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liquefaction pathways of bituminous subbituminous coals andtheir

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100,<br />

50<br />

0.<br />

Retention Time (min.1<br />

100<br />

50<br />

Figure 4. Selective ion monitoring <strong>of</strong> paraffins 10 15 20 25<br />

at m/z 71 from Py-GC-MS pr<strong>of</strong>iles <strong>of</strong> residues from<br />

Retention Time (min.)<br />

thermal <strong>liquefaction</strong>s <strong>of</strong> the coal a) raw, b) vacuum-<br />

dried at 100°C. died in airat l00T for c) 2 h,<br />

d) 20 h, e) 100 h, and f) dned at 150°C for 20 h.<br />

Figure.5. Py-GC-MS pr<strong>of</strong>iles <strong>of</strong> the residues from the<br />

thermal <strong>liquefaction</strong>s in presence <strong>of</strong> tenalin <strong>of</strong> the coal a) raw,<br />

b) vacuum-dried at 100OC, dried in air at 100°C for c) 2 h,<br />

d) 20 h, e) 100 h, and 9 dried at 15OOC for 20 h.<br />

608

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