Download (8Mb) - Etheses - Saurashtra University
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C12-C13 1.372(4) C32-C37 1.390(3)<br />
C13-C14 1.383(4) C33-C34 1.382(3)<br />
C13-O15 1.392(3) C34-C35 1.372(4)<br />
O15-C16 1.387(3) C35-C36 1.379(4)<br />
C16-C17 1.353(4) C36-C37 1.378(3)<br />
C16-C21 1.362(5)<br />
Table-2: Bond lengths (Å)<br />
Atoms Angle(˚) Atoms Angle(˚)<br />
C2-N1-C6 122.62(2) C21-C16-O15 117.5(3)<br />
N1-C2-C3 118.10(2) C16-C17-C18 118.2(3)<br />
N1-C2-C8 113.33(2) C19-C18-C17 119.5(4)<br />
C3-C2-C8 128.53(2) C20-C19-C18 121.0(4)<br />
C2-C3-C30 126.66(2) C19-C20-C21 120.7(4)<br />
C2-C3-C4 118.06(2) C20-C21-C16 119.1(3)<br />
C30-C3-C4 115.09(2) O23-C22-C5 123.7(2)<br />
C3-C4-C5 108.93(1) O23-C22-C24 119.5(2)<br />
C3-C4-C9 114.15(2) C5-C22-C24 116.65(2)<br />
C5-C4-C9 109.54(2) C25-C24-C29 118.8(3)<br />
C6-C5-C22 122.16(2) C25-C24-C22 121.4(2)<br />
C6-C5-C4 118.62(2) C29-C24-C22 119.7(2)<br />
C22-C5-C4 119.04(2) C26-C25-C24 120.6(3)<br />
C5-C6-N1 117.99(2) C27-C26-C25 119.9(3)<br />
C5-C6-C7 127.0(2) C26-C27-C28 120.0(3)<br />
N1-C6-C7 114.96(2) C27-C28-C29 120.9(3)<br />
C10-C9-C14 117.8(2) C28-C29-C24 119.8(3)<br />
C10-C9-C4 123.18(2) O31-C30-C3 118.58(2)<br />
C14-C9-C4 118.97(2) O31-C30-C32 117.36(2)<br />
C9-C10-C11 120.7(2) C3-C30-C32 123.99(2)<br />
C12-C11-C10 121.3(3) C33-C32-C37 119.10(2)<br />
C11-C12-C13 118.6(2) C33-C32-C30 118.92(2)<br />
C12-C13-C14 121.0(2) C37-C32-C30 121.67(2)<br />
C12-C13-O15 116.8(2) C34-C33-C32 120.4(2)<br />
C14-C13-O15 122.0(3) C35-C34-C33 120.1(2)<br />
C13-C14-C9 120.5(2) C34-C35-C36 119.9(2)<br />
C16-O15-C13 119.0(2) C37-C36-C35 120.6(2)<br />
C17-C16-C21 121.5(3) C36-C37-C32 119.9(2)<br />
C17-C16-O15 120.8(3)<br />
Table-3: Bond angles (˚)<br />
Atoms Length (Å) Angle(˚) Symmetry codes<br />
N1–H1. . .O31 2.999(2) 156 1 + x, y, z<br />
Table-4: Hydrogen bonding geometry