/ARLI Contract: WMC I I 


!Matrix: ( soil/water) SOIL 

Sample wt/vol: 5.0 (q/mL) G_ 

Level: (low/mod) TON 

% Moisture: not doe. 17 



Lab File ID: 21221RI3 




Soil Extract Volume: (UL) Soil Aliquot Volume: (UL) 





75-00-3 --------- Chloroethane 


67-64-1---------Acetone 

75-15-0---------Carbon D Sulf de 



540-59-0 -------- 1,2-Dichloroethene (total)_ 

107 -06-2 -------- 1,2-Dich 

78-93-3 --------- 2-Butano 

71-55-6---------1,1,1-Tr 

56-23-5---------Carbon T 

75-27-4 --------- Bromodic 

78 -87-5 --------- 1,2-Dich 

10061-01-5------cis-1,3- 

79-00-5 --------- 1,1,2-Trichloroothane 

71-43-2---------Benzene 


75-25-2 --------- Bromoform 

108-10-1 -------- 4-Methyl-2-Pentanone 

591-78-6 -------- 2-Hexanone 

127-18-4 -------- Tetrachloroethene 


100-41-4 -------- Ethylbenzene 

100-42-5--------Styrene 

1330-20-7 ------- Xylene (iota ) 

FORM I VOA 

1 

12 IU 

12 IU 

12 IU 

12 IU 

9 IJ 

44 

12 U 

12 1U 

3.2 JU 

12 III 

12 IU 

12 IU 

12 III 

12 IU 

12 III 

12 IU 

12 IU 

12 IU 

12 III 

12 IU 

12 III 

12 III 

12 III 

12 IU° 

12 IU 

12 IU 

12 IU 

12 IU 

12 IU 

12 IV 

12 IU 

12 III 

12 1U - 

I I 

3/90 

V 1,^

is 




I 


I 807Q83 

I 

I 

I 

Lab Code: TMATA Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 5.0 (g/mL) G_ Lab File ID: 2122IR13 

Level: (low/med) jDJL_ Date Received: 12/14/92 

i Moisture: not dec. r17 Date Analyzed: 12/21/92 


soil Extract Volume: (uL) Soil Aliquot Volumes _(UL) 



CAS NUMBER COMPOUND NAME RT EST. CONC. Q 

sss^êaas:::^^ I ^::amass::^^âaaasâarô^s^s I samaa I aaaaaa I w^ 

I I I I 


0 

3/90

000025 

IA EPA SAMPLE NO. 


I i 

I B07QBS I 


Lab Code: TMALA _ Case No.: 12047 


Sample wt/vol: 5.0 (g/AL) G 

Level: (low/med) UM_ 


GC Column: PACK ID: 2.00 (ma) 

Soil Extract Volute: (uL) 



Lab File ID: 

21221R14 




1.0 

soil Aliquot Volume: (uL) 


CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 

74-87-3 --------- Chloromethane I 11 I U 



75-00-3 --------- Chloroethane 1 it IU 

75-09-2---------Methylene chloride I 6 IJ_/ 

67-64-1---------Acetone I 23 ISl 

75-15-0---------Carbon Disulfide I 11 I 

75-35-4 --------- 1,1-Dichloroethene I 11 I V 

75-34-3 --------- 1,1-Dichloroethane I 11 I V 

540-59-0 -------- 1,2-Dichloroethene (total _i 11 I U 

67-66-3---------Chloroform I li I U 

107-06-2--------1,2 -Dichloroethane 1 li III 

78-93-3---------2-Butanone 1 11 I U 

71-55-6 --------- 1,1 , 1-Trichlorcethane I 11 IV 

56-23-5---------Carbon Tetrachloride 1 11 IU 

75-27-4---------Bromodichloromethans 1 11 

78-87-5 --------- 1,2-Dichloropropane I it III 

10061-01-5 ------ cis-1,3-Diohioropropene 1 li IU 

79-01-6 --------- Trichloroethens I II. III 

124-48-1 -------- Dibromochloromethane ( it IV 

79-00-5 --------- 1,1,2 -Trichioroethans 1 it III 

71-43-2---------Benzene 1 11 III 

10061-02-6 ------ trans-1,3-D ch oropropens I 11 IV 

75-25-2 --------- Bromofora 1 11 III 

108-10-1 -------- 4-Nethyl-2-Pentanone 1 11 IU 

591-78-6 -------- 2-Hexanons 1 11 IU 

127-18-4 -------- Tatrachloroethene 1 11 IU 

79-34-5 --------- 1,1,2,2-Tetrachloroethane I 11 IV 

108-88-3--------Toluene 1 11 IV 

108-90-7 -------- Chlorobenzene 1 11 IV 

100-41-4 -------- Ethylbenzene 1 11 III 

100-42-5--------Styrene 1 11 I U 

1330-20-7 ------- Xylene (total) I 11 IV 

FORM I VOA 

III_ 

3/90 

C f^S

lE 



00002E 


I B07QBS I 

Lab Name: TMA/ARLI Contract: W(C I I 

Lab Cods: TMALA Cass No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: S.0 (VRL) Q _ lab File ID: 2122IR14 

Level: (low/mad) IOW Date Received: 12/14/92 

t Moisture: not dec. _ 5 Date Analyzed: 12/21/92 

GC Column: PACK ID: 2.00 (ma) Dilution Factor: 1.0 



Number TICS found: _ 0 (ug/L or ug/Kg) UGIKG 

I I I 

I CAS NUMBER I COMPOUND NAME I RT EST. CONC. Q 

I 

^âs^^sâ:sus:tea I sus sass I s^sâ^^ 

I I I 

FORM I.VOA-TIC 

1 

3/90

1A 


000027 


I ( 

( Bo7QB9 

Lab Names TNA/ARLi Contract: WHC ( l 

Lab Code: TNALA Case No.: 12047 SAS No.: NA SDG NO.: Nom_ 


Sample wt/vol: 5.0 (VAL) Q__ 


i Moisture: not dec. _4 


Soil Extract Volumes (uL) 



75-00-3 --------- Chlorcethane 

75-09-2---------Methylene Chlor de 

67-64-1---------Acetone 

75-15-0---------Carbon D suit e 


75-34-3 --------- 1,1-Dichloroethans 

540-59-0 -------- 1,2-Dichloroethens (total) _ 

67-66-3---------Chloroform 


78-93-3 --------- 2-Butanone 


56-23-5---------Carbon Tetrachloride- 

75-27-4 --------- Bromodichloromethano 



124-48-1 -------- Dibromoc 

79-00-5---------1,1,2-Tr 

71-43-2---------Benzene 

10061-02-6------trans-1, 

59 

79-34-5---------1,1,2, 

108 -88-3 -------- Toluen 

100-4 

s 

FORK I.VOA 


Lab File ID: 21221RIS 


Date Analyzed: 12L/92 



=CENTRATION UNITS: 

(ug/L or ug/Kg) US/KG 4 

10 III 

10 Iv 

10 I v 

10 Iv 

I 

I 

1 

22 1J (^ 1 R0 

IV 

10 

10 I II 

0 

1Iv 

10 III 

I 

I 

10 Iv I 

10 I II 

I 

10 

10 

10 

10 

10 

10 

10 

10 

10 

III 

I v I 

Iv 

III 

III 

III 

III 

III 

Iv 

I 

I 

I 

I 

I 

I 

10 

10 I v I 

10 

10 

III 

Iv 

10 

10 

2 

10 

Iv 

Iv 

IJ 

1v 

I 

1 

I 

I 

10 

10 

10 

1v 

1v 

III , 

I 

I 

I 

I 

I 

I 

I 

I 

3/90 

qP

lE 



Lab Name: SHA/ARLI Contract: WRC 

EPA SAMPLE 90:8 

I I 

I B07QB9 I 

I I 

Lab Code: THALA Case No.: 12047 SAS No.: NA SDG No.: Nom_ 

Matrix: ( soil/eater) SOIL 

_ 


Sample wt/vol: 5.0 (q/mL) Q Lab File ID: 21221815 

Level: (low/mad) jog Date Received: 12/14/92 

i Moisture: not dec. ^ 4 Date Analyzed: 12/21/92 




Number TICs found: 0 (ug/L or uq/Rg) UG/RG 

I I 1 I I 


gs^^^s^sâ I asaâ^:mss:s^s^âs^sa^sov I osss:a I s^^^s^m^sa I ^^:sue I 

I I I 1 I 


0

0000? 

1A EPA SAMPLE NO. 


Lab Naze: TMA/ARLI Contract: WHC 

B07QC0 

Lab Code: TMAL& Case No.: 12047 SAS No.: NA SDG No.: M_ 


Sample vt/vol: 5 . 0 (g/mL) 0_ 

Level: ( low/zed) UM 

i Moisture: not dec. _^' 




Lab Pilo ID: 2122?R16 






(ug/L or ug/Kq) UG/KG 0 

74-87-3 --------- Chloromethane 11 IV 

74-83 -9 --------- Bromomethane 11 IV 

75-01-4--------- inyl Chloride 11 IV 

75-00-3 --------- Chloroothano 11 IV 

75-09-2---------Methylene Chloride 5' j.JJ 

67-64-1---------Acetone 28 4^ u 

75-15-0---------Carbon Disulfide it 1 U 

75-35-4 --------- 1,1-Dichloroethena 11 1U 

75-34-3 --------- 1,1-Dichloroethana 11 1 V 

540-59-0 -------- 1,2 -Dichloroothene ( total)_ it IV 

67-66-3---------Chloroform 1 11 IV 

107-06-2 -------- 1,2-Dichloroethane 1 it 1 U 

76-93-3 --------- 2-Butanone 1 11 1U 

71-55-6 --------- 1,1,1-Trichloroethane 1 11 1U 

56-23-5---------Carbon Tetrachloride 1 11 (U 

75-27-4 --------- Bromodichloromethane 11 1 U 

78-87-5 --------- 1,2-Dichloropropane 11 1 U 

10061-01-5 ------ cis-1,3-Dichloropropens 11 IV 

79-01-6 --------- Trichloroethene 11 IV 

124-48-1 -------- Dibromochloromeane 11 1U 

79-00-5 --------- 1,1,2 -Trichloroethane 11 IV 

71-43-2---------Benzene ( 11 I V 

10061-02-6 ------ trans-1,3-D chloropropens 11 1 U 

75-25-2 --------- Bromoform it IV 

108-10-1--------4 -Methyl-2-Pentanons it (U 

591-78-6--------2-Hexanone 11 IV 

127-18-4 -------- Tatrachloroethene ( it 1 U 

79-34 -5 --------- 1,1,2,2-Tetrachloroethane I 11 III 

108-88-3--------Toluene 1 11 1U 

108-90-7 -------- Chlorobenzene it IV 

100-41-4 -------- Ethylbenzene 11 1U 

100-42-5--------Styrene 11 IV 

1330-20-7 ------- Xylene (total) it IV 

i i 

FORM I VOA 3/90

000030 

lE 




807000 i 

Lab Name: TMA/ARLT Contract: wail I I 


_ 



Sample wt/vol: 5.0 (g/mL) Lab File ID: 

Level: (low/zed) LOW Date Received: 

i Moisture: not doe. _ 5 Date Analyzed: 12/21,/92 





i I I I I 

I CAS NUMBER ( COMPOUND NAME I RT I EST. CONC. I Q 

I I I I I, 

FORM I VOA-TIC 3/90



t Moisture: 6 

is 


30.1 (5/R+) SL— 

decanted: ( Y/N) N_ 



000031 


I I 

I 807Q93 I 

Lab Naae: TMA/ARLI Contract: WHC I I 

Lab Coda: TKALa_ Case No.: 12047 SAS No.: NA SDG No.: gam_ 

Matrix: ( soil/water) SOZL Lab Sample ID: A212047-01B 



Date Extracted: 12/21,L 





CAS NO. COMPOUND (ug/L or ug/Rg) UG/XG 

108-95-2--------Phenol 1 350 ÎI1 

111-44-4 -------- bis(2-Chloroethyl ) Ether 1 350 III 

95-57-8 --------- 2-Chlorophenoi 1 350 1U 

541-73-1 -------- 1,3-Dichlorobenzena 1 350 III 

106-46-7 -------- 1,4 -Dichlorobenzena 1 350 IU 

95-50-1 --------- 1,2-Dichlorobenzena 1 350 IU 

95-48-7 --------- 2-Mathylphenol 1 350 III 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_I 350 III 

106-44-5 -------- 4-Methylphenol I 350 III 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne_1 350 III 

67-72-1 --------- Hexachloroethans 1 350 IU 

98-95-3---------Nitrobenzene i 350 I U 

78-59-1 -------- -Isophorons 1 350 I UI 

88-75-5 -------- -2-Nitrophanol 1 350 IV I 

105-67-9 -------- 2,4 -Dimethylphenol 1 350 1Ui 

111-91-1 -------- bis(2-Chloroethoxy) Methane_1 350 IUI 

120-83-2 -------- 2,4-Dichlorophenol 1 350 IV I 

120-82-1 -------- 1,2 , 4-Trichlorobenzone 1 350 1 II 

91-20-3---------Naphthalene 1 350 IV 

106-47-8 ------ --4-Chlorcanil ne 1 350 III 

87-68-3 --------- Hexachlorobutad ene 1 350 I II 

59-50-7 --------- 4-Chloro -3-Methylphenol 1 350 1U 

91-57-6 --------- 2-Methylnaphthalene ( 350 1U 

1 77-47-4 --------- Hexachlorocyclopentad ene I 350 I U 

1 88-06-2 --------- 2,4,6-Trichlorophenol 1 350 1U 

1 95-95-4 --------- 2,4,5-Trichlorophenol 1 850 I II 

1 91-58-7 --------- 2-Chloronaphthalene 1 350 1U 

1 88-74-4 --------- 2-Nitroaniline 1 850 1U 

1 131-11-3 -------- Dimethylphthalate 1 350 1 U 

1 208-96-8 ------ --Acenaphthylene I 350 III 

1 99-09-2 ------- --3-Nitroaniline I 850 1U 

1 83-32-9--------- cenaphthene 1 350 1 U 

1 51-28-5 --------- 2,4-Dinitrophenol 1 850 1U. 

FE 

^' I

1C 


Lab Naas: THA/ARLI Contract: WHC I 

000032 


I I 

I B07Q93 I 

Lab Code: THALA Case No.: 12047 SAS No.: NA SDG No.: Imo_ 

_ 


Lab Sample ID: x212047-OIB 

Sample wt/vol: 30.1 (g/NL) SL_ 

Level: ( low/med) j4 

i Moisture: _ 6 decanted: (YIN) N 


Injection Volumes 2.0(uL) 



100-02-7 -------- 4-Nitrophenol 

132 -64 -9 -------- Dibenzoluran 

121-14 -2 -------- 2,4-Dinitrotoluene 


7005-72-3 ------- 4-Chlorophenyl-phenylether_ 

86-73-7 --------- Fluorene 

100-01-6 -------- 4-Nitroan 1 ne 

534-52 -1 -------- 4,6-Dinitro-2-methylphenol_ 


101-55-3 -------- 4 -Bromophenyl -phenylether 

118-74- 1 -------- Hexachlorobenzone 


120-12- 

86-74-8 

84-74-2 

206-44- 

91-94 -1 --------- 3,3'-Dichlorobenzidine 

56-55-3 --------- Benzo ( a)Anthracens 

117-81-7 -------- bis(2-Ethylhexyl)Phtha ate_ 

218-01-9 ----- ---Chrysene 

117-84-0 ----- ---Di-n-Octyl Phthalate 

205-99-2 -------- Benzo (b)Fluoranthene 

207-08-9 -------- Benzo (k)Fluoranthens 

50-32-8 --------- Benzo ( a)Pyrens 

193-39-5 --------- Indeno ( 1,2,3-cd ) Pyrene 

53-70 -3 --------- Dibenz ( a,h)Anthracens 

191-24 -2 -------- Benzo (g,h,i)Perylene 

Lab Pilo ID: 2123OS10 







850 

350 

350 

350 

350 

350 

350 

850 

850 

350 

350 

350 

850 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

U I 

U I 

U i ^b 


U 

U UUUUUUUUU 

U 

U 

U 

U UUUUU


1F 

.VOLATILE ORGANICS ANALYS 


Lab Code: TNAL ►_ Case No.: 12047 


•Yy 

IS DATA SHEET 

000033 


CONPOUNDS 

Contract: WHC 

I 

I B07Q93 

I 

I 

I 



Sample wt/vol: 30 . 1 (g/aL) G Lab File ID: 21230910 


t Moisture: _ 6 decanted: ( Y/N) N Date Extracted: 12/21/92 


Injection Volume: 2.O(UL) Dilution Factor: 1.0 

GPC Cleanup: ( Y/N) Y pH: 7.7 


Number TICS found: 4 (ug/L or ug/Kg) U!G/KQ 

CAS NUMBER COMPOUND NAME RT 

!!!!i!!!!i!ili^! I i!!!i!!!!q!i!!!!!!illiiilO I llYii!! 

1.. (UNKNOWN HYDROCARBON I 6.37 




I 

I 

EST. CONC. I Q 

210 [W 

180 IJ 

1600 1 W 

250 I 

^ô 

FORM I SV-TIC 3/90

000034 

is 


I 


^ 

Lab Name: TNA/ARLI Contract: WHC 

I 807Q94 

I 

Lab Code: j s Case No.: 12047 SAS No.: NA SDG No.: NA 

Matrix: ( soil/water) 1:Qjj,_ Lab Sample ID: x212047 -028 

Sample wt/vol: 30.5 (g/mL) Q_ Lab File ID: 2123OS13 

Level: ( low/mad) LOW Date Received: 12/14/92 

t Moisture: _ 4 decanted: (Y/N) tl_ Date Extracted: 12/21/92 



GPC Cleanup. (YIN) y_ pH: 6.9 


CAS NO. COMPOUND (ug/L or ug/Xg) UG /KG Q 

108-95-2--------Phenol 340 

111-44 -4 -------- bis ( 2-Chloroethyl ) Ether 1 340 1 1 

1 95-57-8 --------- 2-Chlorophenol I 340 IU I 

1 541-73-1 -------- 1,3-Dichlorobenzens 1 340 III I 

1 106-46-7 -------- 1,4 -Dichlorobenzens I 340 I U I 

1 95-50-1 --------- 1,2-Dichlorobenzene ( 340 I V I 

1 95-48-7 -------- -2-Methylphanol I 340 IV I 

1 108-60-1 ------- -2,2'-oxybis(1-Chloropropane)_1 340 III I 

1 106-44-5 -------- 4-Methylphenol 1 340 III I 

1 621-64 -7 -------- N-Nitroso-Di-n-Propylam na_1 340 I V I 

1 67-72-1 --------- Hexachloroethane I 340 III I 

1 98-95-3---------Nitrobenzene ( 340 1 U I 

1 78-59-1 --------- Isophorone 1 340 I U I 

1 88-75-5 --------- 2-Nitrophenol I 340 I U I 

1 105-67-9 -------- 2,4 -Dimethylphenol 1 340 III I 

1 111-91-1 -------- bis ( 2-Chloroethoxy )Mathana 340 1 I V I 

120-83-2 -------- 2,4 -Dichlorophenol -'1 340 III I 

1 120-82-1 -------- 1,2 , 4-Trichlorobanzene I 340 III I 

i 91-20-3---------Naphthalene 1 340 1U I 

1 106-47-8 -------- 4-Chloroanii ne I 340 IV I 

1 87-68 -3 --------- Hexachlorobutad ena 1 340 I V 1 

1 . 59-50-7 --------- 4-Chloro-3-Methylphenol 1 340 1 U I 

1 91-57-6 --------- 2-Methylnaphthalons I 340 IU I 

77-47-4 --------- Hexachlorocyclopentad ^ e ne 1 340 IU I 

1 88-06-2 --------- 2,4,6-Trichlorophenol i i 340 III 

1 95-95-4 --------- 2,4,5-Trichlorophanol I 820 I II I 

1 91-58-7 ------- --2-Chloronaphthalene I' 340 IU 

1 88-74 -4 ---------2-Nitroaniline i 820 1U 

1 131-11-3 -------- Dimethylphthalate I 340 IU 

1 208-96-8 -------- ACenaphthylene I 340 1 U I 

1 99-09-2 --- -- ---- 3-Nitroaniline 1 820 IV I 

1 83-32-9 --------- Acenaphthene I 340 Iv 

1 51-28-5 --------- 2 , 4-Dinitrophenol 1 820 IU 

411I)d

1C 


132-64-9 -------- Dibenzof 

121-14-2 -------- 2,4-Dini 

606-20-2 -------- 2.6-Dini 

7005-72-3-------4 

100-01-6--------4- 

534-52-1--------4, 

86-30-6 --------- N- 

118-74-1--------Hexachlorobenzene 


85-01-8 --------- Phenanthrene 

120-12-7 -------- Anthracene 

86-74-8 --------- Carbazole 

206-4 

(1)_ 


56-55-3 --------- Benzo (a)Anthracene 

117-81-7 -------- bis ( 2-Ethylhexyl ) Phthalate_ 

218-01-9 ---- ----Chrysens 

117-84 -0 --------Di-n-Octyl Phthalate 

205-99-2--------Benzo (b)Fluoranthene 

207-08-9--------Benzo (k)Fluoranthene 

50-32-8 --------- Benzo (a)Pyrene 

193-39-5 -------- Indeno ( 1,2,3-ed ) Pyrene 

53-70-3 --------- Dibenz (a,h)Anthracene 

191-24-2 -------- Benzo (g,h,i)Perylene 

00003.1 


I I 

I 807Q94 I 


Lab Code: TMAJA— Case No.: 12047 SAS No.: NA SDG No.: Na_ 




i Moisture: _4 decanted: ( Y/N) N_ 





FORM I SV-2 

Lab Sample ID: x212047-028 

Lab File ID: 21230S13 





:ONCENTRATION UNITS: 

(ug/L or ug/Rg) UG/KG Q 

820 ÎI^- 1 

340 II 

340 I II I^ 

340 IQ I 

340 1U I 

340 1U 

820 1U 1 

820 1U 1 

340 1U 1 

340 1U 1 

340 1U 1 

820 1U 1 

340 III i 

340 1U 1 

340 III 1 

340 1U 1 

340 III 1 

340 1U 1 

340 III 1 

340 1U I 

340 1U 1 

340 1U 1 

340 1U I 

340 III i 

340 1U I 

340 1U I 

340 1U 1 

340 1U I 

340 1U I 

340 JU 

I 

I 

I 

I 

3/90

IF EPA Bi^$fkAt^6 

SEHIVOLATILE ORGANICS ANALYSIS DATA SHEET 


I B07Q94 I 

Lab Name: TMA/ARLI Contract: %7HC I I 

Lab Code: TMALh Case No.: 12047 SAS No.: NA SDG No.: 2(a__ 

Matrix: ( soil/water) SOIL Lab Sample IDs A212047-02B 

Sample wt/vol: 30 . 5 (g/aL) Q.— Lab File ID: 21230513 

Level: ( low/med) ION Date Received: 12/14/92 

t Moisture: _ 4 decanted: (Y/N) N Date Extracted: 12/21/92 

Concentrated Extract Volume: 500.0 ( UL) Date Analyzed: 12/30/92 

injection Volume: 2.0 (UL) Dilution Factor: 1.0 

GPC Cleanup: ( YIN) y_ pH: 6.9 


Number TICs found: _ 3 (ug/L or ug/Rg) UG/RG 

I I I 

( CAS NUMBER I COMPOUND NAME I 

I 

RT 1 EST. 

I I 

CONC. I Q I 

I^ssassssamas^ I âtslat+#^ssssasfsis^ss^sffaa I ss^s^sî l a:î:smms(Ôe I 

I 1. ISUBST. BENZENE I 6.42 1 100 11 1 

1 2. 1UNXNOWN HYDROCARBON 7.37 1 1 1400 &o- 

I 3. 1 UMOWN ALCOHOL i 8 . 72 i 240 p I I i 

I 

I I 

FORM I SV-TIC 

Q 

1^^-I y3 

3/90

1a 


340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

830 

340 

830 

340 

340 

830 

340 

830 

000037 

EPA SAMPLZ NO. 

I 1 

I B07Q95 I 

Lab Name: THA/ARLI Contracts WHC ( I 

Lab Codes TNALA Case No.: 12047 SAS No.: NA SDG No.: ga_ 


Sample wt/vol: 30.5 (q/ML) Sz_ 

Levels (low/mad) IO_ 

i Moisture: _5 decanted: (Y/N) K 


Injection volume: 2.0(UL) 



111-44-4 -------- bis ( 2-Chloroethyl)Ether 

95-57-8 --------- 2-Chlorophenol 

541-73-1 -------- 1 , 3-Dichlorobenzene 


95-50-1---------1,2-Dichlorobenzene 

95-48-7 --------- 2-Methylphenol 

108-60 - 1 -------- 2,2'-oxybis ( 1-Chloropropane)_ 

106-44-5 -------- 4-Methylphenol 

621-64 -7 -------- N-Nitroso -Di-n-Propylam ne_ 

67-72-1 --------- Bexachloroethane 

98-95-3-------- -Nitrobenzene 

78-59-1 --------- Isophorone 

105-67-9 -------- 2,4- 

111-91-1 -------- bis( 

120-83-2--------2,4- 

120-82-1--------1,2, 

106-47 

59-50-7 --------- 4 -Chlorc-3-Nethylphenol 

91-57-6 --------- 2-Mothylnaphthalens 


68-06-2 --------- 2,4 , 6-Trichlorophenol 

95-95-4 --------- 2,4 , 5-Trichlorophenol 

83-32-9 --------- Acenaphthene 

51-28-5 --------- 2,4-Dinitrop enol 









^^ I 

ttl i


000038 



Lab Code: TMALA Cass No.: 12047 

Matrix: (soil/water) SOIL - 


I I 

i B07Q95 i 


SAS No.: NA SDG No.s Kh 



Level: (low/zed) LOW Date.Received: 12/14/92 

t Moisture: _5 decanted: (Y/N) N Date Extracted: 12/21/92 



GPC Cleanup: WN) X— pH: 7.3 


CAS NO. COMPOUND (ug/L or ug/Rg) UG/RG M 

100-02-7 -------- 4-Nitrophenol j 830 

132-64-9 -------- DibenzoEuran ( 340 


606-20-2 -------- 2,6-Dinitrotoluene I 340 

84-66-2 --------- Diethylphthalate I 340 

7005-72-3 ------- 4-Chlorophanyl-phenylether I 340 

86-73-7 --------- Fluorene I 340 

100-01-6 -------- 4-Nitroan 1 ne I 830 

534-52-1 -------- 4,6-Dinitro-2-methylphenol_I 830 

86-30-6 --------- N-Nitrosodiphenylamine (1) 1 340 

101-55-3 -------- 4-Bromophenyl-phenylether — I 

340 

118-74-1 -------- Hexachiorobenzene I 340 

87-86-5 --------- Pentachlorophencl 1 830 

85-01-8 --------- Phenanthrene I 340 

120-12-7 -------- Anthracene I 340 

86-74-8 --------- Carbazole I 340 

84-74-2 --------- Di-n-Butylphthalate ( 340 

206-44-0 -------- Fluoranthene I 340 

129-00-0 ---- ----Pyrens I 340 

85-68-7 ---------Butylbenzylphthalat i 

3340 

91-94-1 --------- 3,3'-Dichlorobenzidine I 340 

56-55-3 --------- Benzo(a)Anthracene 1 340 

117-81-7 -------- bis(2-Ethylhexyl)Phthalate 1 340 

218-01-9 ---- - --- Chrysene —) 340 

117-84-0 ---- ---- Di-n-Octyl Phthalate I 340 

205-99-2 -------- Benzo(b)Fluoranthene I 340 

207-08-9 -------- Benzo(k)Fluoranthene 1 340 

50-32-8 --------- Benzo(a)Pyrene 1 340 

193-39-5 --------- Indeno(1,2,3-cd)Pyrene 1 340 

53-70-3 ---------- Dibenz(a,h)Anthracene 1 340 

191-24-2--------Benzo(g,h,i)Perylene I 340 


/'/ 

/ 6 

-11

IF 

RT EST. CONC. 

6.37 I 210 

6.68 I 170 

7.37 I 1600 

8.72 I 210 

18.13 69 

25.68 I 100 

28.18 I 69 

000033 




I B07095 I 

Lab Name: TKA/ARLI Contract: WHC I I 

Lab Code: THAZA Case No.: 12047 SAS No.: NA SDG No.: NA 

r_ 




Level: (low/mad) LOW _ Date Received: 12L4/92 

% Moisture: _5 decanted: (YIN) N 


Concentrated Extract Volume: ,500.0 (uL) Date Analyzeds 12/30/92 


GPC Cleanup: (Y/N) y pH: 7.3 


Number TICS found: 7 (ug/L or ug/Rg) UG/RG 


1. IUNRNOWN HYDROCARBON 

2. IUNRNOWN HYDROCARBON 

3. IUNXXOWN HYDROCARBON 

4. I UN101OWN ALCOHOL 

5. PROPANOIC ACID ISOMER 

6. IHEXANEDIOIC ACID ISOMER 

7. (UNKNOWN HYDROCARBON 

I 

J 

J 

g47,2 

FORM I SV-TIC 3/90

000090 



I I 

I E07Q96 I 


Lab Code: J&TA Case No.: 12047 SAS No.: HA SDG No.: NA 

Matrix: (soil/water) SOIL Lab Sample IDs 

Sample wt/vol: 30.5 (9/ILL) G Lab File ID: 


t Moisture: ,4 decanted: ( Y/N) N Date Extracted: 12/21/92 



OPC Cleanup: (YIN) Y pH: 8.8 


I 

108-95-2--------Phenol I 

111-44-4 -------- bis(2-Chloroethyl)Ether I 

95-57-8 --------- 2-Chlorophenol I 


106-46-7 -------- 1,4-Dichlorobenzens 

95-50-1 --------- 1,2-Dichlorobenzens 

95-48-7---------2-Methylphenol 

108-60-1 -------- 2,2'-oxybis(1-Chloropropane)_^ 

106-44-5 ----- ---4-Nethylphenol 

1 621-64-7 ----- ---N-Nitroso-Di-n-Propylam ne_I, 

67-72-1 --------- Hexachloroothane 


78-59-1 --------- Isophorone 

88-75-5 --------- 2-Nitrophanol 

105-67-9 -------- 2,4-Dinothylp enol 

1 

111-91-1 -------- his (2-Chioroethoxy)Methano- 



91-20-3---------Naphthalene 

106-47-8 -------- 4-Chloroanil e 

1 

I A7-RA-1---------Aevanhlnrnhnted ewe 

91-57-6---------2-Me 

77-47-4 --------- Hexa 

88-06-2---------2,4, 

95-95-4---------2,4, 

91-58-7 --------- 2-Cb 

88-74-4---------2-N! 

208-96-8--------A 

99-09-2---------3 

51-28-5---------2, 

FORM I SV-1 




(u9/L or uq/Kq) UQ/ KGQ 

340 iUT 

340 III 

340 III 

340 IU 

340 III 

340 III 

340 III 

340 IV 

340 IU 

340 III 

340 IU 

340 IU 

340 III 

340 III 

340 IU 

340 IU 

340 IU 

340 III 

340 III 

340 IV 

340 I 

340 I 

340 IU 

340 IU 

340 I 

820 I 

340 I 

620 I 

340 I 

340 I 

820 I 

340 I 

820 I 

i

1C 


000041 


I B07Q96 


Lab Code: TMALA Case No.: 12047 SAS No.: HA SDG No.: NA 


Sample wt/vol: 30.5 (9/ML) Q 

Level: ( low/ned) LOW 

% moisture: _ 4 decanted: ( Y/N) N 


Injection volume: 2.0 (UL) 

GPC Cleanup: (YIN) Y . 


100-02-7 

121-14-2--------2,4 

606-20-2--------2,6 

84 -66-2---------Die 

7005-72-3-------4-C 

pH: 8.8 

100-01-6 -------- 4-Nitroanil ln—e 


86-30-6 --------- N-Nitrosodiphenylanine (1)_ 




o -^1-0 --------- MU ..... 

120-12-7 -------- Anthracens 

129-00-0 ------ --Pyrene 

85-68-7 ----- ----BUtylbenzylphthalate 

91-94 -1--- ------ 3,31-Dichlorobenzidine 

56-55 -3 ---- -----Benzo (a)Anthracens 

117-81-7 ------ --bis (2-Etbyihexyl)Phthalate_ 

218-01-9 -------- Chrysene 

117-84 -0--------Di-n-OCtyl Phthalats 

205-99-2--- ----- Benzo (b)Fluoranthens 

207-08-9 ----- ---Bsnzo(k)Fluoranthene 

50-32-8---------Benzo ( a)Pyrene 

193-39-5-- ---- --Indenc ( 1,2,3-cd ) Pyrens 









CONCENTRATION UNITS:• 

(ug/L or ug/Rg) UGJKG Q 

820 IUr 

340 

340 

340 

340 

340 

340 

820 

820 

340 

340 

340 

820 

340 

340 

340 

46 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

IU 

IU 

IU 

III 

IU 

IV 

U 

IU 

IU 

IU 

IV 

IU 

IV 

IV 

I 

IJ. 

U3 

IUT 

IU 

IU 

IU 

IU 

IU 

IV 

III 

IU 

IU 

IU 

IU 

I 

I_ 

FORM I.SV-2 3/90 

JR^, r

000042 

iD EPA SAMPLE NO. 



I B07Q96 I 


Lab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.. NA 


Sample wt/vol: 30.5 (g/mL) Q_ Lab File ID: 21231502 

Level: ( low/mod) JQff_ Date Received: 12/14/92 

t Moisture: 4 decanted: (YIN) N Date Extracted: 12/21/92 



GPC Cleanup: (Y/N) Y_ PH: 8.8 


Number TICS found: _6 (ug/L or ug/Rg) UG/RG 


!!!!!!!!iQ!!!!! 1!!!!!!!!!!!!!!!!i!!!!^ 

1. 1UNXNOWN HYDROCARBON 

2. ( UNKNOWN HYDROCARBON 

3. IUNXNOWN ALCOHOL 

4. IPROPANOIC ACID ISOMER 

5. IUNIINOWN CARBOXYLIC ACID ESTE 

6. 1HEXANEDIOIC ACID ISOMER 

RT I EST. CONC. I Q I 

!!!!!! 1 !i!!!!!!liiii1 !s:! 1 

6.65 I 140 IJ 

7.35 1300 W 1 

I 

8.68 I 210 Imo" u 

18.12 I 140 IJ 1 

21.12 1 1100 IJ I 

25.67 1 

I 

210 I J 1 

I I 

FORM I SV-TIC 3/90. 

-

is 


000043 


I I 

I B07Q98 I 

Lab Name: TMA/ARLi Contract: WHC I 

Lab Code: TKALA Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 30.0 (g/aL) SL_ 


t Moisture: 4 decanted: (Y/N) N_ 



GPC Cleanup: (YIN) Y pH: 


1 108-95-2--------Phenol 

111-44-4 -------- bis(2-Chloroethy 

i 95-57-8 --------- 2-Chlorophenol 

1 541-73-1 -------- 1,3-Dichlorobanz 

106-46-7 -------- 1,4-Dichlorobenz 

1 95-50-1 --------- 1,2-Dichlorobenz 

108-60-1 -------- 2,2`-oxybis(1-Chloropropane)_ 

106-44-5 -------- 4-Methylphanol 




105-67-9 -------- 2,4-Dimethylphanol 

111-91-1 -------- bis (2-Chloroethoxy) Methane_ 



91-20-3---------Naphthalene 

106-47-8 -------- 4-Chlorcanil ne 

77-47-4 --------- Hexa 

88-06-2---------2,4, 

95-95-4---------2,4, 

91-58-7---------2-Ch 

88-74-4---------2-N! 

99-09-2---------3-Ni 

51-28-5---------2 

Lab Sample ID: x212047-13B 

Lab File ID: 

21231SO9 






(ug/L or ug/Rg) yG/KS Q 

1.0 

340 IUD 

340 U 

340 U 

340 

340 I I P 

I II 

340 IU 

340 IU I 

340 1 I 

340 IU 

340 IU I 

340 IU 

340 IU 

340 IU I 

340 IU I 

340 IU I 

340 IU I 

340 IU I 

340 IU I 

340 IU 

340 IU I 

340 (U I 

340 IU 

340 IU I 

340 IU 

340 IU 

830 IU I 

340 IU I 

830 IU I 

340 IV i 

340 IV I 

830 (U I 

340 IU I 

830 1 I 

3/90

1C 



000044 


B07Q98 

Lab Code: 'TMALA Case No.: 12047 SAS No.: NA SDG No.: KA 


Sample wt/vol: 30.0 (9/AL) Q__ 





GPC Cleanup: (YIN) g_ pH: 8.8 


100-02-7 

121-14-2 -------- 2 , 4-Dinitrotoluena 1 


84-66-2 -------- -Diethylphthalate 

7005-72-3 ------- 4-Chlorophenyl -phenylether_^ 

86-73-7 --------- Fluorene 

100-01-6 -------- 4-Nitroan 1 ne 

534-52-1 -------- 4,6-Dinitro -2-methylphenol 

86-30-6 --------- N-Nitrosodiphenylamine (1)^1 

101-55-3 -------- 4-Bromophenyl-phenylether l 


120-12-7 -------- Anthracene 

86-74 -8 --------- Carbazole 

84-74-2 

206-44- 


56-55-3---------Benzo ( a)Anthracene 

117-81-7 -------- bis (2-Ethylhexyl) Phthalate_ 

117-84 -0 -------- Di-n-OCtyl Phthalate 

205-99-2 -------- Benzo (b)Fluoranthene 


50-32-8 --------- Benzo (a)Pyrene 

193-39-5 ---- ----Indeno ( 1,2,3-cd ) Pyrene 

53-70-3 ---------Dibenz (a,h)Anthracene 





Date Analyzed: 12/31/9 2 




830 

340 lU 1 Y2 

340 

340 JU 1 

340 (U 1 

340 JU 1 

830 JU 

340 Û 1 

340 JU 1 

340 JU 1 

830 lU 1 

340 J U 1 

340 J U 1 

340 l V 1 

340 JU 1 

340 JU 1 

340 IV 1 

340 IV 1 

340 l U 1 

340 J U 1 

340 I U 1 

340 J U 1 

340 JU 1 

340 JU 1 

340 JU 1 

340 J U 1 

340 JU 1 

340 lU 1 

340 iII 


ql1^



2. ISUBST. BENZENE 



5. (UNKNOWN ALCOHOL 

6. (UNKNOWN ALCOHOL 

7. 1PR0PANOIC ACID ISOMER 

S. (UNKNOWN CARBOXYLIC ACID ESTE 

9. 1HEXANEDI0IC ACID ISOMER 

RT 

6.37 

6.42 

6.68 

7.38 

8.72 

9.05 

18.13 

21.15 

1 25.68 

EST. CONC. Q 

240 

000045 




B07Q98 I 

Lab Name: TMA/ARLi Contract: We! I I 

Lab Code: TMALA Case No.% 12047 SAS No.: NA SDG No.: Imo_ 

_ 



Sample wt/vol: 30.0 (q/mL) Q_ Lab File ID: 21231509 

Level: (low/med) JQK— Date Received: 12/14/92 

4 Moisture: 4 decanted: (Y/N) N Date Extracted: 12/21/92 





Number TICS found: 9 (ug/L or ug/Kg) UG1xG 

Oise 

I Vffk J I 

69 iJ 

170 1N," 

1600 1 

VkL 

2 69 19 K 1 

69 IJ 1 

560 11 ,1- 

140 IWUJI 

.1 I 

FORM I SV-TIC 3/90

00004G 

1B EPA SAMPLE NO. 

SENIVOLKTILE ORGANICS ANALYSIS DATA SHEET 

I I 

I B07Q99 I 

Lab Name: TK1/1RLI Contract: WHC I I 




Level: (low/zed) LO_ 

t Moisture: 4 decanted: (Y/N) N 



GPC Cleanup: MR) Y— pH: 9.0 


108-95-2--------Phenol 

111-44-4 -------- bis(2-Chloroethyl)Ether 

95-57-8 --------- 2-Chlorophenol 

541-73-1 -------- 1,3-Dichlorobenzsns 

106-46-7--------1,4-Dichlorobenzsns 

95-50-1---------1,2-Dichlorobenzens 

108-60-1 -------- 2,2'-oxybis(1-Chloropropans)_ 

106-44-5 -------- 4-Methylphenol 

621-64-7 -------- N-Nitroso-Di-n-Propylaa ne_ 



78-59-1 ------- --Isophorone 

88-75-5 ---------2-Nitrophenol 

105-67-9 -------- 2.4-Dimethylphenol 

120-83-2--------2,4 

120-82-1--------1,2 

91-20-3---------Nap 

106-47-8--------4-C 

59-50-7 --------- 4-Chloro-3 

91-57-6 --------- 2-Methylna 

77-47-4 --------- Hexachlorc 

88-06-2 --------- 2,4,6-Tric 

95-95-4 ---------2,4,5-Tric 

91-58-7 --------- 2-Chlorona 

88-74-4 --------- 2-Nitroani 

131-11-3 -------- Dimethylpb 

83-32-9---------AC 

51-28-5---------2, 


Lab File ID: 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

810 

340 

810 

340 

340 

810 

340 

810 

21231503 






(ug/L or ug/Kg) UG KKGG Q 

1I= 

II, 

U UUUUU 

U 

U 

U 

V 

D 

tr/IL

1C 

SENIVOLhTILE ORGANICS ANALYSIS DATA SHEET 

Lab Name: TEA/ARLI Contract: WHC 

000047 


B07Q99 

Lab Code: TXhLh Case No.: 12047 ._ SAS No.: NA SDG No.: Imo_ 


Sample wt/vol: 30.7 (9/mL) Q_ 

Level: ( low/med) 

i Moisture: _4 decanted: (Y/N) Ii_ 



GPC Cleanup: (Y/N) Y. pH: 9.0 


100-02-7 -------- 4-Nitrophenol 

132-64 -9 -------- Dibenzofuran 

121-14-2 -------- 2,4-Dinitrotoiuene 

606-20-2 -------- 2,6 -Dinitrotoiuene 

7005-72-3 ------- 4 -Chloropheny 

86-73-7 --------- Fluorene 

100-01-6 -------- 4-Nitroa^l^n 

534-52-1 -------- 4,6-Dinitro-2 

86-30-6 --------- N-Nitrosodiph 

101-55-3 -------- 4-Bromophenyl 

118-74-1 -------- Hexachlorober 

87-86-5 --------- Pentachloroph 

120-12 

206-44 

91-94 -1 --------- 3,31-Dichlorobenzidin 

56-55-3 --------- Benzo (a)Anthracene_ 

117-81-7 -------- bis(2-Ethylhexyl)Phth 

218-01-9 -------- Chrysene 

117-84-0 -------- Di-n-Octyl Phthalate_ 

205-99-2 -------- Benzo (b)Fluoranthene_ 

207-08-9 -------- Benzo (k)Fluoranthene_ 

50-32-8 --------- Benzo (a)Pyrene 

193-39-5 -------- Indeno ( 1#2,3-cd)Pyren 

53-70-3 -------- -Dibenz (a,h)Anthracene 

191-24-2 ------- -Benzo(g,h,i)Perylene_ 

FORM I' SV-2 

Lab Pilo ID: 21231S03 






(ug/L or ug/Xg) VG/KG 

(1) 

Q 

810 jU,7" 

340 U 

340 U 

340 U 

340 U 

340 U 

340 IU 

810 U 

810 U 

340 U 

340 U 

340 U 

810 J U 

340 JU 

340 V 

340 U 

340 U 

340 U 

340 U 

340 JU 

340 1U 

340 JU 

340 U 

340 1U 

340 U 

340 V 

340 J U 

340 IV 

340 1U 

340 1U 

340 IU 

3/90 

M 

4114

000048 

1F 




I B07099 I 


Lab Code: TMAj K_ Case No.: 12047 SAS No.: NA SDG No.: jam_ 


Sample wt/vol: 30.7 (9/ML) G Lab File ID: 21231SO3 

Level: ( low/mod) LOW Date Received: 12/14/92 

t Moisture: 4 decanted: (Y/N) N Date Extracted: 12 /21/92 




Number TICS found: _ 8 


(ug/L or ug/Rg) UG/RG 

CAS NUMBER I COMPOUND NAME I RT 

1 0 IUNRNOWN HYDROCARBON I 6.67 

2. IUNRNOWN HYDROCARBON I 7.35 

3. IUNXNOWN ALCOHOL i 8.70 

4. I UNXKOWN ALCOHOL I 9.02 

5. IPROPANOIC ACID ISOMER I 18.10 

6. IHEXANEDIOIC ACID ISO MER I 25.65 

7. IUNXNOWN ACID I 27.98 

S. IOCTADECANOIC ACID ISOMER 

I 28.15 

I 

FORM I SV-TIC 

I 

EST. CONC. i 

iisii J= 

170 1 

1600 Ifi^ 

240 10 

100 IP 

68 1 

100 I)3, 

100 IJ 

140 IJ 

69 P- 

3/90

is 



000049 


807QH0 i 

Lab Code: TMALA Cass No.: 12047 SAS No.: NA SDG No.: ice_ 


Sample wt/vol: 30.2 (9/ML) G 


Lab File ID: 

Level: (low/med) Date Received: 12 /14/92 

t Moisture: _3 decanted: (Y/N) N 





111-44 -4 -------- bis ( 2-Chloroethyl)Ether 

95-57-8 --------- 2-Chlorophenol 



95-50-1 --------- 1 , 2-Dichlorobenzene 

108-60-1 -------- 2,2'-oxybis ( 1-Chloropropane)_ 

106-44 -5 -------- 4-Methylphenol 

621-64 -7 -------- N-Nitroso -Di-n-Propylam ne_ 

67-72-1-------- -Hexachloroethane 

98-95-3-------- -Nitrobenzene 

78-59-1 ---------- Isophorone 

88-75-5 --------- 2-Nitrophenol 

105-67-9 -------- 2,4 -Dimethylphanol 

111-91-1 -------- bis(2-Chloroethoxy)Methane_ 

120-83-2 -------- 2,4 -Dichlorophenol 


91-20-3---------Naphthalene 

106-47-8 ------ --4 -Chloroani ne 


59-50-7 --------- 4 -Chloro-3-Methylphenol 

91-57-6 --------- 2-Methyinaphthalene 

Hexachlorocyclopentane e 


95-95-4 --------- 2,4,5-Trichlorophanoi 

88-74-4---------2-Ni 

83-32-9 --------- Acenaphthene 







340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

•340 

340 

820 

340 

820 

340 

340 

820 

340 

820 

l7A 

U I ^^ 

U I ^/f 

U I 

U I 

U 

UU 

U I 

U I 

a

1C 

aWWTUnT.ITTT.! flDP11VTf%A 1V1TMOTA MT1 STMIT 

Lab Name: TKA/ARL1 Contract: wxC 1 

i I 

i 100-02-7 -------- 4-Nitrophenol 1 820 

1 132-64-9 -------- Dibenzofuran 1 340 

1 121-14-2 -------- 2,4-Dinitrotoluene 1 340 

1 606-20-2 -------- 2,6-Dinitrotoluene 1 340 

1 84-66-2 --------- Diethylphthalate ( 340 

i 7005-72-3 ------- 4-Chlorophenyl-phenyls er_I 340 

186-73-7 --------- Fluorene 1 340 

1 100-01- 6 -------- 4-Nitroan 1 ne 1 820 

1 534-52-1 -------- 4,6-Dinitro-2-methylpheno I 820 

1 86-30-6 --------- N-Nitrosodiphenylamine (1) =1 340 

1 101-55- 3 -------- 4-Bromophenyl-phenylether,l 340 

1 118-74- 1 -------- Hexachlorobenzens I 340 

187-86-5 --------- Pentachlorophenol I 820 

85-01-8 --------- Phenanthrene 1 340 

1 120-12-7 -------- Anthracene 1 340 

1 86-74-8 --------- Carbazole 1 340 

( 84-74-2 --------- Di-n-Butylphthalate 1 84 

1 206-44-0 -------- Fluoranthens i 340 

1 129-00-0 ----- ---Pyrene 1 340 

1 85-68-7 ---------Butylbenzylphthelate 1 340 

i 91-94-1 --------- 3,3`-Dichlorobenzidine 1 340 

1 56-55-3 --------- Benzo(a)Anthracene I 340 

i 117-81-7 -------- bis(2-Ethylhexyl)Phthalate_1 340 

1 218-01-9 ----- ---Chrysene 1 340 

i 117-84-0 ----- ---Di-n-Octyl Phthalate 1 340 

1 205-99-2 -------- Benzo(b)Fluoranthens 1 340 

1 207-08-9 -------- Benzo(k)Fluoranthene 1 340 

1 50-32-8 --------- Benzo(a)Pyrene 1 340 

193-39-5 -------- Indeno(1,2,3-cd)Pyrens 1 340 

1 53-70-3 --------- Dibenz(a,h)Anthracene 1 340 

1 191-24-2 -------- Benzo(g,h,i)Perylene I 340 

000050 


I 

1 B07QBO 

Lab Code: THALA Case No.: 12047 SAS No.: NA SDG No.: N_ 

_ 



Sample wt/vol: 30.2 (g/RL) G 


t Moisture: _3 decanted: (Y/N) j(_ 








GPC Cleanup: (YIN ) Y pH: 8.8 


CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG F1 

1 

T4 

111E 


I

IF EPA0s!!►lilifE tO. 



I B07QB0 

Lab Name: TMA/ARLI Contracts WHC 1 

Lab Code: _ Case No.: 12047 SAS No.: Nom_. SDG NO.: NA 



Level s ( low/med) IAW . Date Received: 12/14/92 

% Moisture: 3 decanted: (YIN) N Date Extracted: 12/21/92 

Concentrated Extract Volume: 500.0 (UL) Date Analyzed: 121 30/92 

Injection volumes 2.0(uL) Dilution Factor: 1.0 



Number TICS found: 5 (ug/L or ug/Kg) yG/KG 

I I I I 1 I 

I CAS NUMBER 1 COMPOUND NAME 1 RT I EST. CONC. I Q I 

Issssssa:sasss^s I ssssssasssssas:ssssaasss::ss 1 asssassl ssssssssassssl sssss 

I 1. (UNKNOWN HYDROCARBON I 6.37 1 170 

I 2. (UNKNOWN HYDROCARBON I 6.68 1 170 IJ 

I 3. (UNKNOWN HYDROCARBON 1 7.37 1 1600 1 U 

I 4• 1 UNKNOWN ALCOHOL 1 8.72 i 270 I GfJI 

I 5. 1PROPANOIC ACID ISOMER 1 18.13 1 240 1J 1 

FORM I SV-TIC 3/90

18 


0 0 0 0 5 2) 


B07QB1 

Lab Name: TMA/ARLI Contract: WHC 1 I 



Sample wt/vol: 30.4 (9/mL) Sz_ 

Level: (low/mad) lgg_ 

i Moisture: 3 decanted: (YIN) N 











(u9/L or u9/K9) UG/RG Q 

) 108-95-2--------Phenol 340 ( U-X 

111-44-4 -------- bin (2-Chloroethyl)Ether 340 V 

95-57-8 --------- 2-Chlorophenol ( 340 10 

541-73-1 -------- 1,3-Dichlorobenzene 340 JU 

106-46-7 -------- 1,4-Dichlorobenzene 340 IV 

) 95-50-1 --------- 1,2-Dichlorobenzene I 340 JU 

i 95-48-7 --------- 2-Methylphenol 1 340 IV- 

108-60-1 -------- 2e2'-oxybis(1-Ch oropropane)_I 340 10 

106-44-5 -------- 4-Methylphenol 340 III 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne 340 JU 

67-72-1 --------- Hexachioroethane 340 JU 

98-95-3---------Nitrobenzene 340 IV 

78-59-1 ------- --Isophorone 340 JU 

88-75-5 ------- --2-Nitropheno 340 JU 

105-67-9 -------- 2,4-Dimethylphenol 340 JU 

111-91-1 -------- bis(2-Chloroethoxy)Methano I 340 JU 

120-83-2 -------- 2,4-Dichlorophenol 340 JU 

120-82-1 -------- 1,2,4-Trichlorobenzene 340 JU 

91-20-3---------Naphthalene 340 JU 

106-47-8 ------ -- 4-Chloroanil ne 340 IV 

87-68-3 --------- Hexachlorobutad ene 340 JU 

59-50-7 --------- 4-Chloro-3-Methyiphenoi 340 JU 

91-57-6 --------- 2-Methylnaphthalene 340 JU 

i 77-47-4-------- -Hexachlorocyclopentad e — I 340 IV 

88-06-2---------2,4,6-Trichlorophenol 340 IV 

95-95-4---------2,4,5-Trichlorophenol 810 JU 

( 91-58-7 ------- --2-Chloronaphthalene 340 JU 

88-74-4 ------- --2-Nitroaniline 810 JU 

( 131-11-3 -------- Dimethylphthalate 340 IV 

208-96-8 ------ --Acenaphthylene 340 IV 

99-09-2 ------- --3-Nitroaniline 810 IV 

83-32-9 ---------- Acenaphthene 340 JU 

51-28-5 --------- 2,4-Dinitrophenol 810 JU 

FORM I SV-1 

1a 

LIP,

1C 

SEMIVOLKTILE ORGANICS ANALYSIS DATA SHEET 

000053 

EPA AMPLE NO. 

B07QB1 I 

Lab Name: TMA/ARLI Contract: WHC 1 I 

Lab Code: TKALh_ Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 30.4 (VUL) Sr_ 

Level: (low/mad) i9W 

% Moisture: `3 decanted: (Y/N) )i__ 





Lab File ID: 






CAS NO. COMPOUND (uq/L or uq/Kq) UG/RG Q 

100-02-7 -------- 4-Nitrophenol 810 IUT 

132-64-9 -------- Dibenzoluran I 340 IUI 

121-14-2 -------- 2,4-Dinitrotoluene i 340 IU 

606-20-2 -------- 2,6-Dinitrotoluene I 340 IU 

84-66-2 --------- Diethylphthalate 1 340 1 

7005-72-3 ------- 4-Chlorophenyl-phenylether I 340 IU 

86-73-7 --------- Fluorene I 340 IV 

--------4-Nitroaniline 1 e I 810 IV 

534-52-1 -------- 4,6-Dinitro-2-methylphanol i 810 IV 

86-30-6 --------- N-Nitrosodiphenylamine (1)`1 340 IV 

101-55-3 -------- 4-Bromophenyl-phenylether I 340 IV 

118-74-1 -------- Hexachlorobenzene I 340 IV 

87-86-5 --------- Pentachlorophenol I 810 IU 

85-01-8 --------- Phenanthrene I 340 III 

120-12-7 -------- Anthracene 1 340 III 

86-74-8 --------- Carbazole I 340 (U 

84-74-2 --------- Di-n-Butt' phthalate 1 340 IU 

206-44-0 -------- Fluoranthene I 340 iU 

129-00-0 -------- Pyrens I 340 IU 

85-68-7---------Butylbenzylphthalate 1 340 III 

91-94-1---------3,3 1 -Dichlorobenzidine I 340 IU 

56-55-3 ------- --Benzo(a)Anthracene 1 340 1U 

117-81-7 --------bis(2-Ethylhexyl)Phthalate_I 340 IV 

218-01-9 ------ --Chrysene 1 340 IU 

117-84-0 --------Di-n-Octy1 Phthalate I 340 IV 

205-99-2 -------- Benzo (b) Fluoranthene 1 340 IU 

207-08-9 -------- Benzo(k)Fluoranthens 1 340 1U 

50-32-8 --------- Benzo(a)Pyrene 1 340 1U 

193-39-5 ----- ---Indeno (le 2,3-cd)Pyrane I 340 1V 

53-70-3 ---------Dibenz(a,h)Anthracene 1 340 IUI 

191-24-2 -------- Benzo(q,h,i)Perylens 1 340 IU 

K$ 

FORM I SV-2- 3/90 

q/i'-

Number TICS found: ^3 


(uq/L or uq/Rq) UG/RG 

: 

I CAS NUMBER 

I 

1. 

2. 

I 3. 

I I 

I 

I I 

COMPOUND NAME I RT I EST. CONC. I Q 

I^^sa^sYâ^sa^îaâ:^^ I ÔtsPa I ^â^f^^sq^Ra I Rss I 

(UNKNOWN HYDROCARBON I 6.65 I 170 IJ 

(UNKNOWN HYDROCARBON I 7.33 I 1500 liwuh 

IUNKNOWN ALCOHOL I 8.68 200 I I 

1 

000054 

iF 




I B07QB1 I 





Sample wt/vol: 30.4 (V )RL) G Lab File ID: 2123OS15 

Level: ( low/mod) Date Received: 12 /14/92 



Injection volume: 2.o(UL) Dilution Factor: 1.0 


FORM I SV-TIC 

98* '7 l a/ys 

3/90

la 


340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

820 

340 

820 

340 

340 

820 

340 

820 

0 0 0 0 5 5 


i 1 

I a07Qa2 I 

Lab Name: TKA/ARLI Contract: WHC I i 

Lab Code: TH&L),_ Case No.: 12047 SAS No.: NA SDG No.: Imo_ 

Matrix: (soil/water) SOIL Y Lab Sample ID: A2 12047-088 

Sample wt/vol: 30.6 (g/mL) G_ Lab File ID: 21231191 

Level: ( low/mad) WX Date Received: 12/14/92 

t Moisture: 4 decanted: (Y/N) N Date Extracted: 12/21/92 




GPC Cleanup: (Y/N) Y._.. pH: 9.7 


CAS NO. COMPOUND (ug/L or ug/Kg) UQ/KG Q 

108-95-2--------Phenol 

111-44-4 -------- bis ( 2-Chloroethyl)Ether 

95-57-8 --------- 2-Chlorophenol 




108-60-1 -------- 2,2'-oxybis( 

106-44 -5 -------- 4-Methylphen 

621-64 -7 -------- N-Nitroso-Di 

67-72-1 --------- Hexachloroet 


88-75-5 --------- 2-Nitrophenol 

105-67-9 -------- 2 , 4-Dimethylp enol 

111-91-1 -------- bis ( 2-Chloroethoxy ) Methans_ 

120-83-2 -------- 2,4 -Dichlorophenol 

120-82-1 -------- 1,2 , 4-Trichlorobenzene 

106-47 

59-50-7 --------- 4-Chloro-3 

91-57-6 --------- 2-Methylna 

77-47-4 --------- Hexachlorc 

88-06-2 --------- 2,4,6-Tric 

95-95-4 --------- 2,4,5-Tric 

131-11-3 

208-96-8 

83-32-9---------A 

51-28-5---------2 

U^ 

U 

U 

U II 

II 

U UU 

U UUUUUUUUUUUUUUUU 

U 

Rig 

V/D/

1 117-81-7 

00005G 


SEMIVOLBTILE ORGANICS ANALYSIS DATA SHEET 


100-02-7 -------- 4-Nitrophenol 820 

132-64-9 -------- Dibenzoturan 340 


606-20-2 -------- 2,6-Dinitrotoluene ( 340 

84-66-2 --------- Diethylphthalata 340 

7005-72-3 ------- 4-Chlorophanyl-phenylether 340 

86-73-7 --------- Fluorene 340 

100-01-6 -------- 4-Nitroan 1 ne 820 

534-52-1 -------- 4,6-Dinitro-2-methylphenol_ 820 





85-01-8 --------- Phenanthrene 340 

120-12-7 -------- Anthracene 340 

86-74-8 --------- Carbazole 340 


206-44-0 -------- Fluoranthene 340 

129-00-0 ------ --Pyrene 340 

85-68-7 ------- --Butylbenzylphthalete 340 


56-55-3 --------- Benzo(a)Anthracens 340 

-------- bis(2-Ethylhexyl)Phthalate_I 340 

218-01-9 ------- -Chrysene ( 340 

117-84-0 ------- -Di-n-Ootyl Phthalate 340 

205-99-2 -------- Benzo(b)Fluoranthene 340 


50-32-8 --------- Benzo(a)Pyrene 340 

193-39-5 ------ --Indeno(1,2,3-cd)Pyrens 340 

53-70-3---------Dibenz(a,h)Anthracene 340 

191-24-2--- ----- Benzo(g,h,i)Perylens 340 

B07QB2 

Lab Code: 'THALA_ Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 30.6 (g/mL) G_ 


t Moisture: 4 decanted: (YIN) N 




Lab File ID: 




Dilution Factor: 110 



CAS NO. COMPOUND (ug/L or ug/Rg) UG/RG N 


'0 

'0

000057 

IT 




I B07QB2 I 

Lab Name: TMA/ARLI Contract: WKC I I 

Lab Code: TKAja_ Case No.: 12047 SAS No.: NA SDG No.: j'I'E— 


Sample wt/vol: 30.6 (g/aL) Qr_ Lab File ID: 21231SOA 


t Moisture: _ 4 decanted: (Y/N) N Date Extracted: 12/21/92 






CAS NUMBER 

I 

1 

COMPOUND NAME 

1. ISUBST. BENZENE 


3. 1UMMOWN HYDROCARBON 

4. 1UNKNOWN ALCOHOL 

5. 1UNENOWN ALCOHOL 

6, 1PROPANOIC ACID ISOMER 

7. (UNKNOWN CARBOXYLIC ACID ESTE 

8. 1HEXANEDIOIC ACID ISOMER 

I 

I 


I I 

I Q I 

6.38 1 68 IJ 1 

6.67 1 170 IX 

7.37 I 1700 1Br 

8.70 240 1W tAT- 

9.03 1 100 1Bi3r V--4- 

18.12 I 100 1 1 1 

21.12 I 650 iJ 

25.67 1 

I 

d u31 

100 1 

I I 


/^

000058 

laEPA SAMPLE NO. 



390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

940 

390 

940 

390 

390 

940 

390 

940 

B07QB3 

Lab Code: THATA Case No.: 12047 SAS No.: NA SDG No.: NA 

satrix: (soil/water) 

;ample wt/vol: 30.7 (9/ML) Q._ 

Level: ( low/mad) LoDW 


Zoncentrated Extract Volume: 500.0 (UL) 

[ejection Volume: 2.0(uL) 

3PC Cleanup: (YIN ) Y pH: 9.2 


108-95-2------- -Phenol 

i 111-44 -4 -------- bis ( 2-Chlorcethy 

541-73-1 -------- 1,3 -Dichlorobenzene 



95-48-7 --------- 2-Methylphenol 

108 -60-1 -------- 2,2' -oxybis ( 1-Chloropropane)_ 

106-44-5 ------- -4 -Methylphenol 

621-64-7 ------- -N-Nitroso -Di-n-Propylam ne_ 



88-75-5 -------- -2-Nitrophenol 

105-67-9 ------- -2,4-Dimethyl enol 

111-91-1 --------- bis ( 2-Chloroethoxy) Methane 

120-83-2--------2,4 -Dichlorophenol 

120-82-1 -------- 1,2,4-Trichiorobenzene 

106-47-8 -------- 4 -Chloroan 

87-66-3 --------- Hexachlorc 

59-50-7 --------- 4-Chloro-3 

77-47-4 --------- Hexa 

88-06-2---------2,4, 

95-95-4---------2,4, 

91-58-7 --------- 2-Ct 

88-74-4---------2-N! 

131-11-3--------Dime 

208-96-8 -------- Acer 

99-09-2 --------- 3-Nitroaniline7- 

83-32-9---------Acenaphthene 

51-28 -5 --------- 2,4-Dinitrophenol 









III: r 

IU 

III 

JU 

j II 

J U 

JU 

III 

JU 

III 

JU 

JU 

III 

Cl 

1.1 

U 

U U 

U UUUUV 

3 

^^ G l

940 

390 

390 

390 

120 

390 

390 

940 

940 

390 

390 

390 

940 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

390 

000053 



I B07QB3 


Lab Code: TMAja_ Cass No.: 12047 SAS No.: NA SDG No.: KA 




%-Moisture: 17 decanted: (Y/N) N 



GPC Cleanup: (y/ N ) y_ pH: 9.2 


100-02-7 -------- 4-Nitrophenol 

132-64 -9 -------- Dibenzoturan 

121-14 -2 -------- 2,4-Dinitrotoluene 

606-20-2 -------- 2 , 6-Dinitrotoluene 


7005-72-3 ------- 4-Chlorophenyl -phenylether_ 

534 -52-1--------4, 



118-74 -1 -------- Hexachlorobenzene 

87-86-5 --------- Pentachlorophenol, 

85-01-8 --------- Phenanthrene 

120-12-7 -------- Anthracens 

84-74 -2 --------- Di-n-Butylphthala 

206-44 -0 -------- Fluoranthens 

129-00-0 ------ --Pyrene 

85-68-7 ---------BUtylbenzylphthal 

91-94-1 --------- 3,31-Dichlorobens 

56-55-3 --------- Benzo ( a)Anthracer 

117-81-7 -------- bis ( 2-Ethylhexyl) 

117-84 -0 -------- Di-n-Octyl Phthalate 



50-32-8 --------- Benzo (a)Pyrene 

193-39-5 -------- Indeno ( 1,2,3-cd ) Pyrene 

53-70-3 --------- Dibenz (a,h)Anthracens 









l^ 

III 

U 

U JUJ7 

U 

U UUUUUUUU 

IV 

IU U 

IV 

Iv 

Iu 

III 

Iu 

IU 

Iv 

IU 

Iu 

IU 

IV 

FORM I"SV-2 3/90 

I

000060 

1F EPA SAMPLE NO. 


TENTATIVELY IDENTIFIED COMPOUNDS 1 1 

B07083 I 

Lab Name: TMA/ARLI Contract: WHC ( 1 

Lab Code: THALA Case No.: 12047 SAS No.: 

_ 

NA SDG No.: NA 

Matrix: ( soil/water) SOIL Lab Sample ID: A212047 -098 

Sample wt/vol: 30.7 (9/XL) Q Lab File ID: 21231505 

Level: ( low/med) IQW Date Received: 12/14/92 

% Moisture: 17 decanted: (Y/N) N Date Extracted: 12/21/92 






CAS NUMBER 1 COMPOUND NAME RT EST. CONC. I Q 

IRîliif^'T..is I C...-^.-f60OifE'^fflSis^liafli 1 S^îsf I iYiiiiBSO^Q I ^S I 

I 1. ISUBST. BENZENE 1 6.38 I 79 IJ I 

I 2 • 1UNKNOWN HYDROCARBON 

IJ 

I 3 • (UNKNOWN HYDROCARBON 6.67 1160 LW t4 

I 4. (UNKNOWN ALCOHOL 1 8.70 1 200 ,W 0) 

I 5 • [UNKNOWN ALCOHOL 1 9.03 1 120 LBJ• ul— 

1 6. 

IPROPANOIC ACID ISOMER 1 18.12 

1 

79 IJ I 

I 7. (UNKNOWN CARBOXYLIC ACID ESTEI 21.12 1 710 IJ I 

I S. IHEXANEDIOIC ACID ISOMER 1 25.67 1 240 18J I 

I 9• (UNKNOWN HYDROCARBON 1 

1 1-1 

29.03 1 79 IJ I 

A6 

z l /^-- /^ 

1-1 

FORM I "SV-TIC 3/90'

18 

SEMIVOLIITILE ORGANICS ANALYSIS DATA SHEET 

Lab Name: TMA/ARL1 Contract: WHC I 

000061 


1 

1 807088 

Lab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: KA 


Sample wt/vol: 30.1 (9/ML) SL_ 


t Moisture: _5 decanted: (Y/N) j-_ 





Ys 

Lab Sample ID: A212047-10B- 







(ug/L or ug/Rg) UG/KG 

108-95-2--------Phenol 350 

111-44-4 -------- his (2-Chloroethyl)Ether 350 

95-57-8 --------- 2-Chlorophenol 350 

541-73-1 -------- 1,3-Dichlorobenzens 350 


95-50-1 --------- 1,2-Dichlorobanzens 350 

95-48-7 ------- --2-Methylphenol 350 

108-60- 1 --------2,2 1 -oxybis(1-CAloropropane)_I 350 

106-44-5 -------- 4-Methylphenol 1 350 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne,_ 1 350 

67-72-1 --------- Hexachloroethane 1 350 

98-95-3---------Nitrobenzene I 350 

78-59-1 --------- Isophorone 1 350 

88-75-5 ---------- 2-Nitrophenol 1 350 

105-67-9 -------- 2,4-Dimethylphenol 1 350 

111-91-1 -------- bis(2-Chlorosthoxy)Methane_1 350 

120-83-2 -------- 2,4-Dichlorophanol ( 350 

120-82-1 -------- 1,2,4-Trichlorobanzene 1 350 

91-20-3---------Naphthalene 1 350 

106-47-8 ------ --4-Chlorcani ne ( 350 

87-68-3 --------- Hexachlorobutad ens 350 

59-50-7---------4-Chlorc-3-Methylphenol 1 350 


77-47-4---------Hexachlorocyclopentad ene -' 1 350 

88-06-2 ------- --2,4,6-Trichlorophenol 1 350 

95-95- 4 ---------2,4,5-Trichlorophenol 1 840 

91-58-7---------2-C hloronaphthalene 1 350 

88-74-4 --------- 2-Nitroaniline 1 840 

131-11-3 -------- Dimethylphthalate 1 350 

208-96-8 -------- Acenaphthylene 1 350 

99-09-2 --------- 3-Nitroaniline 1 840 

83-32-9 --------- Acenaphthene 1 350 

51-28-5 --------- 2,4-Dinitrophenol 1 840 

F 

79J 

U I 

U 

U 

U 

U 

U 1 

U 1 

U I 

E 

a

1C 


I 

000062 


I B07QB8 I 

Lab Name: TMA/ARLI Contract: MC I I 

Lab Code: THALh Case No.: 12047 SAS No.: NA SDG No.: KA 


Sample wt/vol: 30.1 (g/aL) Q Lab File ID: 


i Moisture: _5 decanted: (Y/N) JL_ Date Extracted: 12/21/92 

Concentrated Extract Volume: 500.0 (UL) Date Analyzed: 

Injection volume: 2.0(UL) Dilution Factor: 



CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q. 

j100-02-7 -------- 4-Nitrophenol 840 jUT 

1 132-64-9 -------- Dibenzoturan I 350 III 

1 121-14-2 -------- 2,4-Dinitrotoluene 1 350 IU 

1 606-20- 2 -------- 2,6-Dinitrotoluene 1 350 III 

184-66-2 --------- Diethylphthalate 1 350 1U 

1 7005-72-3 ------- 4-Chlorophenyl-phenylether_I 350 IU 

86-73-7 --------- Fiuorene ( 350 III 

1 100-01- 6 -------- 4-Nitroan 1 ne I 840 IV 

1 534-52-1 -------- 4,6-Dinitro-2-aethylphenol I 840 III 

1 86-30-6 --------- N-Nitrosodiphenylanine (1)_1 350 IV 

1 101-55-3 -------- 4-Bromophanyl-phanylether 1 350 III 

1 118-74-1 -------- Hexachlorobenzene 1 350 1U 


1 85-01-8 --------- Phenanthrene I 350 1U 

1 120-12-7 -------- Anthracene I 350 IU 

1 86-74-8 --------- Carbazolo I 350 III 

1 84-74-2 --------- Di-n-Butylp the ate 1 350 IU 

1 206-44-0 -------- Fluoranthene 1 350 1U 

1 129-00-0 ------ --Pyrene I 350 III 

1 85-68-7 ---------Butylbenzylphthalate I 350 IU 

1 91-94-1 --------- 3,3 1 -Dichlorobsnzidine I 350 IU 

1 56-55-3 ------- --Benzo(a)Anthracene 1 350 1U 

1 117-81-7 ------ --bis(2-Ethylhexyl)Phthalate I 350 1U 

1218-01- 9 ------ --Chrysens 1 350 IU 

1 117-84-0 ------ --Di-n-Octyl Phthalate 1 350 1U 

i 205-99-2 -------- Benzo(b)Fluoranthone 1 350 19 

1207-08-9 -------- Benzo(k)Fluoranthene I 350 IV 

i 50-32-8 ------- --Benzo(a)Pyrene I 350 IU 

1 193-39-5 ------ --Indeno(1,2,3-cd Pyrene I 350 1U 

153-70-3 --------- Dibenz(a,h)Anthracene I 350 1U 

1191-24-2 -------- Benzo(g,h,i)Perylene I 350 IU 

FORK I SV-2 3/90 

i 

K e 

0r-

1>r 

000063 




B07QBS 1 


Lab Code: THALa _ Casa No.: 12047 SAS No.: NA SDG No.: gam._ 

Matrix: (soil/vater) SOIL Lab Sample ID: A212047 -10B 

Sample wt/vol: 30.1 (q/RL) G_ Lab Pilo ID: 21231506 

Level: (low/mod) L40W Date Received: 12/14/92 

t Moisture: _ 5' decanted: (YIN) jI 




GPC Cleanup: ( YIN) X— pH: 8.4 


Number TICS found: ^5 (ug/L or ug/Kq) UG/KG 

I 

1 

CAS NUMBER 

I 

1 

COMPOUND NAME 

Iiiii iii liiii! I liliOii!lliCi!!!i!!!ii!!!!! 

1 1. (UNKNOWN HYDROCARBON 

1 2. 1UNKNOWN HYDROCARBON 

1 3. (UNKNOWN ALCOHOL 

1 

i 


5. 

1HEXANEDIOIC ACID ISOMER 

I 

FORK I.SV-TIC 

I 

RT 

i I EST. CONC. 1 Q 

iflifai I is!liiili!liil!liif 

6.37 280 U 

7.37 1400 

8.72 I 210 I 

18.13 1 70 IJ 

1 25.68 1 100 1 ST Li. 

3/90

1D EPA SALE H0. 


Lab Name: TKA/ARLI Contract: WHC 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

830 

340 

830 

340 

340 

830 

340 

830 

807089 

Lab Code: MJ&ya_ Case No.: 12047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 30.2 (g/nL) Q_ 

Level: (low/ned) Igo 

i Moisture: _ 4 decanted: (Y/N) K_ 



GPC Cleanup: (YIN ) Y PH: 9.3 


108-95-2--------Phenol 

111-44-4 -------- bis(2-Chloroathy 




95-48-7 --------- 2-Hethylphenol 

108-60-1 -------- 2,2'-oxybis(1-Chloroprcpane)_ 



98-95-3 --------- Nitrobanzene 

78-59-1---------Isophorone 

88-75-5---------2-Nitrophenol 

105-67-9 -------- 2,4-Dimethylp eno 

111-91-1 --------- bis(2-Chioroathoxy)Methane_ 

120-83-2--------2,4-Dichlorophanol 


91-20-3---------Naphthalene 

87-68-3 --------- Hexachlorc 

59-50-7 --------- 4-Chlorc-3 

91-57-6 --------- 2-Methylna 

77-47-4 --------- Hexachlorc 

88-06-2 --------- 2,4,6-Tric 

95-95-4 --------- 2,4,5-Tric 

208-96-8--------A 

99-09-2---------3 

51-28-5---------2, 

Lab Sample ID: A212047 -118 

Lab File ID: 21231SO7 






(ug/L or ug/Kg) UG/KG Q. 

U 

U 

U 

U, 

U UUUUU 

U 

U UUUU 

11l 

q1,y

1C 


Lab Name: TMA/ARLI Contract: W= 

I 

100-02-7 -------- 4-Nitrophenol 1 830 

132-64 -9 -------- Dibenzofuran 1 340 

121-14-2 -------- 2,4 -Dinitrotoluene 1 340 

606-20-2 -------- 2 , 6-Dinitrotcluene 1 340 

84-66-2 --------- Diethylphthalate ( 340 

7005-72-3 ------- 4-Chlorophenyl-phenylether 1 340 

86-73 -7 --------- Fluorene I 340 

100-01-6 -------- 4-Nitroan 1 e I 830 

534-52-1 -------- 4,6-Dinitro -2-methylphenol_I 830 


101-55-3 -------- 4-Bromophanyl -phenylether i 340 


1 


85-01-8 --------- Phenanthrene 1 340 

120-12-7 -------- Anthracene 1 340. 

86-74 -8 --------- Carbazole 1 340 

84-74-2 --------- Di-n-Butt' p the ate 1 340 

206-44 -0 -------- Fluoranthene 1 340 

129-00-0 -------- Pyrene 340 

1 


91-94-1 --------- 3,3'-Dichlorobenzidine i 340 

56-55 -3 ----- ----Benzo (a)Anthracene 1 340 

1 117-81-7--------bis (2-Ethylhexyl ) Phthalate_I 340 

218-01-9 ---- ----Chrysene 1 340 

117-84-0--------Di-n-OCtyl Phthalate 1 340 

205-99-2--------Benzo (b)Fluoranthene ( 340 

207-08-9 -------- Benzo (k) Fluoranthens— 1 340 

50-32-8 --------- Benzo (a)Pyrene ( 340 

193-39-5 ---- ----Indeno ( 1,2,3-cd)Pyrene 1 340 

1 53-70-3 ---------Dibenz(a,h)Anthracene ( 340 

1 191-24 -2 -------- Benzo (g,h,i)Peryiene 1 340 

I 

III 

0 

H 

000065 


i 89 B07Q 

Lab Code: TMALA _ Case No.: 12047 SAS No.: NA SDG No.: NA— 


Sample wt/vol: 30.2 (g/aL) Q__ 

Level: ( low/mad) L40N _ 

i Moisture: _ 4 decanted: ( Y/N) Nt_ 



Lab File ID: 





GPC Cleanup: ( Y/N) Y_ pH: 9.3 


CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 0 

I 

I I^^Îr 

FORM I SV-2 3/9 0

000066 

1F 




B07QB9 I 


Lab Code: TMALh_ Case No.: 12047 SAS No.: NA SDG No.: NA_ 


Sample wt/vol: 30.2 (9/2L) Q Lab File ID: 21231507 

Level: ( low/med) Date Received: 12f14/92 

t Moisture: 4 decanted: (Y/N) N Date Extracted: 12/21/92 





Number TICS found: 7 (u9/L or u9/R9) UG/RG 

CAS NUMBER 

1. 

2. 

3. 

4. 

5. 

6. 

7. 

COMPOUND NAME 

ISUBST. BENZENE 

JUNXNOWN HYDROCARBON 


JUNMOWN ALCOHOL 

1PROPANOIC ACID ISOMER 

IUNXNOWN CARBOXYLIC ACID ESTE 


FORM I SV-TIC 

RT 

I 

I EST. CONC. 

I I 

6.40 ( 69 IJ I 

6.68 I 140 IJ 

7.37 I 1400 T 

8.72 1 210 1 JI 

18.13 69 

21.13 620 IJ 

^ 

1 

25.68 I 69 

I tJ 

I 

I 

r^ 

a 

Q 

3/90

000067 

laEPA SAMPLE NO. 


I i 

i 907QCO I 


Lab Code: TKALa_ Case No.: 12047 

_ 




Sample wt/vol: 30 . 3 (q/mL) G Lab File ID: 21231SOB 

Level: ( low/med) Lpx_ Date Received: 12/14/92 

t Moisture: _ 5 decanted: (YIN) N 






CAS NO. COMPOUND (uq/L or ug/Rg) UG/RG Q- 

108-95-2 -------- Phenol 1 340 1 7 -1 1 

111-44-4 -------- bis ( 2-Chloroethyl ) Ether 1 340 1U 1 

95-57-8 --------- 2-Chlorophenol I 340 IV 1 

541-73 -1 -------- 1,3-Dichlorobenzene I 340 I V 1 

106-46-7 -------- 1,4 -Dichlorobenzene 1 340 I II 1 

95-50-1 --------- 1,2-Dichlorobenzene 1 340 I II 1 

95-48-7 --------- 2-Methylphenol 1 340 IV 1 

108-60-1 -------- 2,2 9 -oxybis ( 1-Chloropropane )_) 340 III I 

106-44 -5 -------- 4-Methylphenol 1 340 I II I 

621-64-7 -------- N-Nitroso -Di-n-Propylam ne, i 340 III 

67-72-1 --------- Hexachloroethane i 340 III I 

98-95-3---------Nitrobenzene I 340 IU 1 

78-59-1 --------- Isophorons I 340 I V 1 

88-75-5 --------- 2-Nitrophenol I 340 III 1 

105-67-9 -------- 2,4 -Dimethylphenol I 340 III I 

111-91-1 -------- bis ( 2-ChlorcethoxyjMethane_1 340 IV 1 

120-83-2 -------- 2,4-Dichlorophenol i 340 III 1 

120-82-1 -------- 1,2,4-Trichlorobenzene I 340 III 1 

91-20-3---------Naphthalene I 340 III 1 

106-47-8 -------- 4-Chloroanii ne I 340 III 1 

87-68-3 --------- Hexachlorobutad ene I 340 III I 

59-50-7 --------- 4-Chloro-3-Methylphenol ( 340 III 1 

91-57-6 --------- 2-Methylnaphthalene 1 340 III 1 

77-47-4 --------- Hexachlorocyclopentad ene I 340 III 1 

88-06-2 --------- 2,4 , 6-Trichlorophenol I 340 I II I 

95-95-4 --------- 2,4 , 5-Trichlorophenol I 830 III 1 

91-58-7 --------- 2-Chloronaphthalens I 340 III 1 

88-74 -4 --------- 2-Nitroaniline i 830 I U 1 

131-11-3 -------- Dimethylphthaiate 1 340 I V 1 

208-96-8 -------- Acenaphthylene 1 340 IU 1 

99-09-2 --------- 3-Nitroaniline 1 830 IU I 

83-32-9---------Acenaphthene I 340 III I U, 

1 

51-28-5 ----- ----2,4 -Dinitrophenol 1 830 

I 

I 

1 

J 

I ^/13 

I

iC 


000068 


I i 

I B07QCO I 


Lab Code: TMALA Cass No.: 12047 SAS No.: K_ SDG No.: $A__ 

Matrix: (soil/eater) SOIL Lab Sample ID: A212047-12B 

Sample wt/vol: 30.3 (9/ML) Q_ 


%-Moisture: 45 decanted: (Y/N) N 



GPC Cleanup: (YIN) X_ pH: 9.4 


100-02-7 ------ --4-Nitrophenol 

132-64-9 --------Dibenzofuran 




7005-72-3 ------- 4-Chlorophenyl-phenylether_, 

86-73-7 --------- Fluorene 

100-01-6 -------- 4-Nitroan ne 


86-30-6 --------- N-Nitrosodiphenylamine (1)_, 

101-55-3 -------- 4-Bromophenyl-phenylether_ 



85-01-8---------Phenanthrene 

120-12-7 -------- Anthracene 


117-81-7 -------- bis(2-Ethylhexyl)Phthalate 

205-99-2 -------- Benzo(b)F 

207-08-9 -------- Benzo(k)F 

50-32-8 --------- Benzo(a)P 

193-39-5 -------- Indeno(1, 

53-70-3 --------- Dibenz(a, 

191-24-2 -------- Benzo(q,b 







(uq/L or uq/Kg) UG/RG Q 

830 IUS 

340 III 

340 IU 

340 IU 

340 IU 

340 III 

340 III 

830 III 

830 III 

340 IU 

340 IU 

340 IU 

830 III 

340 IU 

340 III 

340 IV 

340 IU 

340 IU 

340 IU 

340 IV 

340 IU 

340 IU 

340 IV 

340 III 

340 IU 

340 IU 

340 IU 

340 IU 

340 III 

340 IU 

340 IU 

r li 

42-. 

FORM I SV-2 3/90

IF 




I B07000 

Lab Name: TMA/ARLI Contract: W C I 

Lab Code: TMhLh Case No.: 12047 SAS No.: NA SDG No.: III_ 

_ 



Sample wt/vol: 30.3 (g/mL) 0 Lab File ID: 21231508 


% Moisture: 5 decanted: (Y/N) $_ Date Extracted: 12/21/92 

Concentrated Extract Volume: 500.0 (UL) Date Analyzed: 1/92 

12/31/92 

injection Volume: 2.0(UL) Dilution Factor: 1.0 




CAS NUMBER COMPOUND NAME RT ( EST. CONC. I Q I 

I 1. ISUBST. BENZENE ( 6.40 I 69 IJ 

I 2. (UNKNOWN HYDROCARBON I 7.37 I 1500 I B2r I 

I 3. (UNKNOWN ALCOHOL I 8.72 I 210 

4. JHEXANEDIOIC ACID ISOMER i 25.68 i 69 

I I 

FORM I SV-TIC 

3/90

000070 



I I 

I B07Q93 


Lab Code: TMALA _ Case No.: 12047 SAS No.: NA SDG NO.: N_ 

4atrix: (soil/water) SOIL Lab Sample ID: A212047-018 

iample wt/vol: 30.2 (9/ML) Q_ Lab File ID: 

t Moisture: 6 decanted: (Y/N) M_ Date Received: 12/14/92 


:oncentrated Extract Volume: 5000 (uL) Date Analyzed: 01/05/93 

Lnjection Volume: 1.00 (uL) Dilution Factor: 1.00 

3PC Cleanup: (YIN ) Y_ pH: 7.7 Sulfur Cleanup: (Y/N) E_ 


CAS NO. COMPOUND (ug/L or ug/Rq) UG/RG Q 

319-84-6 -------- alpha-BHC 

319-85-7 -------- beta-BHC 

319-86-8 -------- delta-BHC 

58-89-9 --------- gamma-BHC (L ndane) 

76-44-8---------Heptachlor 

309-00-2 -------- Aldrin 

1024-57-3-------Heptachlor epoxide 

959-98-8 -------- Endosulfan I 

60-57-1 ------- --Dieidrin 

72-55-9 ------- --4140-DDE 

72-20-8 --------- Endrin 

33213-65-9------Endosulfan II 

72-54-8 --------- 4,4' -DDD 


50-29-3---------4,4'-DDT 

72-43-5 --------- Methoxy or 

53494-70-5 ------ Endrin ketone 

7421-36-3 ------- Endrin aldehyde 

5103-71-9-------alpha-Chlordane 

5103-74-2-------gamma-Chlordane 

11104-28-2 

5346 

1267 

1.81US 

1.81U 

1.81U 

1.81U 

1.81U 

1.81U 

1.81U 

1.81U 

3.51U 

3.51U 

3.51U 

3.51U 

3.51U 

3.51U 

3.51U 

18 III 

3.51U 

3.51U 

1.81U 

1.81U 

180 III 

35 1U 

71 IV 

35 1U 

35 IU 

35 IU 

35 III 

35 III 

FORM I PEST 3/90.

1D 


I 

000071 


1 B07Q94 1 

Ab Name: TKA/ARLI Contract: WC 1 I 

'ab Code: THAI+L Case No.: 12047 SAS No.: NA SDG No.: NA 

tatrix: ( soil/water) SOIL Lab Sample ID: A212047-029_ 

;ample Wt/vol: 30.3 (9/UL) Q_ Lab File ID: 

t Moisture: 4 decanted: (Y/N) N Date Received: 12/14/92 

3xtraction: ( SepF/Cont/Sonc) SONC Date Extracted: 12/21/92 



;PC Cleanup: ( YIN ) y_ pH: 6.9 Sulfur Cleanup: (YIN) 7N 


CAS NO. COMPOUND (uq/L or uq/Rq) UG/RG Q- 

319-84-6 -------- alpha-BHC 

319-85-7 -------- beta-BHC 

319-86 -8 -------- delta-BHC 

76-44-8 --------- Heptach 

309-00-2 -------- Aldrin 

1024-57-3 ------- Heptach ayv+c a.as 

959-98-8 -------- Endosui I 

60-57-1 --------- Dieldri 

72 -55-9---------4g4'-DD 

72-20-8 --------- Endrin 

33213-65 -9 ------ Endosui 

72-54 -8---------4x41-DD 

1031-07 - 8 ------- Endosul 

50-29-3 --------- 4.41-DD 

72-43-5 --------- Methoxyc for 

53494 -70-5 ------ Endrin ketone 



5103 -74-2-------gamma-Chlordane 

8001-35-2 ------- TOxaphene 

12674-11-2 ------ Aroclor-1016 

11104-28-2 ------ Arocior-1221 

53469-21 

12672-29 

11097-69 

1.81U- 

1.81U 

1.81U 

1.81U 

1.81U 

1.SIU 

1.81U 

1.81U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

18 IUI 

3.41U'i 

3.41U1 

1.81U 

1.81U' 

180 IU 

34 IU 

69 IU 

34 IU 

34 III 

34 IU 

34 IU 

34 IU 

FORM I PEST 3/90- 

I 

03 

u^/Y

1D 


I 

000072 


I B07Q95 1 

ab Name: TMA/ARLI Contract: WHC I I 

ab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: NA 

atrix: (soil/water) SOIL Lab Sample ID: A212047-058 

ample wt/vol: 30.6 (VUL) Lab Pilo ID: 

Moisture: 5 decanted: (YIN) N Date Received: 12/14/92 

xtraction: (SepF/Cont/Sonc) SONC Date Extracted: 12/21/92 

oncentrated Extract Volume: 5000 (uL) Date Analyzed: 01/06/93 

njection Volume: 1.00 (UL) Dilution Factor: 1.00 

PC Cleanup: (YIN) Y pH: 7.3 Sulfur Cleanup: (YIN) N 


CAS NO. COMPOUND (ug/L or ug/Kg) M/KG Q 

319-84-6 -------- alpha-BHC I - 1.81UJ 

319-85-7 -------- beta-BHC 1 1.81U 

319-86-8 -------- delta-BHC 1 1.81U 

58-89-9 --------- gamma-BHC (L ndans) 1 1.81U 

76-44-8---------Heptachlor 1 1.81U 

309-00-2 -------- Aldrin 1 1.81U 

1024-57-3 ------- Heptachor epox de 1 1.81U 

959-98-8 -------- Endosulfan I 1 1.8jU 

60-57-1 --------- Dieldrin 1 3.41U 

72-55-9 --------- 4,4'-DDE 1 3.41U 

72-20-8 --------- Endrin 1 3.41U 


72-54-8 --------- 4,4'-DDD 1 3.41U 


50-29-3---------4,4'-DDT ( 3.41U 

72-43-5 --------- Methoxychlor 1 18 lU 

53494-70-5 ------ Endrin ketone I 3.41U 


5103-71-9-------alpha-Chlordane 1 1.S1U 

5103-74-2-------gamma-Chlordane 1 1.81U 

8001-35-2 ------- Toxaphene I 180 IU 

12674-11-2 ------ Aroclor-1016 1 34 1U 

11104-28-2 ------ Aroclor-1221 I 69 iU 

11141-16-5 ------ Aroclor-1232 1 34 1U 

53469-21-9 ------ Aroclor-1242 1 34 iU 

12672-29-6 ------ Aroclor-1248 1 34 IU 

11097-69-1 ------ Aroclor-1254 1 34 IU 

11096-82-5 ------ Aroclor-1260 I 34 IU 


1

1D 


,ab Name: TMA/ARLI Contract: WHC 


B07096 I 

,ab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: Nom._ 

tatrix: (soil/water) SOIL Lab Sample ID: A212047-06B 

,ample wt/vol: 30.9 (g/mL) G_ Lab File ID: 

Moisture: 4 decanted: (Y/N) K Date Received: 12/14/92 

:xtraction: (SepF/Copt/Sonc) SONC Date Extracted: 12/21/92 


:njection Volume: 1.00 (uL) Dilution Factor: 1.00 

;PC Cleanup: (Y/N) Y pH: 8.8 Sulfur Cleanup: (YIN)I)• 


CAS NO. COMPOUND (ug/L or ug/Kg) UG G Q 

319-84-6 -------- alpha-BHC 

319-85-7 -------- beta-BHC 

319-86-8 -------- delta-BHC 

58-89-9 --------- gamma-BHC (L ndane) 

76-44-8---------Heptachlor 

309-00-2 -------- Aldrin 


959-98-8 -------- Endosulfan I 

60-57-1 --------- Dieldrin 

72-55-9 -------- -4,40-DDE 

72-20-8 -------- -Endrin 

33213-65-9 ------ Endosulfan II 

72-54-8 --------- 4,41-DDD 


50-29-3---------4,4'-DDT 

72-43-5 --------- Methoxychlor 

53494-70-5 ------ Endrin ketone 




8001-35-2 ------- Toxaphene 

11104-28-2 ------ Aroclor-1221 

11141-16-5 ------ Aroclor-1232 

53469-21-9 ------ Aroclor-1242 

12672-29-6 ------ Aroclor-1248 

11097-69-1 ------ Aroclor-1254 

11096-82-5 ------ Aroclor-1260 

I 

1.71UJ 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

3.31U 

3.31U 

3.31U 

3.31U 

3.31U 

3.31U 

3.31U 

17 IU 

3.31U 

3.31U 

1.71U 

1.71U 

170 IU 

33 1U 

68 IU 

33 IU 

33 1U 

33 1U 

33 IU 

33 IU 


1 

6 

0/gal

ID 


000073 


1 1 

1 B07Q98 1 

,ab Name: TMA/ARLI Contract: WHC I I 

Ab Code: TKALA_ Casa No.: 12047 SAS No.: NA 

s 

SDG No.: Imo_ 



:ample wt/vol: 30.7 (g/mL) G_ Lab File ID: 

c Moisture: 4 decanted: (YIN) N Date Receiveds 12/14/92 

:xtraction: ( SspF/font/Sonc) $ONC Date Extracted: 12/21/92 

:oncentrated Extract Volumes 5000 (uL) Date Analyzed: A" '"S/93 

:njection Volume: 1.00 (uL) Di] LJU 

:PC Cleanup: ( YIN ) Y pH: 8.8 Sr. .' nci6 N 

CONCENTR1 

CAS NO. COMPOUND (ug/L or 

319-84 -6--------alp 

319 -85-7--------bet 

319-86-8--------del 

58-89-9---------gam 

76-44-8---------Hop 

309-00-2 -------- Ald 

1024-57-3-------Hop 

72-55-9 --------- 4,4'-DDE 

72-20-8 --------- Endrin 

33213-65-9 ------ Endosulfan II 

72-54-8 --------- 4t4'-DDD 


50-29-3---------4#4'-DDT 

72-43-5 --------- Methoxy or 

53494-70-5 ------ Endrin ketone 



R7 n'%-7A-9-------nA A.f4%1 ^. AA"A 

8001-35-2 ------- Toxaphene 

12674-11-2 ------ Aroclor-101 

11104-28-2 ------ Aroclor-122 

11141-16-5 ------ Aroclor-123 

53469-21-9 ------ Aroclor-124 

12672-29-6 ------ Aroclor-124 

11097-69-1 ------ Aroclor-125 

11096-82-5 ------ Aroclor-126 

,SID S 

Vo p e 

C 0``^ 1 71"-r 

1.71U 

1.71U 

1.71U1 

1.71U 

1.71U 

1.71U 

1.71U 

3.41U 

3.41U 

3.41U. 

3.41U 

3.41U 

3.41U 

3.41U 

17 1U 

3.41U 

3.41U 

1.71U 

1.71U 

170 1 U 

34 1U 

68 IU 

34 1U 

34 IU 

34 1U 

34 1U 

34 1 

FORM I'PEST 3/90 

116 

811-1

1D 



000074 


807099 

Lab Code: TMALA Case No.: 12047 SAS No.: N_ SDG No.: N_ 

d 


Lab Sample ID: A2 12047-078 

Sample wt/vol: 30.4 (g/RL) Q_ Lab File ID: 

% Moisture: 4 decanted: (Y/N) I^_ Date Received: 12/14/92 

Extraction: (SepF/Copt/Sonc) SONC Date Extracted: 12/21/92 

Concentrated Extract Volume: 5000 1L) Date Analyzed: 01/06/93 


GPC Cleanup: (Y/N) Y pH: 9.0 Sulfur Cleanup: (Y/N) N 


CAS NO. COMPOUND (ug/L or ug/Rg) UG/RG Q. 

319-84-6--------alp 

319-85-7--------bet 

319 -86-8--------del 

58-89-9---------clam 

309-00-2 -------- Aldrin 


959-98-8 -------- Endosulfan I 

60-57-1 --------- Dieldrin 

72-55-9 ---------- 4,41-DDE 

72-20-8 ---------Endrin 

33213-65-9------Endosulfan II 

72 -54-8 ------- --4,4'-DDD 

1031-07-8 ----- --Endosulfan sulfate 

50-29-3---------4,4'-DDT 

72-43-5 ------- --Methoxych or 

53494-70-5 ------ Endrin ketone 




8nnl-35-2 ------- TrVA"harw 

12674 

11104 

53469-21-9 ------ Aroclor-124 

12672-29-6 ------ Aroclor-124 

FORM I PEST 

1.71U.T 

1.7IU 

1.7IU 

1.7IU 

1.7IU 

1.7IU 

1.7IU 

1.7IU 

3.4IU 

3.41U 

3.4IU 

3.4IU 

3.4IU 

3.4IU 

3.4IU 

17 JU 

3.41U 

3.4IU 

1.7IU 

1.7IU 

170 III 

34 IU 

69 IU 

34 IU 

34 IU 

34 JU 

34 IU 

34 IV 

3/90

iD 


Ab Name: THA/ARLI Contract: WHC I 

0000'75 


I 1 

I B07QBO I 

gab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: jam_ 

tatrix: (soil/water) 

ample wt/vol: 30.8 (q/mL) 0 

Moisture: 3 decanted: (Y/N) N 

:xtraction: (SepF/font/Sonc) SONC 


'njection Volume: 1.00 (UL) 

;PC Cleanup: (YIN) Y_ pH: 8.8 


Lab File ID: 





Sulfur Cleanup: (Y/N) ]1_ 


CAS NO. COMPOUND (ug/L or ug/Rq) UG/KG Q 

319-84-6 -------- alpha-BHC 

319-85-7 -------- beta-BHC 

319-86-8 -------- delta-BHC 

76-44-8-- 

309-00-2- 

1024-57-3 

959-98-8- 

72-55-9 ------- -- 4,41 -DDE 

72-20-8 ------- --Endrin 

33213-65-9 ------ Endosulfan II 

72-54-8 ------- --4t4'-DDD 

1031-07-8 ----- --Endosulfan sulfate 

50-29-3---------4j4'-DDT 

72-43-5 ----------Methoxych or 

53494-70-5 ------ Endrin ketone 


12674-11-2 ------ Aroclor-1016 

11104-28-2 ------ Aroclor-1221 

11141-16-5 ------ Aroclor-1232 

53469-21-9 ------ Aroclor-1242 

12672-29-6 ------ Aroclor-1248 

1.71tIT 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

3.31U 

3.31U 

3.31U 

3.31U 

3.31U 

3.31U 

3.31U 

17 JU 

3.31U 

3.31U 

1.71U 

1.71U 

170 IU 

33 JU 

67 JU 

33 IU 

33 IU 

33 JU 

33 JU 

33 III 

FORM I PEST 3/90. 

7fJ /7

000076 



B07QB1 i 

Lab Name: TMA/ARLI Contract: NBC. I I 

Lab Code: SMALa_ Case No.: 12047 SAS No.: NA SDG No.: K_ 

4atrix: (soil/water) SOIL 

Sample wt/vol: 30.8 (9/XL) Sr_ Lab File ID: 

Lab Sample ID: A212047-048_ 

% Moisture: 3 decanted: (Y/N) N Date Received: 12/14/92 


Concentrated Extract Volume: 

5000 (uL) Date Analyzed: 01/06/93 


GPC Cleanup: (YIN) Y _ PH: 8.4 Sulfur Cleanup: (Y/N) N 


CAS NO. COMPOUND (ug/L or ug/Rg) UG/KG Q 

319-8 

319-8 

58-89-9 

309-00-2 

60-57-1 --------- Dieldrin 

72-55-9 --------- 4,4' -DDE 

72-20-8 --------- Endrin 

33213-65-9 ------ Endosulfan II 

72-54-8 --------- 4,4'-DDD 


50-29-3---------4,4'-DDT 

72-43-5 --------- Methoxyc or 

53494-70-5 ------ Endrin ketone 


5103-74 

11104-28-2 ------ Aroclor-122 

11141-16-5 ------ Aroclor-123 

53469-21-9 ------ Aroclor-124 

12672-29-6 ------ Aroclor-124 

11097-69-1 ------ Aroclor-125 

11096-82-5 ------ Aroclor-126 

FORM I PEST 

1.711 

1.711 

1.71U 

1.711 

1.71U 

1.711 

1.71U 

1.711 

3.31U 

3.31U 

3.31U 

3.311 

3.31U 

3.311 

3.31U 

17 IU 

3.31U 

3.310 

1.71U 

1.71U 

170 IU 

33 IU 

67 IU 

33 IU 

33 IU 

33 IU 

33 IU 

33 IU 

3/90, 

114

1D 


000077 


I 

I 

i B07QB2 I 

ab Name: TMA/ARLI Contract: WHC I I 

,ab Code: TMALA Case No.: 12047 SAS No.: NA 

_ 

SDG No.: KA 

fatrix: (soil/water) SOIL 


;ample wt/vol: 30.6 (g/aL) G File ID: 

c Moisture: 4 decanted: (Y/N) K—Date Received: 12/14/92 

:xtraction: (SepF/Cont/Sonc) SONC Date Extracted: 12/21/92 

:oncentrated Extract Volume: 5000 (UL) Date Analyzed: 01/06/93 

:njection Volume: 1.00 (uL) Dilution Factor: JA 

;PC Cleanup: (YIN) Y_ pH: 9.7 Sulfur Cleanup: (Y/N) tN 


CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q: 

I I 

319-84-6 -------- alpha-BHC I 

I 

1.71UJ 

1 319-85-7 -------- beta-BHC I 1.7IU 

1 319-86- 8 -------- delta-BHC 1 1.71U 

1 58-89-9 --------- gamma-BHC (L ndane) 1 1.71U 

i 76-44-8---------Heptachlor i 1.71U 

1 309-00-2 -------- Aldrin 1 1.71U 

1 1024-57- 3 ------- Heptach or epoxlde i 1.71U 

1 959-98-8 -------- Endosulfan I 1 1.71U 

1 60-57-1 --------- Dieldrin 1 3.41U 

1 72-55-9 -------- - 4,4' -DDE 1 3.41U 

1 72-20-8 -------- -Endrin 1 3.41U 

1 33213-65-9 ------ Endosulfan II I 3.41U 

1 72-54-8 --------- 4 # 4'-DDD I 3.41U 


1 50-29-3---------4f4'-DDT I 3.41U 

1 72-43-5 ---------- Methoxych or 1 17 IU 

1 53494-70-5 ------ Endrin ketone I 3.41U 

1 7421-36-3 ------- Endrin aldehyde I 3:41U 



1 8001-35-2 ------- Toxaphene 1 170 IU 

1 12674-11-2 ------ Aroclor-1016 1 34 1U 

1 11104-28-2 ------ Aroclor-1221 1 68 IU 

1 11141-16-5 ------ Aroclor-1232 1 34 IU 

1 53469-21-9 ------ Aroclor-1242 1 34 1U 

1 12672-29-6 ------ Aroclor-1248 1 34 IU 

1 11097-69-1 ------ Aroclor-1254 ( 34 

1 11096-82-5 ------ Aroclor-1260 I 34 IU 

IUD 


A'g 

y/ij

1D 


I B07QB3 

Ab Name: TMA/ARLI Contract: WHC I 

1111 


,ab Code: TMALA Case No.: 12047 

-. 


tatrix: (soil/water) SOIL 

Lab Sample ID: A212047-09B_ 

ample wt/vol: 30.7 (g/mL) G 


'.xtraction: (SepF/font/Sonc) SONC 

:oncentrated Extract Volume: 5000 (UL) 

Cnjection Volume: 1.00 (uL) 

;PC Cleanup: (Y/N) Y_ pH: 9.2 


Lab File ID: 




Dilution Factor: 1200 




319-84-6 -------- alpha-BHC 2.OIUT 

319-85-7--------beta-BHC 2.0 IU 

319-86-8 -------- delta-BHC ( 2.OIU 

58-89-9 --------- gamma-BHC (L ndane) 2.OIU 

76-44-8---------Heptachlor 2.OIU 

309-00-2 ------ --Aldrin 2.OIU 

1024-57-3-------Heptachlor epoxide 1 2.OIU 

959-98-8 -------- Endosulfan I 2.OIU 

60-57-1 --------- Dieldrin 3.91U 

72-55-9 ------- --4,4'-DDE 3.91U 

72-20-8 ---------Endrin 3.91U 

33213-65-9 ------ Endosulfan II 3.91U 

72-54-8 -------- -4,4 1 -DDD 3.91U 

1031-07-8 ------- Endosulfan sulfate 3.91V 

50-29-3---------4,4'-DDT 3.91U 

------- Methoxychlor or 20 IU 

53494-70-5 ------ Endrin ketone 3.9IU 

7421-36-3 ------- Endrin aldehyde 3.91U 

5103-71-9-------alpha-Chlordane 1 2.OIU 

5103-74-2-------gamma-Chlordane 1 2.OIU 

8001-35-2 ------- TOxaphene 1 200 IV 

12674-11-2 ------ Aroclor-1016 I 39 IU 

11104-28-2 ------ Aroclor-1221 I 79 IU 

11141-16-5 ------ Aroclor-1232 1 39 ID 

53469-21-9 ------ Aroclor-1242 1 39 IV 

12672-29-6 ------ Aroclor-1248 1 39 IU 

11097-69-1 ------ Aroclor-1254 i 39 IU 

11096-82-5 ------ Aroclor-1260 1 39 

I 

FORM I PEST 3/90. 

IU 

I 

P/3 

Y1/l1

000079 



I I 

1 B07QBB 1 

,ab Name: TMA/ARLI Contract: WHC I I 

,ab Code: TMALA Case No.: 12047 SAS No.: NA SDG No.: Imo_ 

tatrix: ( soil/water) SOIL Lab Sample ID: A212047-108 

:ample wt/vol: 30.4 (9/ML) G Lab File ID: 

c Moisture: 5 decanted: ( Y/N) N_ Date Received: 12/14/92 

extraction: ( SepF/Copt/Sonc) SONC Date Extracted: 12/21/92 

:oncentrated Extract Volume: 5000 ( uL) Date Analyzed: 01/06/93 

Cnjection Volume: 1.00 (uL) Dilution Factor: 1.00 

;PC Cleanup: ( Y/N) Y_ pH: 8.4 Sulfur Cleanup: ( Y/N) 



319-84-6- 

319-85-7- 

319-86-8- 

58-89-9-- 

76-44-8-- 

309-00-2- 

1024-57-3 

72 -55-9---------4,4' 

33213-65-9 ------ Enda 

72 -54-8---------4t4' 

1031-07-8 ------- Enda 

50-29-3---------4,41 

7421-36-3 ------- Endrin 

12674-11-2 ------ Aroclor-1016 

11104-28-2 ------ Aroclor-1221 

11141-16-5 ------ Aroclor-1232 

53469-21-9 ------ Aroclor-1242 

12672-29-6 ------ Aroclor-1248 

1109 

1.81UT 

1.81U 

1.81U 

1.81U 

1.81U 

1.81II 

1.BIU 

1.SI U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

18 IU 

3.41U 

3.41U 

1.81U 

1.81U 

ISO IU 

34 IU 

70 III 

34 IU 

34 IU 

34 IU 

34 IU 

34 1U 


0 

^1Z ^,

000080 



I I 

B07QB9 1 

Ab Name: TMA/ARLI Contract: WHC I i 

Ab Coda: rya_ Case No.: 12047 SAS No.: NA SDG No.: NA 

tatrix: (soil/water) SOIL 

ample wt/vol: 30.7 (g/aL) Q Lab File ID: 


Moisture: _4 decanted: (YIN) N_ Date Received: 12/14/92 

:xtraction: (SepF/font/Sonc) SONC Date Extracted: 12/21/92 



;PC Cleanup: (YIN) Y pH: 9.3 Sulfur Cleanup: (Y/N) N_ 


CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q, 

I 1 319-84-6 -------- alpha-BHC 

319-85-7 -------- beta-BHC 

1 319-86-8 -------- delta-BHC 

1 58-89-9 --------- gamma-BHC (L ndane) 

1 76-44-8---------Heptachlor 

1 309-00-2 -------- Aldrin 

1 1024-57-3-------Heptachlor epoxide 

959-98-8 -------- Endosulfan I 

1 60-57-1 --------- Dieldrin 

1 72-55-9 --------- 4,41 -DDE 

1 72-20-8 --------- Endrin 

1 33213-65-9 ------ Endosulfan I1 

1 72-54-8 --------- 4,41-DDD 

1 1031-07-8 ------- Endosulfan sulfate 

1 50-29-3---------4,41-DDT 

1 72-43-5 --------- Methoxy or 

i 53494-70-5 ------ Endrin ketone 

1 7421-36-3 ------- Endrin aldehyde 

1 5103-71-9-------alpha-Chlordane 

1 i7/1Q-9d-9-------'.a. .-/.1.l w"A.- A 

12674-11-2 ------ Aroclor-1016 

11104-28-2 ------ Aroclor-1221 

11141-16-5 ------ Aroclor-1232 

53469-21-9 ------ Aroclor-1242 

12672-29-6 ------ Aroclor-1248 

11097-69-1 ------ Aroclor-1254 

11096-82-5 ------ Aroclor-1260 

FORM I PEST 

1.71W 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

1.71U 

3.41U 

3.41U 

3.41U. 

3.41V 

3.41U 

3;41U 

3.41U' 

17 JU 

3.41U 

3.41U 

1.71U 

1.71U 

170 JU 

34 IV 

68 IV 

34 1U 

34 1U 

34 JU 

34 JU 

34 III 

3/90

'` 000081 

1D 



J I 

I B07000 I 

Lab Name: TMA/ARLI Contract: WHC I J 

Lab Code: TMALA_ Case No.: 12 047 SAS No.: NA SDG No.: NA 


Sample wt/vol: 30.7 (g/mL) G Lab File ID: 

Moisture: 5 decanted: (Y/N) N_ Date Received: 12/14/92 


Concentrated Extract Volume: 5000 (uL) Date Analyzed: 01/06/93 


GPC Cleanup: ( Y/N) Y_ pH: 9.4 Sulfur Cleanup: (YIN) tN 


CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q. 

319-84 -6 -------- alpha -BHC I 1.7JUS' 

319-85-7 -------- beta-BHC I 147 

319-86-8 -------- delta -BHC J 1.7JU 

58-89-9 --------- gamma -BHC (L ndane) J 1.7 1 U 

76-44-8---------Heptachlor J 1.7 1 U 

309-00-2 -------- Aldrin I 1.7I U 

1024-57 - 3-------Heptachlor epoxide I 1.7 1 U^ 

959-98-8 -------- Endosulfan 1 J 1.7 U1 

60-57-1 --------- Dieldrin J 3.4JU( 

72-55-9 --------- 4,4'-DDE I 3.4JUtF[ 

72-20-8 --------- Endrin J 3.4JU t 

33213-65-9 ------ Endosulfan II J 3.4IU^ 

72-54-8 --------- 4,4'-DDD J 3.4JU 

1031-07-8 ------- Endosulfan sulfate ( 3.4 1 II. 

50-29-3---------4,41-DDT ( 3.4JU 

72-43-5 --------- Methoxych or J 17 JU 

53494-70-5 ------ Endrin ketone J 3.4JU 

7421-36-3 ------- Endrin aldehyde J 3.4JU 

5103-71-9------ -alpha-Chlordane J 1.7JU 

5103-74-2-------gamma-Chlordane J 1.7JU 

8001-35-2 ------- Toxaphene J 170 JU 

12674-11-2 ------ Aroclor-1016 I 34 JII 

11104-28-2 ------ Aroclor-1221 J 69 I UI 

11141-16-5 ------ Aroclor-1232 ( 34 JUf 

53469-21-9 ------ Aroclor-1242 J 34 J U 

12672-29-6 ------ Aroclor-1248 J 34 JU ' 

11097-69-1 ------ Aroclor-1254 J 34 Jul 

1 11096-82-5 ------ Aroclor-1260 J 34 JW 

FORM I PEST 

3/90

1 00P('05 

IA EPA BAXPLZ NCO. 


Lab Name: TMA/ARLIContract: NHC 

B07aw 

Lab Code: TMAjii _ Case No.: 12074 SAS No.: NA SDG No.: NA 

Matrix: ( soil/vater) SOIL 

_ 


Sample wt/vol: 5.0 (g/ML) G Lab File ID: 21223811 

Leval: ( lov/med) LOW 





74-87 

75-01-4-------- -Vinyl 


67-64-1---------Acetone 


75-35-4-------- -1,1-Dichloroethene 

75-34-3 --------- 1,1-Dichloroathans 

540-59-0 -------- 1 , 2-Dichloroethens (total)_ 

107-06-2 -------- 1 , 2-Dichloroethans 

78-93-3 --------- 2-Butanone 

71-55-6---------1 , 1,1-Trick oroethane 



78-87-5---------1 , 2-Dichloropropane 

79-00-5 --------- 1,1,2-Trichioroethane 

10061-02-6------trans-1, 

79-34-5 ---- -- --- 1,1,2 , 2-Tetrachloroethans 

108-88-3--------Toluene 


100-41-4-- ------Ethylbenzene 

100-42-5--------Styrene 

1330-20-7-------Xyiene (total) 

Date Received &- --12/21/92 



11 III 

11 III 

11 ju 

it III 

2 IJ 

11 (II 

11 III 

11 III 

11 III 

11 j II 

11 jII 

11 III 

11 III 

11 jII 

11 III 

it ÎI 

11 ÎI 

it III 

11 III 

11 III 

11 III 

11 III 

11 III 

11 III 

11 j II 

11 III 

it III 

4 IJ 

11 j II 

it III 

11 III 

11 III 

1.0 

Soil Aliquot Volume: — (UL) 


(ug/L or ug/Rg) UG/KQ 4 

U ./^Zr3 

FORM I VOA 3/90

0 

1Z 

VOLATILE ORGANICS ANALYSIS DATA BNEET 


Lab Name: TSA/ARLI Contract: ml 

00 11 0('6 

3PA SAMPLE 310. 

807QB5 

Lab Code: THAj A _ Case No.: 12 074 SAS No.: NA SDG No.: KA 

Matrix: (soil/eater) SOZL 

d 

Lab Sample ID: A2 12074-05A 

Sample et/vol: 5.0 (q/mL) G Lab File ID: 21223R11 

Level: (low/med) WW _ Date Received:- 12/21/92 

% Moisture: not doe. —2 Date Analyzed: 12/23/92 




Dilution Factors 1.0 



(ug/L or uq/Kq) UG/KG 

FORK I VOA-TIC 

I I I 

RT i EST. CONC. I Q I 

Î IRmI 

I I I 

0 

3/90


000007 


( 1 

807QB6 1 

Lab Name: TRA/ARLI Contract: NHC I 1 

Lab Code: MI&L&_ Casa No.: 12074 SAS No.: NA SDG No.: 

4 


Lab Sample ID: A212074-0GA 

Sample wt/vol: 5.0 (q/mL) G Lab File ID: 21223812 

Level: ( low/med) TOW Date Raceivad:-- 12/21/92 

t Moisture: not doe. _^3, Date Analyzed: 12/23/92 




74-87-3 --------- Chlorcaathan 

74-83-9 --------- Bromomsthane 

75-01-4---------Vinyl Chlori 


67-64-1---------Acetone 

75-15-0---------Carbon D sulf de 

75-35-4 --------- 1,1-Dichloroothens 

75-34-3 --------- 1,1-Dichloroothana 

67-66-3 --------- Chl 

107-06-2--------1,2 

..n _n n - --------- -n 

71-55-6 --------- 1,1,1-Tri oroethane 


75-27-4 --------- Broaddichloromathans 

10061-0 

124-48-1 ------- Dibz 

79-00-5 --------- l,l, 

71-43-2---------Bang 

10061-02-6------tray 

75-25-2---------Bros 

108-10-1 -------- 4-Ne 

12 

it 

108-90-7--------Chlorobenzene 

100-41-4 ------- Ethylbenzens 

100-42-5--------Styrene 

1330-20-7 ------- %ylens ( total) 

FORM I.VOA 


(uq/L or uq/Kq) UG/RG Q 

10 1U 

10 1U 

10 1U 

10 1U 

2- IT 

12 JZ- 

10 1U 

10 III 

10 III 

10 1U 

10 III 

10 1U 

10 1U 

10 1V 

10 1U 

10 IV 

10 IV 

10 1V 

10 1V 

10 1U 

10 1V 

10 IU 

10 III 

10 1V 

10 1V 

10 1V 

10 1U 

10 IV 

11 1 

10 III 

10 III 

10 1U 

10 1U 

4;1- 

G 

i 

Ate 

,qlK/ ,^ 

3/90. 

Y

000008 

u IPA Slu@LE IUD. 



I 807036 

Lab Name: TNA/A Tff Contract: NBC I 

Lab Code: THALa_ Case No.: 12074 SAS No.: NA SDG No.: Z — 


Sample wt/vol: S.0 (g/NL) G_ 

Level: (low/mad) L0M 

4r Moisture: not doe. _3 



Number TICs found: Q 

Lab File ID: 21223R1 2 




soil Aliquot Volumes (uL) 



CAS NUMBER COMPOUND NAME RT EST. CONC. 

AA 

41is`r3 


a

Lab Name: 

000009 

lA EPA SAMPLE NO. 

VOLAITILE ORGANICS ANALYSIS DATA SKEET 

Lab Code: MQL&_ Cass No.: 12074 s,> 



Level: (low/med) S8K_ 

E Moisture: not dec. _ 6 



I 

174-87-3 --------- Chloromethan, 

174-83-9---- ----- Bromomethans 

175-01-4---------vinyl ChlorIJ 

175-00-3-- ------- Chloroethans 

175-09-2 --------- Nethylene Ch 


75-35-4 --------- 1,1-Dichloroethsns 

75-34-3 --------- 1,1-Dichloroethanei 

540-59-0 -------- 1,2-Dichloroethena 

107-06-2 -------- 1,2-Dichloresthane 

78-93-3 ----- ----2-BUtanons 


56-23-5---------Carbon Tetrachlorids 

75-27-4---------Bromodichloromethane 

10061-0 

79-00-5 --- -- ---- ltl, 

10061-02-6------trans-1, 

591-78-6 -------- 2-Sexanons 

127-18-4---- ---- Tetrachlor 

79-34-5---------1,,1,,2j2-Ts 

I I B07QD7 

Contract: NBC I 

SAS No.: jQ1_ SDG NO.: H&— 

Lab Sample ID: A212074-OLA 

G Lab File IDS 21223ROS 

Date Receivedr' 12/21/92 




CONCENTRATION 4 

UNITS: 


11 

11 

11 

11 2 

12 

11 

11 

11 

it 

11 

11 

11 

2 

it 

it 

11 

11 

11 

li 

11 

11 

11 

11 

11 

11 

11 

it 

11 

11 

11 

11 

11 

U UUJ 

U 

J 

U 

H 

H 

U 

U' 

U 

II 

II 

U 

FORM I VOA 3/90 

AA 

00S

000clo 

u EPA SAIQW No. 



B07Q97 

Lab Names TMA/ARLI Contract: W HC ( 1 

Lab Code: TH&JA Case No.: 12074 SAS No.: NA SDG No.: M 


d 

Lab Sample ID: A2 12074-OIA 

Sample wt/vol: 5.0 (q/mL) G Lab File ID: 21223R05 

Level: (low/Red) LOW_ Date Received:--•12/21/92 

i Moisture: not dac. _¢ Date Analyzed: 12/23/92 

GC Column: PACK IDs 2.00 (mm) Dilution Factor: 1.0 

Soil Extract Volume: (uL) Soil Aliquot Volumes (uL) 

=NCENTRATION UNITS: 

Number TICS found: _Q (uq/L or uq/Xq) UG/KG 

CAS NUMBER COMPOUND NAME RT I EST. CONC. i Q 

»^ ^ l ono 

Z0 

A4 

17, 

'Al'? 

1 


9

lA EPA SAMPLE W. 


I I 

I E07QDB I 

Lab Nana: TMA/ARLI Contract: NBC I I 

Lab Code: TMALA Casa No.: 12074 SAS No.: NA SDG No.: ô 



5.0 (g/mL) G 

Level: ( low/med) LON_ 

i Moisture: not dec. 4 




Lab File ID: 

21223ROS 

Date Received:- -12/21/92 





CAS NO. COMPOUND (ug/L or ug/Rg) OG/RG 

74-87-3 --------- Chlor 

74-83-9 --------- Bromo 

75-01-4---------Vinyl 


67-64-1---------Acetone 

75-15-0---------Carbon D auli de 

75-35-4 -------- 1,1-Dichloroethene 


540-59-0 -------- 1 , 2-Dichloroothene (total)_ 

107-06-2--------1, 

71-55-6---------1,1,1-' 

56-23-5---------Carbon 

75-27-4---------Bromod 


71-43-2---------Benzene 

10061-02-6 ------ trans -1,3-D chloropropene 

79 -34-5---------1,1,2, 

100-41-4 -------- Ethylbe 

100-42-5--------Styrene, 

1330-20-7-------Xylem 

FORM I VOA 

10 

10 

10 

10 2 

14 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 

10 1 

10 

10 

10 

10 

U UUUUUUUUUUUUUUU 

U 

U 

Ll^ 

7


lE 

VOLATILE ORGANICS ANALYSIS DATA SSEET 


Moisture: not doe. _t 

GC Column: PAC ID: 2.00 (mm) 


Number TICS found: _ Q 

Contract: WHC 

00volz 

EPA SAMPLE N0. 

1 1 

B07QDD ) 

I i 


>s 

Matrix: (soil/vater) SOIL 


Sample wt/vol: 5.0 (9/ML) G_ 

Lab File ID: 21223ROa 

Level: (low/med) jam_ 

Date ReCeiVed:"'12/21/92 





(ug/L or uq/Kg) UG/XG 

I I I I I I 

CAS NUMBER I COMPOUND NAM I RT I EST. CONC. I 4 

i I I I I I 

FORM I. VOA-TIC 

3/90

Lab Name: 

u 


Lab Code: TNALa Case No.: 12074 


Sample wt/vol: 5.0 WAL) 

Level: (low/med) Imo_ 

t Moisture: not doe. _3 




DATA SBEET 

000013 


1 i 

i Bo7QD9 I 

Contract: MC 1 I 

SAS No.: NA SDG No.: MA 


s^ Lab File ID: 21223R09 

Date Received:-- 12/21/92 





(uq/L or uq/Kg) UG/RG 76b 

74-87-3 --------- Chloromethane j 10 I^ 

74-83-9 --------- Bromomethane 1 10 IQ 

75-01-4---------Vinyl Chloride I 10 

III 

75-00-3 --------- Chloroethans I 10 IV 

75-09-2---------Methylene Chlor de i 10 IV 

67-64-1---------Acetone I 12 JX&f 

75-15-0---------Carbon Disulfide 1 10 IU 1 

75-35-4 --------- 1,1-Dichloroethens I 10 IV 1 

75-34-3 --------- 1,1-Dichloroethans I 10 III 1 

540-59-0 -------- 1,2-Dichloroethene (tota )_1 10 IQ 1 

67-66-3 --------- Chlorotors I 10 III 1 

107-06-2 -------- 1,2 -Dichloroethans 1 10 J u 1 

78-93-3 --------- 2-Butanons 1 10 I U 1 

71-55-6 --------- 1,1,1-Trichlorosthane I 10 III 1 

56-23-5---------Carbon Tetrachloride 1 10 IU 

75-27-4 --------- Bromodichloromethane 1 10 III 1 

78-87-5 --------- 1,2-Dichloropropane 1 10 III I 

10061-01-5 ------ cis-1,3-Dichlorcpropens I 10 III 1 

79-01-6 --------- Trichiorosthene 1 10 IV 1 

124-48-1 -------- Dibromochlorome ans 1 10 III 1 

79-00-5 --------- 1,1,2-Trichlorosthane I 10 I V1 

71-43-2---------Benzene 1 10 III 1 

10061-02-6 ------ trans-1,3-D ch oropropene 1 10 IV 1 

75-25-2 --------- Bromolorm 1 10 III 1 

108-10-1 -------- 4-Methyl-2-Pentanone 1 10 Iv 1 

591-78-6 -------- 2-Nexanone 1 10 IV 1 

127-18-4 -------- Tetrachloroethens 1 10 III 1 

79-34-5 --------- 1,1,2 , 2-Tetrachloroethans 1 10 IV 1 

108-88-3--------Toluene 1 10 1II 1 

108-90-7 -------- Chlorobenzene I 10 IV 1 

100-41-4 -------- Ethylbanzens 1 10 IV 1 

100-42-5--------Styrene 1 10 I V 1 

1330-20-7 ------- Xylene (total) 1 10 IU' I 

I I 

FORM I VOA 3/90

Lab Naas: TMA/ARLI 

000i2*s 

lE EPA SAMPLE NO. 



Lab Code: THAj,a _ Came No.: 12074 



Level: (low/mad) LOW_ 





I B07QD9 

Contract: WHC i 










I I I I I 


I I I I I 


J

000015 

lA EPA SAME 110. 

VOUTILE ORGANICS ANALYSIS DATA SHEET 

I I 

I B07QFO I 

Lab Naas: TNA/ARLI Contract: WHC I I 

Lab Coda: TMALa_ Cass No.: 12074 SAS No.: NA SDG No.: NA _- 


Sample wt/vol: 5.0 (q/aL) G File IDs 2 12 23R10 

Level: (lov/mod) LOW_ Date Received: •- 12/21/92 

s Moisture: not doe. 2 Date Analysed: 12/23/22 



CAS NO. 

74 


75-00-3 ----- ----Woroethans 

75-09-2 --------- Ksthylene Chloride 

67-64-1---------Acetone 

75-15-0---------Carbon D sul! de 

75-35 -4 --------- 1,1-Dichloroethene 

75-34-3 --------- 1,1-Dichloroethano 

107-06-2--------1, 

71-55-6 --------- l,l,l-! 

56-23-5---------Carbon 

76-87-5---------1 

79-00-5 --------- l,l, 

10061-02-6----- -trans-1,3-D chloropropene 

75-25-2 --------- Bromotorm 

108-10-1 -------- 4 -Kethyl-2-Pentanons 

79-34-5---------1,1,2, 

FORK I VOA 


Soil Aliquot Volume: — (UL) 


(u9/L or u4/R9) UGZKQ QlI/^ 

10 III 

10 III 

10 III 

10 III 

10 III 

13 

10 UII 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III_ 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 III 

10 IV - 

10 III 

10 III 

10 IV- 

3/90.-

OW SIG 

is sPA SAMPLE 70. 



507QFO I 

Lab Name: TMA/ARLI Contract: NHC 

Lab Codi: Zffkj,_ Case No.: 12074 SAS No.: K_ SDG No.: Imo_ 


Sample wt/vol: 5:0 (q/mL) g_ Lab File ID: 21223RIO 

Level: (low/med) "M__ Date Received: - 12/21/92 

i Moisture: not dec. _ 2 Date Analyzed: 12/23/92 


Soil Extract Volume: (UL) Soil Aliquot Volumes —(UL) 



CAS NUMBER 

I I I 

RT I EST. CONC. ( Q I 

e3 

r 

I I I 

q3 

FORM I"VOA-TIC * 3/90

000017 

la EPA SAXPLa NO. 


I I 

I B07QN 1 

Lab Name: M/ARLI Contract: IMC I i 

Lab Code: TKhrA Case No.: 12074 SAS No.: NA SDG No.s 


Sample wt/vol: 30.1 (9/KL) Q _ Lab File ID: 30125807 

bevel: (low/med) LOM Date Received":-' - 12/21/92 

4 Moisture: _ 9 decanted: (Y/N) ^- Date Extracted: 12/23/92 

Concentrated Extract Volume: 500.0 (uL) Date Analyzed: 0,/25/93 

injection volume: 2.0 (UL) Dilution Factor: 1.0 



CAS NO. COMPOUND (u9/L or u9/Kg) UG/KG Q 

I 1 1 I 

108-95-2 

360 III 1 

95-57-8---------2-C 

541-73-1--------1,3 

106-46-7--------1,4 

95-50-1---------1,2 

108-60-1--------2,2' 

106-44-5--------4-Me 

621-64-7--------N-N1 

98-95-3---------Ni 

105-67-9 -------- 2,4- 

111-91-1 ------- bis( 

120-83-2 -------- 2,4- 

120-82-1--------1,2. 

87-68 

77-47-4 --------- Hexa 

88-06-2---------2,4, 

95-95-4---------2,4, 

99-09-2---------3 

83 -32-9---------A 

51-28-5---------2 

( 

360 

360 

360 

360 

IU 

1U 

IV 

IV 

360 IV 

360 III 

360 Iv 1 

360 IV 1 

360 III 1 

360 III 1 

360 1U 1 

360 IV 1 

360 U 

360 JU 1 

360 III 1 

360 III 1 

360 III 1 

360 III 1 

360 IV 1 

360 1U 1 

360 IU 1 

360 IV 1 

360 III 1 

360 III I 

88o III 1 

360 IV 1 

880 I II 1 

360 III 1 

360 I II I 

880 IV 1 

360 1U, I 

880 IV I 

I rf 

1 

1 y^^sr

000018 

1C spa SANMW NO. 

SEMIVOrATILE ORGANICS ANALYSIS DATA SHEET 

Lab Name: TMA/ARLI Contract: NHC 

B07QB5 

Lab Code: Tom_ Case No.: 12074 SAS No.: NA SDG No.: H&_ 

Matrix: ( soil/eater) SOIL Lab Sample 10: A212074-058 

Sample wt/vol: 30 . 1 (q/mL) G 

Level: ( low/sad) IW 

i Moisture: _9 decanted: (Y/N) N 



GPC Cleanup: (YIN) X-- pH: 8.9 


100-0 

121-14-2--------2, 

606-20-2 -------- 2. 

86-7 

534-52-1--------4,6- 

86-30-6---------N-Ni 

118-74 -1 -------- Nexaehlorobenzene 


85-01-8 --------- Phenanthrene 

120-12-7 -------- Anthracene 

84-74 

91-94 -1 ------- --3,3'-Dichlorobenzidine 

56-55-3 --------- Senzo(a)Anthracene 

117-81-7 -------- bis(2-Ethylhexyl ) Phthalate 

117-84-0 -------- Di-n-OCtyl Pht 

205-99-2 -------- Benzo(b)Fluora 

207-08-9 --- -- --- Benzo(k)Fluora 

50-32-8 --------- Benzo (a)Pyrene 

193-39-5--------Indeno(1,2,3- c 

53-70-3 --------- Dibenz(a,h)Ant 

191-24-2 -------- Benzo(q,h,i)Pe 






CONCENTRATION UNITS: i 

(uq/L or uq/Rq) UG/KG Q 

880 JU 

360 JU 

360 JU 

360 JU 

360 (U 

360 JU 

360 JU 

880 J U 

880 I V 

360 19 

360 JU 

360 JU 

880 JU 

360 JU 

360 J U 

360 j U 

?60140- IV 

360 III 

360 JU 

360 J U 

360 J U 

360 IV 

360 JU 

360 IV 

360 JU 

360 JU 

360 J U 

360 JU 

360 1U 

360 I V 

FORM I -SV-2 3/90 

1.1 

q^/5. 

, -f

OOne19 

17sPA SAMPLS CFO. 



807QU 

Lab Names TMA/7 ►RLI Contracts MRC I 

Lab Coda: TMALA Cage No.: 12074 SAS No.: !Ul.._ SDG No.: NA 


Sample wt/vol: 30.1 (g/RL) G Lab File IDs 30125S07 

Level: ( low/med) LOW Date Received!- • 12,/21/92 

i°Ncistures _9 decanted: (YIN) N Date Extracted: 12/23/92 

Concentrated Extract Volumes 500.0 (UL) Date Analyzed: 01/25!93 

Injection Volume: 2.0 (UL) Dilution Factors 1.0 

GPC Cleanup: (YIN) Y_ 

PH: 8.9 


Number TICS found:, (ug/L or ug/Kg) nG/xc 

1 

1 

1' 

1 

1 

i 

CAS NUMBER i COMPOUND NAME i RT i EST. CONC. i Q 

2. 

3 . 

4. 

. 

S 

5 . 

7 

8.. 

9. 

1UNKNOWN HYDROCARBON 1 5.25 1 470 IJ 

( UNKNOWN HYDROCARBON 1 5.85 1 1900 v 

1 UNXNOWN HYDROCARBON 1 5.90 

( 580 4 

1UNKNOWN HYDROCARBON ( 6.00 1 1600 LWttI 


1 7.73 91900 Ij' ^ I 

UNKNOWN HYDROCARBON LA I 

tA I 

1 UNKNOWN HYDROCARBON 1 9.05 1 260 W 

1PROPANOIC ACID ISOMER 1 18.35 1 220 1J I 

1 

I UNXNOWN CARBOXYLIC ACID ESTEI 21.42 1 110 1 I 

1 10. 

(UNKNOWN ArXANE 1 28.37 1 73 

11. 

1JJ CA 

1 

I 

UNINOWN ALEANE i 30.48 i 150 1 

FORK I SV-TIC 3/90

000020 

is spa amu s so. 

SEMIVOLATILE ORGANICS ANALYSIS DATA 8B1 

I I 

I B07QBS J 

Lab Name: TMA/ARLI Contract: RHC 1 I 

Lab Cods: TMALA Case No.: 12074 SAS No.: NA_ 8DG No.: KL_ 


_ 


Sample wt/vol: 31.0 (q/mL) ¢_ Lab File ID: 30125808 

Level: ( low/wed) ;Q_ Date Recsivsdr 1,2121/92 






CAS NO. COMPOUND ( uq/L or uq/Xq) UG/XG Q 

108-95-2--------Phenol J 330 J U 

111-44-4 -------- bis(2-Chlorosthyl ) Ether J 330 IV 

95-57-8---------2-Chlorophenol J 330 JU 

541-73-1 -------- 1,3 -Dichlorobenzens i 330 JU 

106-46-7 -------- 1,4 -Dichlorobenzene J 330 JU 

95-50-1 --------- 1,2-Dichlorobanzene J 330 JU 

95-48-7 -------- 2-Nethylphsnol J 330 IV 

108-60-1 -------- 2,2 1 -oxybis ( 1 croprcpane) _ I 330 IV 

106-44-5 -------- 4-Methylphenol i 330 IV 

621-64 -7 -------- N-Nitroso-Di-n-Propyl ne_J 330 JU 

67-72-1 --------- Hexachloroethane J 330 JU 

98 -95 -3---------Nitrobenzene J 330 JU 

78-59-1 ------ ---Isophorone J 330 III 

88-75-5 ------ ---2-Nitrophenol J 330 JU 

105-67-9 ------- 2,4-Dimethylphenol J 330 JU 

111-91-1 -------- bis ( 2-Chlorosthoxy)Nethane_ J 330 IV 

120-83-2 ------- 2,4-Dichlorophanol I 330 JU 

120-82-1--------1,2 0 4-Trichlorobenzene ( 330 JU 

91-20-3-------- -Naphthalene J 330 IV 

4-Moroaniline 

-------- ne J 330 JU 

87-68-3 --------- Hexachlorobutad eno ( 330 JU 

59-50-7 --------- 4-Chloro-3-Methylphenol J 330 JU 

91-57-6 --------- 2-Methylnaphthalene J 330 JU 

77-47-4 --------- Nexachlorocyclopentad — end— J 330 JU 

88-06-2 ---------- 2,4 , 6-Trichlorophenol J 330 JU 

95-95-4--- ------ 2,4,5-Trichlorophenol J 800 JU 

91-58-7---------2-Chloronaphthalene J 330 JU 

88-74-4---------2-Nitroaniline I 800 IV 

131-11-3--------Dimethylphthalate J 330 JU 

208-96-8 -------- Acenaphthylene J 330 JU 

99-09-2 --------- 3-Nitroaniline J Soo IV 

83-32-9 --------- Acenaphthene 330 III 

51-28-5 --------- 2,4-Dinitrophencl I 800 JU 

^^îz

lc 

SEKIVOLATILE ORWXCS ANALYSIS DATA SHEET 

000021 

sPA SAMPLE NO. 

1 I 

I B07QB6 I 

Lab Name: TKA/ARLI Contract: WHC I I 

Lab Code: THAU Casa No.: 32074 SAS No.: N_ SDG No.: ga_ 

Matrix: ( soil/water) ,oiL Lab Sample ID: A2 12074-068 

Sample wt/vol: 31.0 (q/mp G Lab File ID: 30125808 

Level: ( low/nod) U_ Data Receivedr --12/21/92 

s Moisture: _3 decanted: (Y/N) N 





100-02-7 

121-14 -2 -------- 2,4-Dinitrotolue 

606-20-2 -------- 2,6-Dinitrotolua 

84-66-2 --------- Diethylphthalats 

7005-72-3 ------- 4 -Chlorophanyl-p 

86-73-7 --------- Fluorsna 

100-01-6 -------- 4-Nitroan^ 

534-52-1 -------- 4,6-Dinitro-2-=e 

86-30-6 --------- N-Nitrosodipheny 

118- 

87-8 

91-94-1---------3,3 

117-8 

205-99-2---- ---- Benzo(b)PI 

207-08-9 ------ --Benzo(k)F3 

50-32-8 --------- Benzo(a)Py 

193-39-5 ------- Indeno(1,2 

53-70-3 ----- ----DiboM (a,b 

191-24 -2 -------- Benzo(q,h, 

FORM I SV-2 


(ug/L or uq/Kg) UG/XG Q 

(1) 

33 a 

800 III 

330 1 

330 IU 

330 IU 

330 IU 

330 IU 

330 IU 

800 III 

800 IU 

330 III 

330 III 

330 III 

800 III 

330 III 

330 III 

330 III 

39 0 U 

330 III 

330 III 

330 III 

330 III 

55 IJ 

330 III 

330 IV 

330 IU 

330 III 

330 IU 

330 IV 

330 III 

330 1 

y'2 

3/90. 

46

0000?2 

is 

!PA SAMPLM NO. 

SENIVOLATILE ORGANICS ANALYSIS DATA SKEET 

TENTATIVELY IDENTIFIED COMPOUNDS ( I 

I B07QBG I 

Lab Saxe: TMA/ARLI Contract: WHC i i 

Lab Codas TMALA Case No.s 12074 SAS No.: NA SDG No.: 



Saxpla wt/vol: 3 1. 0 (q/RL) G Lab Pilo IDs 3212559a 

Level: (low/xed) U_ Data Received:- - 12/21/92 


Data Extracted: 12/2 3192 

Concentrated Extract volume: 500.0 (uL) Date Analyzed: 0,/25/93 

Injection volume: 2.0 (uL) Dilution Factor: 1.0 

OPC Cleanup: (YIN) Y _ pH: 8. 7 


Number TICS found: _]^ (uq/L or uq/Rq) UG KG 

CAS NUMBER I COMPOUND NAME 1 RT I EST. CONC. Q 

^^ 

. 

1. ÛMXNOWN HYDROCARBON 1 5.85 830 IJ 

2. IUNMIOWN HYDROCARBON 1 5.90 i 800 IJ^,,^ 

3. IUNXNOWN HYDROCARBON I 6.02 I 1500 I 

UNMTOWN HYDROCARBON I 6.57 ( 84000 U 

I ^.l 

5. IUNIOIOWN HYDROCARBON I 7.15 I 130 I 

6 0 IUN=OWN HYDROCARBON I 7.33 I 67 1J 

7. IUNXNOWN XETONE ( 7.73 1 1800 

S. IUNXNOWN HYDROCARBON 1 9.05 1 270 ^ u 

9. IUMXNOWN CARBOXYLIC ACID ESTEI 21.42 I 100 

10. 1UNSNOWN ALM= 1 26.73 1 130 1J 

11. 1UNXNOWN ALKANE I 28.38 ( 100 IJ 

12. IUNWOWN ALXANE i 30.48 1 130 1J 

6a 

c(f 15 /113 

FORM I SV ,-TIC 3/90

000023 

yN ZPA ahlOTE NO. 


I( 3070M ) 

Lab Naas: TKA/ABET Contract: NBC t I 

Lab Coda: THALA Casa No.: 12074 SAS No.: NA SDG No.: 10L_ 


Sample wt/vol: 30 . 4 (q/aL) G Lab File ID: ,30125SO3 

Level: ( low/wed) Date Received: 12/21/92 

i Moisture: _ 6 decanted: (Y/N) 2L 




Injection volume: 2.0(UL) Dilution Factor: 1.0 

pH: 9.3 

GPC Cleanup: (YIN) Y. 


. r.i . (uq/L or uq/Kq) UG/_$0 

350 

350 

350 

541-73-1--------1, 350 

106-46-7--------1, 350 

95-50-1---------18 350 

350 

108-60-1 -------- 2,2'-oxybis(1-Chloroproptine)_ 350 

350 

350 

350 

350 

350 

350 

105-67-9--------2#4 350 

111-91-1--------big 350 

350 

120-82-1--------1#2 350 

350 

106-4 350 350 

350 

350 

77-47-4 --------- Hexa 350 

88-06-2---------2#4# 350" 

95-95-4---------204f 840 

350 

840 

350 

350 

99-09-2---------3-Ni 840 

350 

840 

U 

II 

II U 

U 

U 

v UUUUUUUv 

U 

U 

U 

Q 5^ 

I 

I 

i 

1 

I 

I 

n^ 

qj,

00 00 24 

IC EPA smam 90. 

SENIVOLATILa ORGANICS AMALYSIS DATA SHEET 

Date Analyzed: Q1/25/93 



(uq/L or uq/Rq) UG/KG 0 

(1) 

840 

350 

350 

350 

350 

350 

350 

840 

840 

350 

350 

350 

840 

350 

350 

350 

0 

35 350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

350 

I 

I B07QD7 

Lab Name: TM/ARLI Contract: NEC I 

Lab Code: THAId_ Case No.: 12074 SAS No.: NA,_ SDG No.: Imo_ 

Matrix: (soil/water) gOIL Lab Sample ID: A212074-01D 

Sample wt/vol: 30.4 (9/ML) G_ 

Level: (low/Red) jE 



t Moisture: _-6 decanted: (Y/N) N 






I 

1 100-02-7 -------- 4-Nitrophenol_, 

1 132-64-9 -------- Dibenzoruran 

1121-14-2 -------- 2,4-Dinitrot 

1606-20-2 -------- 2.6-Dinitrotolum 

7005-72-3 ------- 4-Chlorophanyl 

86-73-7 --------- Fluorene 

100-01-6--------4-Nitroann=ne 

534-52-1 -------- 4.6-Dinitro-2 

86-30-6 --------- N-Nitrosodiphe 

101-55-3 -------- 4-Bromophenyl 

118-74-1--------Hexachlorobenz 

87-86-5 --------- Pentachlorophe 

85-01-8 --------- Phenanthrene 

86-74-8---------Carbazole 

84-74-2--- --- ---Di-n-Bnty 

206-44-0 -------- Fluoranth 

129-00-0 ---- ----Pyren4k__ 

91-94-1 --------- 3,3'-Dichlorobenzi 

56-55-3 --------- Benzo(a)Anthracens 

117-81-7 -------- bis(2-Ethylhexyl)P 

205-99-2 -------- Benzo(b)8luoranthene 


50-32-8 --------- Benzo(a)Pyrene 


53-70-3 ----- ----Dibenz(a,h)Anthracens 

191-24-2 -------- Benzo(q,h,i)Perylsne 

FORM I SV-2 

0 

U U U 

II 

U U 

II 

II 

W 

U 

II 

II 

U V 

U 

U I 

I 

3/90 

yu 

41 151

1! 

SENIVOLATILE ORGCS ANI ANALYSIS DATA SHEET 

TENTATIVELY IDENTIFIED COMPOUNDS 1 

vvvvG.1 

3PA. SAMPLN NO. 

307007 

Lab Name: TNA/ARLI Contract: VHC 1 

Lab Coda: 22 L1► Case No.: 12074 SAS No.: NA SDG No.: IM__ 

Matrix: ( soil/water) SOIL . Lab Sample ID: A212074-OID 

11 

Sample wt/Vol: 30.4 (VUL) G File ID: 30125503 

Level: (low/med) jgOL_ Date Received: 12 /21/92 

% Moisture: 6 decanted: (Y/N) N Date Extracted: 12/23/92 



GPC Cleanup: (Y/N) Y_ p8: 9.3 


Number TICs found: 9 (uq/L or ug/Rg) yG/KG 

1 

I CAS NUMBER 

I I 

I COMPOUND NAME ( 

I 

RT 1 EST. CONC. 

I I 

I Q i 

1 

1. UNKNOWN HYDROCARBON I 5.80 1000 Izf u 2. (UNKNOWN HYDROCARBON ( 5.87 i 980 IJ I 

1 3. (UNKNOWN HYDROCARBON I 6.00 i 1300 I,W W I 

i 4. ( UNKNOWN HYDROCARBON i 6.53 I 97000 1$; N I 

I 5. (UNKNOWN KETONE I 7.72 1 2000 1 Â I 

1 6. 1 UNKNOWN HYDROCARBON 1 9.03 I 350 1 Ar 1A I 

1 7. 1PROPANOIC ACID ISOMER 1 18.33 I 210 1J 1 

I 

I a. ( UNKNOWN CARBOXYLIC ACID ESTE I 21.37 I 100 Im 0 I 

I 9. 

IHEXANEDIOIC ACID ISOMER I 

140 IJ I 

I I 

25.88 i 

I 

I I 

FORM I Sv-TIC 3/90

13 EPA SAXW= NO. 

ORGANICS ANALYSIS DATA SHEET I 1 

I D07QW 

Lab Name: TXK/ABLi - Contract: NHC 

Lab Code: 'HALA Case No.: 12074 SAS No.: NA 8DG No.: n 

Matrix: (soil/eater) SOIL LL Lab Sample ID: A212074-028 

Sample wt/vol: 3 0. 8 (VUL) Ste_ 

Level: (low/med) jQK- 


Concentrated Extract Volume: 500.0 MIA) 


QPC Cleanup: (Y/N) X— pH: 8.2 


541-73-1 -------- 1,3-Dichlorobenzane 

106-46-7 -------- 1,4-Dichlorobenzeni 

95-50-1 --------- 1,2-Dichlorobenzeni 

95-48-7 --------- 2-Methylphenol 

108-60-1 -------- 2,2'-oxybin(1-Chlor 

98-95-3 

105-67-9--------2,4 

111-91-1 -------- bis 

120-83-2--------2,4 

120-82-1--------1,2 

106-4 

88-06-2---------2,4, 

95-95-4---------2,4, 

91-58-7---------2-M 

88-74-4---------2-Ni 

131-1 

208-9 

83-32-9 --------- Acenaphthene 


FORM I SV-1 






CONCENTRATION UNITS: O' 

(uq/L or uq/Rq) UG/KG Q 

n ,. 

330 III 

330 IU 

330 III 

330 III 

330 III 

330 IV 

330 III 

330 ID 

330 III 

330 III 

330 III 

330 III 

330 IV 

330 IV 

330 III 

330 III 

330 III 

330 III 

330 III 

330 III 

330 1 

330 III 

330 III 

330 III 

330 III 

810 IV 

330 III 

810 1 

330 IV 

330 IV 

810 IV 

330 III 

810 1 

Ke

UUUUl7 

lC 11PA SLIUMS M. 

BMW L&TILE ORGANICS ANALYSIS DATA SHEET 

Lab Name: =/ARLI Contract: NBC I 

I 507QDO I 

Lab Coda: MJAJA ^ Casa No.: 12 074 SAS No.: $A_ 8DG No.: jam_. 

Matrix: (soil/water) figIL Lob Sample ID: A212074-02D 

Sample wt/vol: 30.8 (9/RL) G_ 

Leval: ( low/med) UN 

t Moisture: _ .4 decanted: (Y/N) 9 




Date Received: 12 /21/92 

Data Extracted:V 12/23/92 



GPC Cleanup: (Y/N) Y pHs -3 .2 


CAS NO. COMPOUND (u9/L or uq/K9) UG,1XQ 0 

100-02-7 -------- 4-Nitrophenol 1 810 IV 

1 132-64 -9 -------- Dibenzoluran 1 330 III 

1 121-14-2 -------- 2,4-Dinitrotolueno 1 330 I U 

1 606-20-2--------2,6-Dinitrotoluena 1 330 III 

1 84-66-2 --------- Diethylphthalate I 330 IV 

1 7005-72-3 ------- 4 -Chlorophanyl-phenylether 

i 

1 86-73-7 --------- Fluorena 

330 JU IV 

1 100-01-6 -------- 4-Nitroan ne I 810 III 

i 534-52-1 -------- 4,6-Dinitro-2-methy phenol I 810 IV 

1 86-30-6 --------- N-Nitrosodiphenylamine (1)=I 330 IV 

1 101-55-3 -------- 4-Broacphenyl-phanylether i 330 IV 

1 118-74-1 -------- Hexachlorobenzene I 330 I U 

1 87-86-5 --------- Pentachlorophonol 1 810 IV 

85-01-8 --------- Phenanthrene I 330 I V 

1 120-12-7 -------- Anthracena I 330 JU 

1 86-74-8 --------- Carbazole 3i^ 30 

V 

g 

1 84-74-2 --------- D1-n-BUtyiphtha eta 

JA 

1 206-44 -0 -------- Fluoranthens 330 

i 

III 

1 129-00-0 -------- Pyrena I 330 IU 

1 85-68-7 --------- Bntylbenzylphtha ate ( 330 III 

1 91-94-1 --------- 3,3'-Dichlorobenzidina I 330 III 

1 56-55-3 --------- Benzo (a)Anthracene I 330 III 

1 117-81-7 ------ —bin (2-Ethylhexyl)Phthalata_I 330 IU 

i 218-01-9 ----- ---Chrysena I 330 IV 

1 117-84 -0 -------- Di-n-OCtyl Phthalate I 330 I V 

1 205-99-2 -------- Benzo(b)Fluoranthene i 330 I V 

207-08-9 -------- Benzo(k)Fluoranthene I 330 IV 

1 50-32-8 --------- Benzo(a)Pyrene 1 330 IV 

1 193-39-5 -------- Indeno(I t 2 0 3-cd)Pyrono I 330 IU 

53-70-3 --------- Dibenz(a,h)Anthracena 1 330 IV 

1 191-24-2 --- -----Benzo(9,h,i)Perylena I 330 III 

I i 

1.0 

FORM I SV-2 3/90

IF 



v v V V G O 


I 807QDS I 

Lab Name: TMA/ARLI Contract: NBC I I 

Lab Code: TNALA Cass No.: 12074 SAS No.: NA SDG NO.: K 


Sample wt/vol: 30.8 (q/BL) G_ Lab File ID: 30122321 

level: (low/mod) LOW_ Date Received: 12/21/92 

t Moisture: _ 4 decanted: (YIN) N Date Extracted: 12/23/92 


Injection Volume: 2.o(UL) Dilution Factor: 1.0 



Number TICS sound: (uq/L or uq/Xq) UG/KG 

I i i i 

CAS NUMBER 1 COMPOUND NAME I RT I EST. CONC. 1 4 

1. (UNKNOWN HYDROCARBON 1 5.25 I 850 IJ 

2. (UNKNOWN HYDROCARBON 1 5.85 1 1000 iw4? 

3. 1UNKNOWN ALKANE 1 5.90 1 780 iJ 

4. 1UNKNOWN HYDROCARBON 1 6.02 I 1500 

5. (UNKNOWN HYDROCARBON 1 6.57 I 100000 Pwcy 

6. ISUBSTITUTED BENZENE 1 6.73 1 140 IJ 

7. IUNXNCwx HYDROCARBON 1 7.15 1 140 14T 

S. (UNKNOWN HYDROCARBON 1 7.32 1 100 1J 

9. (UNKNOWN KETONE I 7.73 I 1800 WC-A 

10. 1UNKNOWN HYDROCARBON 

11. 1UNKNOWN HYDROCARBON 9.03 1 

1 140 W14 

12. 1PROPANOIC ACID ISOMER 1 18.35 1 200 IJ 

13. 1UNKNOWN CARBOXYLIC ACID ESTEI 21.40 I 100 JArV 

FORM I SV-TIC 3/90

1)3 

SEMIVOL&TILE ORGANICS ANALYSIS DATA S 1 It 

UUUIl.: Zj 

=PA anew No. 

1 I 

I a07QD9 


Lab Code: Tom_ Case No.t 12074 SAS No.: NA SDG No.: 

Matrix: ( soil/water) $QZL ,y ` Lab Sample IDs A212074-038 

Sample wt/vol: 30.0 (q/aL) G _ Lab File ID: 30122822 


t Moistures _^3 decanted: (Y/N) N Date Extracted: 23/92 




GPC Cleanup: (YIN) Y p8: 9.5 


CAS NO. COMPOUND (uq/L or uq/Rq) QG RG Q 

108-95-2--------Phenol I 

111-44 -4 -------- bis(2 oroethyl ) Ether I 340 

95-57-8 --------- 2-Chlorophonol I 340 

541-73-1 -------- 1,3-Dichlorobanzeno I 340 

106-46-7 -------- 1,4 -Dichlorobenzene I 340 

95-50-1 --------- 1,2-Dichlorobanzens I 340 

95-48-7 ------- --2-NothylPhenol I 340 

108-60-1 ------ --2,2' -oxybis ( 1- oropropane)_I 340 

106-44 -5 -------- 4-Methylphenol I 340 

621-64-7 -------- N-Nitroso-Di-n-Propylam ne_I 340 

67-72-1 --------- Rexachloroethane I 340 

98-95-3---------Nitrobenzene I 340 

78-59-1 ------- --Isophorone I 340 

88-75-5 ------- --2-Nitrophonol I 340 

105-67-9 -------- 2,4-Dimethylphenol I 340 

111-91-1 -------- bis(2-Ch loroathoxy ) Nathane_I 340 

120-83-2 -------- 2,4-Dichlorophanol I 340 

120-82 -1 -------- 1,2,4 -Trichlorobenzens I 340 

91-20-3---------Naphthalene ( 340 

106-47-8 ------ --4-Chlorcani e I 340 

87-68-3 ------- -Nexachlorobutad ene I 340 

59-50-7 --------- 4 -Chloro-3-Nethylphenol I 340 

91-57-6 -------- 2-Nothylnaphthalona I 340 

77-47-4---------Hexachlorocyclopentad ene I 340 

88-06-2-- ------ 2,4,6 -Trichiorophenol I 340 

95-95-4 --------- 2,4,5-Trichlorophenol ( 820 

91-58-7 --------- 2- Chl oronaphthalene I 340 

88-74-4 ------- --2-Nitroaniline I 820 

131-11-3 ------ --Dimethyiphthalate I 340 

208-96-8--------ACenaphthylens I 340 

99-09-2---------3-Nitroanilina I 820 

83-32-9---------Acenaphthene i 340 

51-28-5 --------- 2,4-Dinitrbphenol I 820 

I 

340 

yîs

iC 

SEN tATILE ORGANICS ANALYSIS DATA SHEET 

!PA SAMPL3 NO. 

Lab Name: TM1/ARL2 _ Contract: NEC 

I 

I B07QD9 

I 

1 

I 

Lab Code: Tom_ Case NO.: 12074 SAS No.: NA SDG NO.: 

Matrix: (soil/eater) SOIL .d Lab Sample I0: A212074-03B 


Level: (low/mod) jam_ 


Concentrated Extract volume: 500.0 (uL) 

injection volume: 2,O(UL) 

GPC Cleanup: (YIN) Y 


PH: 9.5 






1.0 


(uq/L or uq/Kq) UG/KG Q 2 e 

100-02-7 -------- 4-Nitrophenol I 820 IV 

132-64-9 -------- Dibonzoturan i 340 III 

121-14-2-------- 2,4-Dinitrotoluone I 340 III 

606-20-2--------2,6-Dinitrotoluone I 340 III 

64-66-2 --------- Diethylphthalate I 340 III 

7005-72-3 ------- 4-Chlorophanyl-phany atEeir I 340 IU 

86-73-7 --------- Fluorena I 340 III 

100-01-6 ------ -- 4-Nitroan ! I 820 IV 

534-52-1 ------- -4,6-Dinitro-2-as ylphano _1 820 III 

86-30-6 -------- -N-Nitrosodiphsnylamine (1)_I 340 III 

101-55-3 -------- 4-Bromophanyl-phanylether 1 340 1V 

118-74-1 -------- Nexachlorobenzene 1 340 IU 

87-86-5 --------- Pentachlorophenol I 820 III 

85-01-8 --------- Phenanthrine i 340 IV 

120-12-7 -------- Anthracene 1 340 IU 

86-74-8 --------- Carbazol! I 340 IU 

84-74-2 ----- ----Di-n-Buty ph at! "eA- 8' Im tt 

206-44-0 -------- Flucranthene I 340 IV 

129-00-0 ------ --Pyrene I 340 IV 

85-68-7 ------- --Butylbanzylph at I 340 III 

91-94-1---------3 8 3-Dichlorobinzidin! ( 340 IU 

56-55-3 --------- Benzo(a)Anthraceno I 340 IU 

117-81-7 -------- bis(2-Ethylhaxyl)Phthalate I 340 (U 

218-01-9--------C&rY5sn! I 340 IV 

117-84-0--------Di-n-Octyl Phtha at! ( 340 III 

205-99-2 -------- Benzo(b)Fluoranthone ( 340 1U 

207-08-9 -------- Benzo(k)Fluoranthene 1 340 III 

50-32-8---------Banzo(a)Pyren! I 340 III 

193-39-5 -------- Indenc(1,2,3-cd)Pyrene I 340 III 

53-70-3 ---------- Dibenz(a,h)Anthracene I 340 III 

191-24-2 -------- Benzo(q,h,i)Perylena 1 340 IV 


I-A 

!(/b"1

UUL'L';91 

1F EPA SAMPLE 1l0. 


TENTATIVELY IDENTIFIED COMPOUNDS i I 

B070" I 

Lab Nana: TNA/ARLI Contract: WRC ( I 

Lab Code: MUUA Case No.: 12074 SAS No.: NA SDG No.: 


Sample wt/vol: 30.0 (q/XQ G Lab File ID: 30122522 

Level: ( low/nod) U)W Date Received: 12/21/92 

S Moisture: _ 3 decanted: (Y/N) N 


Concentrated Extract volume: 500.0 (UL) Date Analyzed: 01/23/93 

Injection volume: 2.0(UL) Dilution Factor: 1.0 

CPC Cleanup: (YIN) 

y_ pH: 9.5 


Number TICS found: _.0 (uq/L or uq/Kq) VG/RG 

i^ NUMBER I COMPOUND NAME I RT I EST. CONC. 14 I 

I 

I 1. 

I 1-1 

1 UNRQUOWN HYDROCARBON I 5.27 I 650 

1- 1 

I 2. 1 UNINOWN HYDROCARBON I 5.85 1 960 IJ 1 

1 3. IUNINOWN HYDROCARBON I 5.90 I 790 1J i 

1 4. I UNXNOWN HYDROCARBON I 6.00 1 1200 I8dû 

I 5. 1 UNKNOWN HYDROCARBON I 6.55 1 95000 W 

I G. [SUBSTITUTED BENZENE 1 6.73 1 69 IJ u i 

I 7. 1UNXNOWN HYDROCARBON 1 7.15 1 140 

i 8. 1UNXNOWN HYDROCARBON I 7.32 I 69 IJ 

1 9. (UNSNOWN XETONE I 7.73 I 1700 IW u 1 

1 10. 1 UH7XOWN HYDROCARBON 1 9.03 1 140 1 J&-( I 

1 11. 1 PROPANOIC ACID ISOMER 1 18.35 I 170 FJ I 

12. iUMMOWN CARBOXYLIC ACID ESTE i 21 

. 40 1 69 (^d//t 

Â 


1J 

I

lE 

SEXIVOLATILE ORGANICS ANALYSIS DATA SNEET 

VVUVJ4 

!PA SAMPLZ 310. 

I I 

507QF0 

Lab Nara: THA/ARLi Contract: WHC I 

Lab Coda: TNALA Casa NO.: 7 2074 SAS No.: NA SDG No.: jam_ 

Matrix: (soil/water) SOIL _ Lab Sample ID: A212074-04B 

Sample wt/vol: 30.1 (q/mL) Q_ Lab File ID: 10125SO6 

rwvel: (low/mod) MAL Data Received: 12/21/92 

% Moisture: _2. decanted: (Y/N) N Data Extracted: 12/23/92 






CAS NO. COMPOUND (uq/L or uq/Xq) UG/XG 

111-44 -4 -------- his( 

95-57-8---------2-Ch 

541-73-1--------1,3- 

106-46-7--------1,4- 

95-50-1---------1,2- 

95-48-7---------2-Me 

108-60-1--------2,2' 

106-44-5--------4-Me 

621-64-7--------N-Ni 


105-67-9--------2,4 

111-91-1 -------- his 

120-82-1--------1,2 

106-4 

91-57-6---------2-Me 

77-47-4 --------- Nexa 

88-06-2---------2,4, 

95-95-4---------2,4, 

131 

51-28-5---------2, 

340 1 

340 

340 J U 

340 J U 

340 JU 

340 J U 

340 IV 

340 JU 

340 J U 

340 III 

340 JU 

340 IV 

340 IV 

340 J U 

340 J U 

340 IV 

340 (U 

340 JU 

340 JU 

340 IV 

340 JU 

340 J U 

340 JU 

340 J U 

340 JU 

810 JU 

340 IV 

810 IV 

340 JU 

340 (U 

810 (U 

340 IV 

810 IV 

f ^J^

vvvvJJ 

lCEPA SMOLE no. 


Lab Names TxniARLi Contract: NHC 

E07QFO j 

Lab Code: Tom_ Case No.: 12074 SAS NO.: NA SDG No.: N_ 

Natrixs (soil/eater) SoiL d ,s Lab Sample ID: A212074-049 

Sample et/vol: 30.1 (q/mL) Q_ Lab File ID: 30125806 

Level: (low/wed) Date Received: 12/21/92 

t Moisture: _ 2 decanted: (Y/N) 2i_ 




GPC Cleanup: (YIN) X— pH: 9.5 


CAS NO. COMPOUND (uq/L or uq/Xq) UG/XQ 



7005-72-3 ------- 4-Chlorophenyl-phenylether 

86-73-7 --------- Fluorene 

100-01-6 -------- 4-Nitroan 1 e 

534-52-1 -------- 4,6-Dinitro-2-me y pheno 

86-30-6---------N-Nitrosodiphenylamine (1)_ 

101-55-3 -------- 4-Bromophanyl-phanylether 


87-86-5-- ------ Pentachlorophenol 

85-01-8 --- -- ---- Phenanthrene 

120-12-7 -------- Anthracene 

86-74-8---- ----- Carbazole 

91-94-1---------3,39-Dichlorobenzidine 


117-81-7--------bis(2-Ethylhexyl)Phthalate 

117-84-0 -------- Di-n-Octyl P 

205-99-2--- ----- Benzo(b)Fluc 

207-08-9--- ----- Benzo(k)Flua 

50-32-8---------Benzo(a)Pyre 

193-39-5--------Indeno(1,2,3 

53-70-3 ---------Dibenz(a,h)A 

191-24-2 -------- Benzo(q,h,i) 

810 

340 

340 

340 

50 

340 

340 

810 

810 

340 

340 

340 

810 

340 

340 

340 

JU 

JU 

IV 

JU 

IJ 

JU 

JU 

IV 

IV 

IU 

IV 

IV 

IU 

JU 

IV 

IV 

0340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

340 

Iu 

IV 

JU 

JU 

JU 

JU 

JU 

IV 

JU 

IV 

IV 

JU 

(U 

JU 


I


IF 



Lab Code: ZMLA Case No.: 12074 


Sample wt/vol: 30.1 (q/mL) Q_ 

Level: (low/mod) jam_ 

i Moisture: _ 2 decanted: (YIN) N 





000034 

EPA SAMPLE N0. 

E07QFO I 


SAS No.: NA SDG No.: 





Date Analyzed: 9J /25 ;. 



(uq/L or uq/Rq) UG/KG 

CAS NUMBER i COMPOUND NAME i RT i EST. CONC. i Q 

I 1. (UNKNOWN HYDROCARBON I 5.43 I 300 J,wv I 

I 2. ( UNKNOWN HYDROCARBON I 5.88 I 1700 IJ 

I 3. I UNKNOWN HYDROCARBON I 6.00 I 1500 (, I 

)($^(/ 1 

U I 

I 4. (UNKNOWN HYDROCARBON I 6.55 I 95000 

I 5. (UNKNOWN HYDROCARBON I 7.15 i 140 

(UNKNOWN KETONE I 7.73 1 1900 1 (^ 1 

I 7. 

1UNKNOWN HYDROCARBON i 9.03 1 3 00 I IA 

I 8 . 

1UNKNOWN CARBOXYLIC ACID ESTEI 21.40 1 100 i N 

FORM I SV-TIC 3/90

iD 

PESTICIDE ORGANICS ANALYSIS DATA SHENT 

"Axo. ooh 

ab Name: TMA/ARLI Contract: 1fHC 

I 

I 307QW 

I 

I 

I 

I 

ib Code: TMAIA_ Case No.s 12074 SAS No.: NA SDG No.: KL_ 

atrix: (soil/water) SOIL Lab sample ID: A2 12074-058 

ample wt/vol: 30.0 (q/mL) G 

Moisture: 9 decanted: (Y/N) N 

xtraction: (SepF/font/Sonc) SONC 

oncentrated Extract Volume: 5000 

njection volume: 1.00 (UL) 

PC Cleanup: ( YIN) Y PH: 8.9 

CAS NO. 

319-84- 

319-86-8--------del 

76-4 

1024 

72-55-9---------4,4' 

33213-65-9 ------ Endosulfan II 

72-54-8 -------- 4#4'-DDD 


50-29-3---------4,4'-DDT 

72-43-5 ------- --Methoxy or 

53494-70-5 ------ Endrin ketone 


5103-7 

I 

Lab File ID: 

Date Received: 12/21/9 2 


Z) Date Analyzed: 01/07/93 



.ONCENTRATION UNITS: 

(uq/L or uq/Rq) UG/RG Q F 

1.9ÎI^ 

1.91LT^ 

1.9ÎI 

1.91 u I 

1.91 u I 

1.91 u I 

3.61U I 

3.61U I 

3.61U I 

3.61U 1 

3.61U 1 

3.61U I 

3.61U I 

19 III I 

3:61U I 

3:61U I 

1.91II I 

1.91II I 

190 III 1 

36 III 1 

74 III 1 

36 III 1 

36 III 1 

36 JU 1 

36 III 1 

36 III I 


`/ 

I 7^^SIG

319-84 

iD 


Alb Names 3 MALT Contract: NHC 

72-55-9 --------- 4t4'-DDE, 

72-20-8 --------- Endrin 

33213-65-9 ------ Endosulf, 

72-54-8 --------- 4,41-DDD 

1031-07-8 ------- Endosulf 

50-29-3---------4,41-DDT 

72-43-5 --------- Methoxyd 

53494-70-5 ------ Endrin k 

7421-36-3 ------- Endrin a 

5103-74-2 ------- ganna-Chlordane 

8001-35-2 ------- TOxaphene 

12674-11-2 ------ Aroclor-1016 

UUUUJO 

=PA sAac ii No. 

I 1 

I 507Q86 I 

.ab Code: TMATA_ Case No.: 12074 SAS No.: NA SDG No.s jam_ 

tatrix: (soil/voter) $OIL Lab Sample ID: A212074-068 

;ample wt/vol: 30.1 (q/uL) G Lab File ID: 

c Moisture: . 3 decanted: (Y/N) N Date Receivads 12/21/92 

:xtraction: (Sopr/font/Sonc) SONC Date 8xtzacted 2 12/24/92 

:oncentrated Extract Volume: 5000 (up Data Analyzeds IZ 108193 


;PC Cleanup: (YIN ) Y _ PH: 8.7 Sulfur Cleanup: (YIN) N 


CAS NO. COMPOUND (uq/L or ug/Xq) UG/XG 

1.71UJ"^ 

^.71U I ^^^S17 

1.71U 1 

1.71U 1 

1.71U I 

1.71U I 

3.41U 1 

3.41V 1 

3.41U I 

3.41U I 

3.41U 1 

3.4IU I 

3:41U 1 

17 III I 

3.41U I 

3.41U I 

1.71U 1 

1.71U 1 

170 IU 1 

34 IU 1 

69 III 1 

34 IU 1 

34 IV 1 

34 III 1 

34 IU 1 

34 IU I 

FORM I.PEST 3/90

ID 


1.81Ur 

1.81U 

1.81U 

1.81U 

1.81U 

1.81Q 

1.81V 

1.81U 

3.51U 

3.51U 

3.51U 

3.51U 

3.51V 

3.51U 

3.51U 

18 IV 

3-51U, 

3.51U 

1.81U 

1.81U 

180 III 

35 IU 

72 IU 

35 IU 

35 IV 

35 IV 

35 IU 

35 IUI 

UUU0j'i 

E'PA SAN= No. 

I I 

I E07QW 

aib Name: THA/ARLT Contract: N7iC I I 

.ab Code: TMALA Cass No.: 12074 SAS No.: NA SDG No.: MR 

Atrix: ( soil/water) 30IL 

ample wt/vol: 29.7 (VAL) G_ Lab File ID: 

Lab Sample ID: 71212074-010_ 

Noisture: 6 decanted: (Y/N) 1'i_Date Received: 12/21/92 

;xtraction: (SepF/font/sonc) SONC Data Extracted: 12/24/92 

!oncentrated Extract Volume: 5000 (UL) Date Analyzed: 01/06/91 

njection Volume: 1.00 (uQ Dilution Factor: 1.00 

.PC Cleanup: MR) y_ pH: 9.3 Sulfur Cleanup: ( Y/N) 

1 


CAS NO. COMPOUND (u4/L or u4/E4) UG/XGS MOF10 77 

1 319-84-6 

1 319-85-7 

1 319-86-8 

58-89-9- 

( 76-44-8- 

1 309-00-2 

959-98-8 -------- EndosulZ 

60-57-1 --------- Dieldrin 

72-55-9 --------- 4,4'-DUE. 

72-20-8 --------- Endrin 

33213-65-9 ------ Endosulf 

72-54-8 --------- 4,4'-DDD 

1031-07-8 ------- Endosulf, 

50-29-3---------4,4'-DDT 

7421-36-3 

5103-71-9 

11141 

1109 

^^ 2 a 

FORK I PEST 3/90 

I 

I 

I 

I 

I 

I 

I 

I 

I 

1 

1 

i 

I 

I 

I 

I 

1 

I

1D 


Ab Maine: TKA/ARLI __-_ _ Co 

Ab Code: THALA_ Case No.: 12074 SAS 

(atrix: (soil/water) SOIL > •> 

asple wt/vol: 30.6 (q/mL) Q_ 

c Moisture: 4 decanted: (YIN) 

:xtraction: (SepF/Coat/Sonc) SONC_ 

:oncentrated Extract Volume: 5000 

njection Volume: 1,,00 (uL) 

:PC Cleanup: (YIN) Y pH: 8.2 


319 

319 

319 

76-44 

72-55-9---------404' 

33213-65-9 ------ Endosulfan II 

72 -54-8 --------- 4,4'-DDD 


50-29-3---------4,40-DDT 

53494-70-5 ------ Endrin 

7421-36-3 ------- Endrin 

5103 -71-9 ------- alpha- 

5103-74-2 ------- gamma- 

8001-35-2 ------- TOxaph 

53 

11096-82-5 ------ Aroclor-1260 

IL 

000038 

EPA SAW= NO. 

I I 

807QN i 

retract: NHC I I 

No .: NA SDO No.: N 

Lab Sample IDs A212074-028 

Lab Pilo ID: 

Date Received: 12/21/9? 


uL) Date Analyzed: 01/07/93 


Sulfur Cleanup: (Y/N) 


(uq/L or uq/Kq) gG/RG Q 

1 1.71UJ I 

1 :71U 1 

i) 1 1.71U 1 ^^ 

1. I 

1.71U 

1.71U 

1.71U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

3.41U 

17 1U 

3.41U 

3.41U 

1.71U 

1.71U 

170 IU 

34 1U 

68 1U 

34 IU 

34 IU 

34 1U 

34 1U 

34 1 


r!i

Ab Name: TMA/A RLI 

319-84 

319-85 

319-86 

76-44-8-- 

309-00-2- 

1024-57-3 

959-98-8- 

72-55-9---------4,41 

72-20-8 -------- Endz 

33213-65-9 ------ Endc 

72-54-8---------4#40 

50-29-3 --------- 4*40 

1D 

53494-70-5------Endrin ketone 

7421-36-3-------Endrin aldehyde 

11141-16-5 ------ Aroclor-1232 

000039 

SPA SANP= NO. 

PESTICIDE ORGANICS ANALYSIS DATA amMT 

Contracts 1030 

I 

3O7QD9 

i 

1 

) 

.ab Code: THALA_ Case No.: 12074 

latrix: ( soil/water) SOIL 

;ample wt/vol: 30.3 (g/mL) Q_ 

r Noisture: 3 decanted: (Y/N) N 

:xtraction: (SepF/cont/sonc) 3ONC 

:oncentrated Extract Volume: 5000 

:njection Volume: 1.00 (uL) 

;PC Cleanup: (Y/N) Y_ PH: 9.5 

Cgq:t l •a KO)IC0610i•^ 

SAS No.: NA SDG No.s NA 

Lab Sample IDs A212074-O3B 

Lab File ID: 


Date Extracted: 12f24/92 

3L) Date Analyzed: 0,/07/93 


Sulfur Cleanup: (Y/N) 

ONCENTRATION UNITS: 

(ug/L or ug/Kg) UG RG 

1.71UT I p 

1.71U 10 

1.71US 

1.71U 

1.71U 1 

1.71U 1 

1.71U 1 

1.71U 1 

3.41U 1 

3.41U 1 

3.41U 1 

3.41U 1 

3.41U 1 

3.41U 1 

3.41U 1 

17 1II 1 

3.41V 1 

3.41U 1 

1.71U 1 

1.71U 1 

170 1U 1 

34 1 U 1 

68 1U 1 

34 1U 1 

34 1U 1 

34 1U 1 

34 1U 1 

34 1U 1 

FORK I PEST 3/90 

1 

I

58-89-9 

1D 


959-98-8 -------- Endosulfan I- 

60-57-1 --------- Dieldrin 

72-55-9 --------- 4 , 4'-DDE 

72-20-8 --------- Endrin 

33213-65-9 ------ Endosulfan II 

72-54-8 --------- 4,4'-DDO 


50-29-3---------4,4'-DDT 

72-43-5 --------- Methoxy or 

53494-70-5 ------ Endrin ketone 




8001-35-2 ------- TOxaphene 

12674-11-2 ------ Aroclor-1016 

11104-28-2 ------ Aroclor-1221 

11141-16-5 ------ Aroclor-1232 

53469-21-9 ------ Aroclor-1242 

1,1096-82 

000040 

EPA aaMFLE 110. 

I 1 

1 807QF0 

.ab Names TMA/ARLI Contract: NHC ( I 

.ab Code: THALA_ Case No.: 12074 SAS No.: NA SDG No.: NA 

Atrix: ( soil/water) SOIL -Z- Lab Sample ID: x212074-048 

ample art/vol: 30.4 (9/ML) G 

Moisture: _2 _ decanted: (Y/N) N 

xtraction: (SepF/COnt/SOnc) SONC 

concentrated Extract Volume: 5000 (UL) 

ejection Volume: x,,00 (uL) 

PC Cleanup: (YIN) Y pH: 9.5 

Lab File ID: 


Date Extracted: ~x,2/24/92 



Sulfur Cleanup: (YIN) RA 


CAS NO. COMPOUND (ug/L or ug/Rg) UG/KG 

1.71U 

1.71 Ur 

1.71U I 

1.71U I 

1.71U I 

1.71U 1 

3.31U I 

3.31U I 

3.31U I 

3.31U I 

3.31U I 

3.31U I 

3.31U 1 

17 III 1 

3.31U I 

3.31U I 

1.71U I 

1.71U 1 

170 III 1 

33 IU 1 

67 1 V 1 

33 1U 1 

33 1U 1 

33 1U 1 

33 1U 1 

33 IU 

—1-1 I 

I ((^^^ 


I 

P


1 




8070e5 

Lab Code: SKINER Case No.: N2-L2-113SAS No.: SOG NO.: 807085 


Lab Samp le ID: 12327-OSS 



Concentration Units (ug /L or mq/K. g dry wei ght): MG/KG ,y G 

;CAS No. ; Anal y te ;Concentration:C: O :M 

:7429-90-5 :Aluminum 8200 .P 

:74&0-36-0 !Antimon y ; 3.7 ; U: ( US' : F 

:7440-38-2 :Arsenic 2.9 S, :F 

:7440-39-3 :Barium 72.7 : :P 

:7440-41-7 :Ber y llium: 0.35:8: :P 

:7440-43-9 ;Cadmium 0.' 2 :!J: :F 

;7440-70-2 :Calcium 5500 ; :P : { 

:7440-47-3 :Chromium 10.1 S• ;P 

:7440-48-4 ;Cobalt 10.3 :P ! 

7440- 50-8 :Copper 17.5 U, :P 

:7439-89-6 :Iron : 20000 :P ' 

:7439-92-1 :Lead 3.1 F F 

:7439-95-4 ;Ma gnesium: 4.:90 :P 

;7439-96-5 :Man ganese: .26 ;P 

7439-97-6 :Mercur yO.OS:U: :CV: 

:7 4140-02-0 :Nickel : i0.. : : :P 

:7440-09-7 :Potassium: 1320 t : :P 

:7782-49-2 :Selenium : 0.64:U: OV UT':F 

:7440-22-4 :Silver : 1.2 :X: (A . :P 

:7440-23-5 :Sodium : 212 :B: :P : 

:7440-28-0 :Thallium 0.54:U: X(jT.:F 

:7440-62-2 :Vanadium : 4 5,9 

:7440-66-6 :Zinc : &Z. 7 

:C yanide ; - 0.52:U: :CA: 

Color Before: BROWN Clarity Before: Texture:. 'MEDIUM 

Color After: BROWN Clarity After: Artifacts: YE 

_ vmm^ll t 5 

STONE'-- 

FORM 1 - 1N 

^j 

tumelz•_.1


1 



Lab Code: SKINER Case No.: N2--12-113 5AS No.: 


Level (low/med): LOW 

V Solids: 95.4 


B07086 

Lab Samp le I0: 12327-06S 

Date Received: 12/2 2 

Concentration Units (uc/L or m g /Kg dry wei ght): MG/KG 

;CAS No. : Ansl y te :Concentration:C: 0 :M 

:7429-90-5 :Aluminum : 9010 : :P 

7 4.&0-36-0 :Antimon y3.7 :U: ,^LAZY- • : P : 

:7440-38-2 :Arsenic 2.`' :F 

:7440-39-3 ;Barium :6 .5 :P_ 

:7440-41-7 :B^r y 111um: 0.34:6: :P 

:7440-43- Q : Cadmium 0. _% 2: i! : : P } 

7440-70-2 :Calcium : 5130 

♦ 

:^° 

• 7440-47-3 :Chromium : 13.7 

:7440-4S-4 :Cobalt 10.4 

:7440-50-8 :Co pper 19.9 :P 

:7439-89-6 :Iron : 19500 :P 1 

:7439-92-1 :Lead : 5.9 

:7439-95-4 :Magnesium: 4390 

:7439-96-5 :Man ganese: 290 :P 

:7439-97-6 :Mercur y0.05:U: :CV; 

:7440-02-0 !Nickel 11.9 :P 

:7440-09-7 :Potassium: 1110 : 1 :P 

:7782- G 9-2 :Selenium : 0.60 U: Ur: F 

:7440-22 -4 :Silver : 1.3 :je:LA : :P : 

:7440-23-5 :Sodium : 254 ;8: :P : 

:7440-2E-0 Thallium : 0.50:U: :F : 

:7440-62-2 :Vanadium : 43.2 : :P 

:7440-66-6 :Zinc : 81.5 ; :S- :P 

:C yanide : 0.49:U: :CA: 

Color Before: BROWN Clarity Before: Texture: FINE 

Color After: BROWN Clarity After: Artifacts: YES 

Camm-- nts: 

STONES 

FORM I - IN 

SOG No.: B070B5 

, 

ILMO2.1

5/27/93 HEIS Data Changes for 100-NR-1 BOREHOLE SAMPLES Page 19 

Data Validation Report YHC-SD-EN-TI-156, Rev. 0 

SN FT 

---------- -- ---- 

FN LC Cl N VR C Q CE US 

--- ------ ---------- --- --------- -- -- ------- ---------- ----- 

B07Q86 

807OD7 

807QD7 

807QD7 

B07QD7 

B07QD7 

807OD7 

807QD7 

B07QD7 

607007 

B07QD7 

B07QD7 

B07QD7 

807QD7 

B07QD7 

B07QD7 

807QD7 

B07QD7 

B07QD7 

807QD7 

B07QD7 

B07QD7 

B07QD7 

807QD7 

B07QD7 

B07QD7 

807QD7 

B07QD7 

B07QD7 

807008 

B07QDB 

B07QD8 

807OD8 

B07QD8 

WON 

807OD8 

807QDB 

607QD8 

B07QDB 

B07QDB 

807QDB 

607008 

B07QD8 

WON 

WON 

B070D8 

B07QD8 

B07QDB 

B07QD8 

B07QD8 

B07QD8 

B07QD8 

BO7QD8 

807QD8 

B07QD8 

B07QD8 

B07Q08 

B07QD9 

B07QD9 

6070FO 

B07QF0 

B07Q85 

807QB5 

B07QB5 

B07OB5 

B07QB5 

B07Q85 

B07QB5 

607066 

807066 

B07QB6 

B07QB6 

8070B6 

807QD7 

CLP, 1D TMALA 319-86-8 GS 

CLP 1D TMALA 319-84-6 GS 


CLP 10 TMALA 319-86-8 GS 




CLP 1D THALA 1024-57-3 GS 



CLP 10 THALA 72-55-9 GS 


CLP 10 TMALA 33213-65-9 GS 


CLP 1D TMALA 1031-07.8 GS 






CLP 10 TMALA 5103-74-2 GS 



CLP 10 TMALA 11104-28-2 GS 




CLP ID TMALA 11097-69-1 GS 

CLP ID THALA 11096-82-5 GS 







CLP 10 THALA 1024-57-3 GS 





CLP 10 TMALA 33213-65-9 GS 






CLP 10 TMALA 7421-36-3 GS 


CLP 10 THALA 5103-74-2 GS 

CLP 10 TMALA 8001-35-2 GS 



CLP 10 TMALA 11141-16-5 GS 




CLP 10 TMALA 11096-82-5 GS 





CLP I SKINER 7440-36-0 GS 









CLP T SKINER 7782-49-2 GS 




UT 

JIJ 

UJ` 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

U4 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

UJ 

J 

U 

UJ 

U 

UJ 

J 

UJ 

J 

UJ 

U 

J 

UJ


1 




807007 

Lab Code: SKINER Case No.: N2-12-1135AS No.: SOG No.: 807085 


Lab Sample'rO: 12327-01S 



Concentration Units (u g /L or mg /Kg dry weight): MG/KG 

:CAS No. ; Analvte :Concentration:C: 0 :M 

17429-90-5 :Aluminum : 5470 :P 

17440-36-0 !Antimon y1 3.6 U: : UT • : P 

/ 

17440-38-2 ;Arsenic 

-.0 :F' 

:7440-39-3 :Barium 44.0 :P 

:7440-41-7 :Ber y llium: 0.21:8: :P 

:7440-43-9 ;Cadmium : 0.31:U: :? . 

:7440-70-2 :Calcium 10700 : :? 

:7440-47-.3 :Chromium •+.'_ , 

:7440-48-4 :Cobalt 8.8 :8: 

:7440-50-8 :Copper : 26.0 :P 

:7439-89-6 :Iron 16900 

?439-92-1 :Lead °_.- ;F 

:7439-95-4 :Magnesium: 3980 : :F 

.7439-96-5 :Manganese: '257 :? . 

:7439-97-6 :Mercury 0.05:U: :CV: 

:7440-02-0 :Nickel :, 9.6 :P . 

:7440-09-7 :Potassium: 769 :B: :P 

:7782-49-2 :Selenium : 0. 60 : U : )6pUS : F 

17440-22-4 :Silver 1.1 :ie:u :P 

17440-23-5 :Sodium : 201 ;8:• :P 

:7440-28-0 :Thallium : 0.50:U: :F 

:7440-62-2 :Vanadium : 36.3 : : :P 

17440-66-6 :2inc : 37.0 ; : YT :P 

:Cyanide : 0.52:U: :CA: 

Color Before: BROWN Clarity Before: Texture: MEDI':"` 

Color After: BROWN Clarit y After: Artifacts: YET 

Comments: 

STONE`. 

FORM 1 - IN 

1 

f7 

4 

LL!1rJ= .


1 



6070D8 

Lab Name: SKINNER & SHERMAN LABS. Contract: 68-00-0108 ; 

Lab Code: SKINER Case No.: N2-12-1135AS No.: SDG No.: 607055 




Concentration Units (ug/L or me/K9 dr y wei ght): MG/KG 

;CAS No. Analyte :Concentration:C: O :M 

:7429-90-5 :Aluminum : 4220 1P 

17440-36-0 :Antimon y 3.5 :U: 1^ u,T'.;P 

:7440-38- 2 :Arsenic : 1.5 :6: to f"' • :F- 

:7440-39-3 .carium 84. 1^1 :P 

:7440-41- 7 :Ber y llium: 0.20:6: :P . 

.?440-43- •? :Cadmium 3..?1:U: :P 

;7440-70--2 :Caloium :5610 :P 

:7440-47-3 :Chromium : 6.5 ^^•:F . 

:7440-48-4 :Cobalt 10.3 :P . 

:7440-50-8 ;Copper '20.5 :f 

:7439-89-6 :Iron 18200 1P . 

:7439-92- 1 : L ead _.. :F 

:7439-95-4 ;Magnesium: 37 50 :P 

:7439-96-5 ;Man •:;anese: 2 37 :P . 

:7439-97-6 :Mercur y: 0.05:U: :CV: 

:7440-02-0 :Nickel °.L ; 1P . 

17440-09-7 :Potassium: 749 :B: :P 

:7732-49-2 :Selenium : 0.63:U: )f 4AT. ;F 

:7440-22-4 :Silver 1 1.1 : Jt :U- :P 

:7440-23-5 :Sodium 355 :B1 .P 1 

:7440-28-0 :Thallium : 0.53:U: :F 

;7440-62-2 :Vanadium : 43.5 : :P 

:7440-66-6 1Zinc : 36.0 ; : j.!f :F 

:Cy anide : 0.51:U1 :CA: 

Mozm 

Color B.-for GREY Clarity Before: T

WESTINGHOUSEMANFORO 

1 


Lab Name: SKINNER & SHERMAN LABS. 6 Contract: 68-DO-0108 


6070D9 

Lab Code: SKINER Case No.: N2-12-113SAS No.: 3OG No.: 807055 

Matrix (soil/water): SOIL Lab Samp le ID: 12327-03S 

Level (low/med): LOW Date Received: 12/2 


Concentration Units (ug /L or m q /K9 dry wei ght): MG/KG 

;CAS No. ; Anal y te :Concentration:C: 0 :M 

; _; 

^1 

1 

: _; 

:7429-90-5 ;Aluminum : 3430 :P 

:7440-36-0 :Antimony 3.7 :U: K UT :P 

:7440-3S-2 :Arsenic 1.0 16: j! f -:F 

:7440-39-3 :Barium 65.Z : :P 

17440-41-7 :Bery llium: 0.23:6: 'P 

;7440-43- z :Cadmium 0.Z^-:U: ;P 

:7440-70-2 ;Calcium 5560 

:7440-47- 5 :Chromium :.4 

:7440-4S -4 ;Cobalt 11.° 

:7440-50-8 :Cop per 20.6 : :P ;- 

:7439-89-6 :Iron 22300 

:7439-92-1 :Lead : 2.3 : :F 

:7439-95-4 :Magnesium: 4030 1 :P : + 

;7439-96-S :Manganese: 234 t 

:7439-97-6 :Mercur y 0.05:U: :CV: j 

:7440-02-0 :Nickel ; 3.0 :B: :F j 

:7440-09-7 :Potassium: 562 :B: :P i 

:7782-49-2 :Selenium : 0.63:U: IVVUT:F 

:7440-22-4 :Silver : 1.3 1 : u - :P 

:7440-23-5 :Sodium : 292 ;8: :P 

:7440-2S-0 :Thallium : 0.53:U: :F 

:7440-62-:, :Vanadium : 46.0 : : ^/ :P : 

:7440-66-6 :Zinc 

37.1 : : f ^ :P 

.: :Cyanide : 

0.51:U: ;CA: ) 

C6? 

Color Before: GREY Clarity Before: T•rxtuin: ,MEDIUM 

Color After: GREY Clarity After: Artifacts: YES 

Comm+ n t s : 

:TONES 

FORM : - IN 

^'._M0'?. 1


1 



B070FO 

Lab Name: SKINNER & SHERMAN LABS. Contract: 68-00-0108 -- 

Lab Code: SKINER Case No.: N2-12-113SAS No.: SDG No.: 507065 


Lab Samp le ID: 12327-04S 

Level (low/med): LOW Date Received: 12/22 

X Solids: 96.7 

Concentration Units (u g /L or mg/Kg dr y weight): MC-/KG 

;CAS No. Analyte :Concentration:C: O ;M 

:7429-90-5 :Aluminum 3050 

:7440-36-0 :Antimon y3.7 :U: KUJ- ; P 

:7440-38-2 :Arsenic 0.76 :B: y T .F 

:7440-39-3 ;Barium 49.4 , : :P 

:7440-41-7 :Ber y llium: 0.21:6: :P 

;7440-43•-'? :Cadmium : 0.3'2:!I: ;P 

:7440-70-2 :Calcium 5510 :P-: 

:7440-47-3 :Chromium 3.9 F : t 

:7440-43-4 :Cobalt 11.9 :P i 

:7440-50-a ;Copper 16.5 :U :P 

:7439-89-6 :Iron : 21700 :P ' 

:7439-92-1 :Lead : 1.8 

:7439-95-4 Magnesium: 3890 : : :P 

:7439-96-5 :Man ganese: 254 : : :P : # 

:7439-97-6 :Mercur y0.05:L!: :CV: 

:7440-02-0 :Nickel 6.8 :B: 

:7440-09-7 :Potassium: 420 :B: :P 

:7782-49-2 :Selenium : 0.58:U: /0113-'F 

:7440-22-4 :Silver : 1.9 :Y:u :P 

:7440-23-5 :Sodium 319 :B: :P 

:7440-2S-0 ;Thallium : 

0.49:U: XUJ-.:F 

:7440-62-2 :Vanadium 46.7 :P 

:7440-66-6 :Zinc : 36.7 : : jrj-. : P 

:C yanide : 0.49:U: :CA: 

I 

Color Before: GREY Clarity Before: Texture: MEDIUM 

Color After: GREY Clarit y After: Artifacts: YES 

Comments: 

STONES 

FORM I - IN 

v itif 

iLMO=.. 

M

Rocolvodt 12/22/92 

000014 

TINA Inc. RE"RT 

Resuitts by Sospls 

York Ordsr 0 A2-12-074 

SAMPLE 10 297083 FRACTION UL TEST CODE YCCL/S MANE Anions In Solids - Y1232 

Dot* A Time Cottoetod 12117112 Catapory 

ANIONS AND YET CHEMISTRY • SOLIDS 

ANALYSIS METHOD RESULT UNITS Limit 

Ftuoride 300.0 2.4j) s3/Kp 0.2 

pN 9045 8.9,E pM 0.1 

Sulfate 300.0 9 (t) sp/Ke 2.0 

FORM 1


000015 

INA Inc. REPORT York Order IF A2-12-874 

Results by Suple 

SAMPLE ID $07086 FRACTION 01 TEST CODE VCCLPS NAME Aniono in Solids - VN232 

Date i Ttne Collected 12117192 _ 

Category 

C 


ANALYSIS METHOD RESULT UNITS. L. MI_ 


PH 9045 8. pM 0.1 

Sulfate 300.0 33 mg/Kg 2.0 

FORK I

2eoeiV*dt 12122192 

000010 

IRA Inc. REPORT 

Rewlts by Saspt* 

Work Or"r 0 A2-12-074 

SAMPLE 10 207007 FRACTION M TEST CODE VCCLPS MANE Anions in Soilds - YN232 

Date S Tise Cot Lected 12(16192 Catolory 

{ 

ANIONS AND MET CHEMISTRY - SOLIDS 


Fluoride 300.0 1.0 sD/KO 0.2 

pN 9045 9. pH 0.1 

Sutfate 300.0 10 , n R/KS 2.0 

FORM 1

m 


ANALYSIS METN00 RESULT UNITS LIMIT 

Fluorlde 300.0 1.30, MS/KS 0.2 

pN 9045 

pN 0.1 

9.20) 

Sulfate 300.0 _!!!g •S/KS 200 

000011 

TWA Inc. REPORT York Order f A2-12-974 

Recefveds 12/22192 Results by Sample 

SAMPLE IO 907006 FRACTION UL TEST CODE WCCLPS NAME Anfons In solfds - W2232 

Dote t Tfse Collected 12/16/92 Category 

FORM I


SAMPLE 10 11070D9 _ 


ANALYSIS METH00 RESULT UNITS LIMIT 

Fluoride 300.0 0.009/90 0.2 

pM 9045 9.SA pM 0.1 

Sulfate 300.0

000013 

TMA Inc. REPORT Vert Order 1 A2-12-074 

Reeetvedt 12122/92 Reaults by UNPIN 

SAMPLE LD 507DF0 FRACTION L% TEST CODE YCCLPS NAME Anions in Setids - VR232 

Date 4 Its* Cottetted 12117192 Category 

mao, 

IZ!lff!R 



FLuorlde 300.0 0. amWKS 0.2 

PH 9045 9.5(4 pN 0.1 

Sulfate 300.0 40 J) MR /K g 2.0 

FORM I 

0

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