semmelweis university 2 0 1 2 / 2 0 1 3
semmelweis university 2 0 1 2 / 2 0 1 3 semmelweis university 2 0 1 2 / 2 0 1 3
Lectures (2 hours per week) Practicals (5 hours per week) Topic Task Spectrophotometric determination of phosphate content in egg shell Semi-quantitativ” Semi-quantitative analysis using analysis “Merkoquant” testpapers Different planar chromatographic (Public) Holiday methods and their use in pharmaceutical analyses. Gas chromatographic methods. High performance liquid chromato- Optional From “Potentiometric determinations” graphy. Supercritical fluid extraction measurements* From “Other determinations” and chromatography. HPCE and its future application. Final test TEST III. Survey on analytical chemistry. (Qualitative and quantitative analysis of complex samples) + Determination Quantitative determination of the sample Summary. Supplements Supplements Closing Closing SEMMELWEIS UNIVERSITY / FACULTY OF PHARMACY Potentiometric determinations: 1. Direct potentiometric determination of fluoride content in tooth paste 2. Potentiometric titration of bromide content of “Elixirium thymi composita” 3. Potentiometric titrations of iodide and chloride ions in presence of each other 4. Potentimetric titration using computer controlled burette: Determination of phosphoric acid content in “Coca Cola” Other determinations: 1. Complexometric determianation of metals in coins: (e.g..1,- Ft; 2,- Ft; 5,- Ft; US cent; Groschen) (Cu2 + -Ni 2 + ;Cu2 + -Ni2 + -Zn2 + ;Cu2 + ;Al3 + ) 2. Determination of calcium and magnesium ions in mineral water (e.g.. Römerquelle, Teodora Quelle, Margitszigeti), in bitter water (Míra) and in tap water 3. Chelatometric determination of aluminium ions in “Aluminium aceticum tartaricum solutum” 4. Iodometric determination of Cr3 + ions 5. Permanganometric determination of hydrogen peroxide content in tablet “Hyperol” 6. Complex analysis of “Solutio iodi alcoholica” 7. Determination of “Papaverinium chloride” in nonaqueous solution (glacial acetic acid) 8. Conductometric determination of acid contents in red wine Faculty of Pharmacy 419
SEMMELWEIS UNIVERSITY / FACULTY OF PHARMACY 420 ORGANIC CHEMISTRY Lecturer: Prof. Dr. Péter Mátyus Tutor: Dr. Péter Tétényi First Semester Week Lectures (4+1*** hours per week) 1 Qualitative molecular orbital theory of organic compounds 2-3 Saturated acyclic and cyclic hydrocarbons. Constitution, conformation 4 Stereochemistry of organic compounds. Configuration. Compounds having one center of chirality. Principles of the IUPAC nomenclature. 5 Isomerism. Steric and electronic effects in organic compounds and reactions. 6-7 Alkenes, alkynes, and their cyclic analogs. Cis-trans isomerism. Elimination. Addition to carbon-carbon double bond. 8 delocalized systems. Aromaticity and?Linear and cyclic antiaromaticity. Interpretation of concerted reactions. 9 Aromatic hydrocarbons. Electrophilic aromatic substitution 10 Spectroscopy of organic compounds. 11-12 Organic halogen compounds. Nucleophilic substitution in aliphatic and aromatic compounds. 13 Organic compounds containing C-O single bonds (alcohols, phenols and their derivatives). Acidity of organic compounds. 14 Amines and other nitrogen containing compounds. Basicity of organic compounds. Organic sulfur compounds. *** number of hour (1) for introductory lecture No. of practices Practicals (seminars: 2 hours biweekly, practices: 8 hours biweekly) 1-2 Basic laboratory processes. 2-6 3-6 5-6 Nomenclature of organic compounds without C=O bond Basic methods for preparations of organic compounds (5 preparations) Spectroscopic analysis of organic compounds
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SEMMELWEIS UNIVERSITY / FACULTY OF PHARMACY<br />
420<br />
ORGANIC CHEMISTRY<br />
Lecturer: Prof. Dr. Péter Mátyus<br />
Tutor: Dr. Péter Tétényi<br />
First Semester<br />
Week Lectures (4+1*** hours per week)<br />
1<br />
Qualitative molecular orbital theory of organic<br />
compounds<br />
2-3<br />
Saturated acyclic and cyclic hydrocarbons. Constitution,<br />
conformation<br />
4<br />
Stereochemistry of organic compounds. Configuration.<br />
Compounds having one center of chirality. Principles of<br />
the IUPAC nomenclature.<br />
5<br />
Isomerism. Steric and electronic effects in organic<br />
compounds and reactions.<br />
6-7<br />
Alkenes, alkynes, and their cyclic analogs. Cis-trans<br />
isomerism. Elimination. Addition to carbon-carbon double<br />
bond.<br />
8<br />
delocalized systems. Aromaticity and?Linear and cyclic<br />
antiaromaticity. Interpretation of concerted reactions.<br />
9<br />
Aromatic hydrocarbons. Electrophilic aromatic<br />
substitution<br />
10<br />
Spectroscopy of organic compounds.<br />
11-12<br />
Organic halogen compounds. Nucleophilic substitution in<br />
aliphatic and aromatic compounds.<br />
13<br />
Organic compounds containing C-O single bonds<br />
(alcohols, phenols and their derivatives). Acidity of<br />
organic compounds.<br />
14<br />
Amines and other nitrogen containing compounds.<br />
Basicity of organic compounds. Organic sulfur<br />
compounds.<br />
*** number of hour (1) for introductory lecture<br />
No. of<br />
practices<br />
Practicals (seminars: 2 hours<br />
biweekly, practices: 8 hours biweekly)<br />
1-2 Basic laboratory processes.<br />
2-6<br />
3-6<br />
5-6<br />
Nomenclature of organic compounds<br />
without C=O bond<br />
Basic methods for preparations of<br />
organic compounds (5 preparations)<br />
Spectroscopic analysis of organic<br />
compounds