semmelweis university 2 0 1 2 / 2 0 1 3
semmelweis university 2 0 1 2 / 2 0 1 3 semmelweis university 2 0 1 2 / 2 0 1 3
PHARMACEUTICAL CHEMISTRY Director: Dr. Péter Horváth Tutor: Prof. Dr. Krisztina Takács–Novák First Semester SEMMELWEIS UNIVERSITY / FACULTY OF PHARMACY Week Lectures (4 hours per week) Introduction. (Pharmaceutical Chemistry, Practicals (5 hours per week) 1 Pharmacopoeias ) Methods for identification of inorganic compounds. Solubility, acidity-basicity. Equipping, repetitional analytical tasks. Preliminary testing of organic compounds, Preliminary testing and systematization of 2 classification inorganic and organic compounds official in Identification of organic functional groups Ph. Eur. Preliminary testing and systematization of 3 General purity tests in Pharmacopoeias inorganic and organic compounds official in Ph. Eur. 4 Structural and physical chemistry of drug action I.-II General reaction of organic functional groups Analysis of IR spectra 5 Structural and physical chemistry of drug action III-IV. General purity tests of inorganic ions I. 6 Narcotics Sedato-hypnotics and anxiolytics General purity tests of inorganic ions II. 7 Major analgetics General purity tests of inorganic ions III. 8 Minor analgetics Complete pharmacopoeial qualification of an inorganic compound official in Ph. Eur. 9 Psychopharmacons UV-VIS spectroscopy in the analysis of drug mixtures Narcotics, sedato-hypnotics 10 ORD and CD spectroscopy in the analysis of drug mixtures Separation techniques I.-V. Major analgetics I. 11 Application of chromatographic methods for the drug analysis. TLC Major analgetics II. 12 GC, HPLC, CE Minor analgetics I. 13 Cholinergic and adrenergic agents Minor analgetics II. 14 Cholinergic and adrenergic agents Psychopharmacons Faculty of Pharmacy 433
SEMMELWEIS UNIVERSITY / FACULTY OF PHARMACY 434 PHARMACEUTICAL CHEMISTRY Second Semester Week Lectures (4 hours per week) Practicals (5 hours per week) 1 Protonspeciation of drugs Equipping, identification 2 Determination of protonation constants Optimization of pH-dependent processes Cardiac glycosides, sugars Analysis of cardiac glycosides, sugars Drugs acting on the vegetative nervous system I. Drugs acting on the vegetative nervous system II. 3 4 Local anaesthetics Local anaesthetics 5 Cardiovascular drugs: antiarrhythmic agents Cardiovascular drugs: antianginal agents Digitalis glycosides, sugars 6 Cardiovascular drugs: antilipaemic agents Cardiovascular drugs: antihypertensive agents Determination of protonation macroconstants 7 Diuretics Determination of protonation microconstants 8 Vitamines Determination of logP 9 Quality assurrance, GLP, validation Non-steroid antiinflammatory agents Diuretics 10 Corticosteroids Sexual hormones Steroidal hormones 11 NMR:??phenomena NMR:??d, J, T1, T2 Complete pharmacopoeial qualification of an organic compound official in Ph. Eur. 12 NMR:??multiplicity, 1D NMR NMR:??spin echo, 2D NMR, MRI, MRS Non-steroidal antiinflammatory agents 13 Desinfectants Chemotherapeutic agents: sulfonamides Chemotherapeutic agents: antimalarial drugs, Quality assurance, GLP, validation I. 14 fluoroquinolones Antidiabetics Quality assurance, GLP, validation II.
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PHARMACEUTICAL CHEMISTRY<br />
Director: Dr. Péter Horváth<br />
Tutor: Prof. Dr. Krisztina Takács–Novák<br />
First Semester<br />
SEMMELWEIS UNIVERSITY / FACULTY OF PHARMACY<br />
Week Lectures (4 hours per week)<br />
Introduction. (Pharmaceutical Chemistry,<br />
Practicals (5 hours per week)<br />
1<br />
Pharmacopoeias )<br />
Methods for identification of inorganic compounds.<br />
Solubility, acidity-basicity.<br />
Equipping, repetitional analytical tasks.<br />
Preliminary testing of organic compounds,<br />
Preliminary testing and systematization of<br />
2 classification<br />
inorganic and organic compounds official in<br />
Identification of organic functional groups<br />
Ph. Eur.<br />
Preliminary testing and systematization of<br />
3 General purity tests in Pharmacopoeias<br />
inorganic and organic compounds official in<br />
Ph. Eur.<br />
4 Structural and physical chemistry of drug action I.-II<br />
General reaction of organic functional groups<br />
Analysis of IR spectra<br />
5 Structural and physical chemistry of drug action III-IV. General purity tests of inorganic ions I.<br />
6<br />
Narcotics<br />
Sedato-hypnotics and anxiolytics<br />
General purity tests of inorganic ions II.<br />
7 Major analgetics General purity tests of inorganic ions III.<br />
8 Minor analgetics<br />
Complete pharmacopoeial qualification of an<br />
inorganic compound official in Ph. Eur.<br />
9 Psychopharmacons<br />
UV-VIS spectroscopy in the analysis of drug mixtures<br />
Narcotics, sedato-hypnotics<br />
10 ORD and CD spectroscopy in the analysis of drug<br />
mixtures<br />
Separation techniques I.-V.<br />
Major analgetics I.<br />
11<br />
Application of chromatographic methods for the drug<br />
analysis.<br />
TLC<br />
Major analgetics II.<br />
12 GC, HPLC, CE Minor analgetics I.<br />
13 Cholinergic and adrenergic agents Minor analgetics II.<br />
14 Cholinergic and adrenergic agents Psychopharmacons<br />
Faculty of<br />
Pharmacy<br />
433