TEST INSTRUCTIONS - Geotech Environmental Equipment

TEST INSTRUCTIONS - Geotech Environmental Equipment TEST INSTRUCTIONS - Geotech Environmental Equipment

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PROCEDURE Use 10 mm square cell adapter. 1. Press and hold ON button until colorimeter turns on. 2. Press ENTER to start. 3. Press ENTER to selct TESTING MENU. 4. Select ALL TESTS (or another sequence containing 37 Cyanuric-UDV)from TESTING MENU. 5. Scroll to and select 37 Cyanuric-UDV from menu. 6. Rinse a clean vial (0156) with sample water. 7. Use the syringe (1184) to add 3 mL of sample to the vial. 8. Insert the vial into chamber, close lid and select SCAN BLANK. 9. Remove vial from colorimeter. 10. Use the syringe (1184) to add 3 mL of sample to a Cyanuric Acid UDV vial (4313). 11. Invert the vial 3 times to mix. 12. Wait 2 minutes. 13. Invert vial 3 more times to mix. NOTE: Firmly tap side of vial 5-10 times to remove all air bubbles. 14. Insert tube into chamber, close lid and select SCAN SAMPLE. Record result. 15. Press OFF button to turn the colorimeter off or press EXIT button to exit to a previous menu or make another menu selection. NOTE: For best possible results, a reagent blank should be determined to account for any contribution to the test result by the reagent system. To determine the reagent blank, follow the above test procedure to scan a distilled or deionized water blank. Then follow the above procedure to perform the test on a distilled or deionized water sample. This test result is the reagent blank. Subtract the reagent blank from all subsequent test results of unknown samples. It is necessary to determine the reagent blank only when a new lot number of reagents are obtained. UDVs from opened pouches should be used promptly. Store unused vials from opened pouches in the Foil Storage Bag (9467) to extend the shelf life of the reagent. Generally, UDVs stored in the bag should be used within 10 days if the humidity is less than 50% and within 5 days if humidity is greater than 50%. The Foil Storage Bag contains a desiccant pack. Cyanuric Acid–UDV 2/2 Smart2 TEST PROCEDURES 2.04

DISSOLVED OXYGEN WINKLER COLORIMETRIC METHOD CODE 3688-SC QUANTITY CONTENTS CODE 30 mL *Manganese Sulfate Solution *4167-G 30 mL *Alkaline Potassium Iodide Azide *7166-G 30 mL *Sulfuric Acid 1:1 *6141WT-G 1 Sample Tube, screw cap 29180 1 Cap 28570 *WARNING: Reagents marked with an * are considered hazardous substances. To view or print a Material Safety Data Sheet (MSDS) for these reagents see MSDS CD or our web site. To obtain a printed copy, contact us by e-mail, phone or fax. Dissolved oxygen is vital to the survival of aquatic organisms. Naturally present, dissolved oxygen enters the water when plants photosynthesize. Wind and wave action also cause oxygen from the air to dissolve into water. Dissolved oxygen is consumed by aquatic animals and by the oxidation, or chemical breakdown, of dead and decaying plants and animals. The concentration of dissolved oxygen in natural waters can range from 0 to 14 ppm and is effected by temperature and salinity. APPLICATION: This method is applicable for the determination of dissolved oxygen in drinking water, all surface waters and wastewater. RANGE: 0.0–11.0 Dissolved Oxygen METHOD: This method uses the azide modification of the Winkler Method with a colorimetric determination of the yellow iodine produced from the reaction with the dissolved oxygen. INTERFERENCES: The presence of other oxidizing agents may cause positive interferences. Reducing may cause negative interferences. Nitrite interferences are eliminated with the azide modification. Smart2 TEST PROCEDURES 2.04 Dissolved Oxygen 1/3

PROCEDURE<br />

Use 10 mm square cell adapter.<br />

1. Press and hold ON button until colorimeter turns on.<br />

2. Press ENTER to start.<br />

3. Press ENTER to selct <strong>TEST</strong>ING MENU.<br />

4. Select ALL <strong>TEST</strong>S (or another sequence containing<br />

37 Cyanuric-UDV)from <strong>TEST</strong>ING MENU.<br />

5. Scroll to and select 37 Cyanuric-UDV from menu.<br />

6. Rinse a clean vial (0156) with sample water.<br />

7. Use the syringe (1184) to add 3 mL of sample to the vial.<br />

8. Insert the vial into chamber, close lid and select SCAN BLANK.<br />

9. Remove vial from colorimeter.<br />

10. Use the syringe (1184) to add 3 mL of sample to a Cyanuric Acid UDV<br />

vial (4313).<br />

11. Invert the vial 3 times to mix.<br />

12. Wait 2 minutes.<br />

13. Invert vial 3 more times to mix.<br />

NOTE: Firmly tap side of vial 5-10 times to remove all air bubbles.<br />

14. Insert tube into chamber, close lid and select SCAN SAMPLE. Record<br />

result.<br />

15. Press OFF button to turn the colorimeter off or press EXIT button to exit<br />

to a previous menu or make another menu selection.<br />

NOTE: For best possible results, a reagent blank should be determined to<br />

account for any contribution to the test result by the reagent system. To<br />

determine the reagent blank, follow the above test procedure to scan a distilled<br />

or deionized water blank. Then follow the above procedure to perform the test<br />

on a distilled or deionized water sample. This test result is the reagent blank.<br />

Subtract the reagent blank from all subsequent test results of unknown samples.<br />

It is necessary to determine the reagent blank only when a new lot number of<br />

reagents are obtained.<br />

UDVs from opened pouches should be used promptly. Store unused vials from<br />

opened pouches in the Foil Storage Bag (9467) to extend the shelf life of the<br />

reagent. Generally, UDVs stored in the bag should be used within 10 days if<br />

the humidity is less than 50% and within 5 days if humidity is greater than<br />

50%. The Foil Storage Bag contains a desiccant pack.<br />

Cyanuric Acid–UDV 2/2 Smart2 <strong>TEST</strong> PROCEDURES 2.04

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