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Tellurite And Fluorotellurite Glasses For Active And Passive

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5. Crystallisation studies; MDO 141<br />

Fig (5.4) shows an XRD trace of the 99.9995% ZnO powder sourced from Alfa Aesar.<br />

Table (5.2) shows the ten most intense peaks with corresponding 2θ (observed and<br />

theoretical) and Miller indices.<br />

Lin (Counts)<br />

15000<br />

14000<br />

13000<br />

12000<br />

11000<br />

10000<br />

9000<br />

8000<br />

7000<br />

6000<br />

5000<br />

4000<br />

3000<br />

2000<br />

1000<br />

0<br />

d=2.80234<br />

d=2.59317<br />

d=2.46696<br />

d=1.90587<br />

d=1.62142<br />

d=1.47477<br />

30 40 50 60 70 80 90 100<br />

2-Theta - Scale<br />

ZnO_Powder - File: ZnO_Powder.RAW - Type: 2Th/Th locked - Start: 10.000 ° - End: 100.000 ° - Step: 0.020 ° - Step time: 2. s - Temp.: 25 °C (Room) - Time Started: 0 s - 2-Theta: 10.000 ° - Theta: 5.000 °<br />

Operations: Import<br />

36-1451 (*) - Zincite, syn - ZnO - Y: 50.00 % - d x by: 1. - WL: 1.5406 - Hexagonal - a 3.24982 - b 3.24982 - c 5.20661 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P63mc (186) - 2 - 47.6216 -<br />

Fig. (5.4): XRD trace of 99.9995% ZnO powder, sourced from Alfa Aesar (⎯ JCPDS<br />

card number 36-1451: ZnO, hexagonal, P63mc).<br />

It can be seen from this trace, that the ZnO powder used in this study was phase pure,<br />

resulting in a match to JCPDS card number 36-1451: ZnO, hexagonal, space group<br />

P63mc.<br />

d=1.40508<br />

d=1.37646<br />

d=1.35671<br />

d=1.23654<br />

d=1.18029<br />

d=1.09235<br />

d=1.08966<br />

d=1.06312<br />

d=1.04161<br />

d=1.03909<br />

d=1.01532<br />

d=1.01296

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