10.06.2013 Views

Tellurite And Fluorotellurite Glasses For Active And Passive

Tellurite And Fluorotellurite Glasses For Active And Passive

Tellurite And Fluorotellurite Glasses For Active And Passive

SHOW MORE
SHOW LESS

You also want an ePaper? Increase the reach of your titles

YUMPU automatically turns print PDFs into web optimized ePapers that Google loves.

8. Fibre drawing; MDO 351<br />

Table (8.5): EDX analysis of fibre drawing samples of composition MOF005 (70TeO2-<br />

10Na2O-20ZnF2 mol. %).<br />

EDX<br />

spectra<br />

Atomic %<br />

5<br />

Comments<br />

O F Na Te Zn<br />

MOF005ii: fibre mounted in epoxy length ways and cross-sectioned:<br />

A Bulk glass ≈ 10 µm from fibre edge 44.02 10.26 4.74 27.81 13.17<br />

B Triangular crystal ≈ 1 µm from fibre surface 30.03 22.01 20.37 18.63 8.96<br />

C Triangular crystal 34.39 10.88 16.20 25.48 13.05<br />

D Edge of snowflake crystal 34.70 12.55 11.54 27.58 13.63<br />

E Cross crystal ≈ 1 µm from fibre surface 26.21 22.92 24.78 17.17 8.91<br />

F Cross crystal 20.89 28.12 26.47 16.81 7.72<br />

G Centre of snowflake crystal 26.00 20.46 23.48 20.15 9.92<br />

H 6 Light particle on surface at centre of fibre 45.56 9.64 3.55 26.91 13.07<br />

MOF005ii: fibre surface mounted on a carbon tab:<br />

I Light crystal protruding from fibre surface 38.15 13.36 13.25 24.33 10.91<br />

J Dark bulk glass on fibre surface 39.02 9.62 10.54 27.58 13.24<br />

K Light crystal protruding from fibre surface 36.39 11.02 10.98 28.53 13.08<br />

L Light crystal protruding from fibre surface 28.95 18.10 24.18 19.34 9.44<br />

M Light crystal protruding from fibre surface 35.48 11.29 13.61 27.08 12.54<br />

MOF005ii: fibre mounted end on in epoxy, and polished back:<br />

N Bulk glass at centre of fibre 43.31 11.39 6.03 26.30 12.98<br />

O Centre of snowflake crystal 25.99 21.26 23.63 19.48 9.64<br />

P Edge of triangular crystal 28.66 19.52 22.77 19.44 9.61<br />

Q Centre of snowflake crystal 24.08 21.93 22.96 20.75 10.28<br />

R Bulk glass at centre of fibre 43.22 9.77 9.65 25.33 12.02<br />

MOF005iii: neck down piece of glass mounted in epoxy and cross-sectioned<br />

S Bulk glass 43.06 14.63 2.25 27.27 12.79<br />

T Cross crystal 36.10 17.26 7.81 26.77 12.06<br />

U Bulk glass at centre of fibre 41.96 17.45 4.91 24.17 11.51<br />

V Cross crystal 35.84 15.11 7.57 28.24 13.24<br />

W Bulk glass 42.46 16.54 3.44 25.50 12.06<br />

X Bulk glass 42.22 15.86 3.40 25.87 12.65<br />

Y Cross crystal 31.79 18.00 12.10 25.53 12.57<br />

5 Batched glass: 47.62 at. % O, 15.87 at. % F, 6.35 at. % Na, 22.22 at. % Te, and 7.94 at. % Zn.<br />

6 1.28 at. % Si

Hooray! Your file is uploaded and ready to be published.

Saved successfully!

Ooh no, something went wrong!