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the coking properties of coal at elevated pressures. - Argonne ...

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I<br />

FIG. 1. Initial ash co<strong>at</strong>ing on quartz<br />

bed m<strong>at</strong>erial. SEM/BEI image. Analysis<br />

A (Table 3). Run 2181, 40 hrs.<br />

FIG. 3. Quartz bed grains loosely ce-<br />

mented by sulf<strong>at</strong>ed aluminosilic<strong>at</strong>e ash.<br />

SEM/BEI image. Analysis D given in Table<br />

3. Run 2181, 69 hrs.<br />

173<br />

FIG. 2. Thickened nodular ash co<strong>at</strong>ing<br />

on quartz bed m<strong>at</strong>erial. SEM/BEI image.<br />

Analysis B <strong>of</strong> fine light sulf<strong>at</strong>ed ash<br />

and C <strong>of</strong> darker interior <strong>of</strong> coarser ash<br />

particle (Table 3). Run 2181, 54 hrs.<br />

FIG. 4. Quartz bed agglomer<strong>at</strong>e bonded by<br />

altered sulf<strong>at</strong>ed ash, bottom <strong>of</strong> <strong>the</strong> dot-<br />

ted boundary (analysis E); Ca-rich, S-<br />

poor glass, top <strong>of</strong> <strong>the</strong> dashed line (analy-<br />

sis F); and intermedi<strong>at</strong>e fringe <strong>of</strong> meli-<br />

lite or augite crystals. SEM/BEI image.<br />

Run 2181, 69 hrs.

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