24.04.2013 Views

TEST INSTRUCTIONS - Geotech Environmental Equipment

TEST INSTRUCTIONS - Geotech Environmental Equipment

TEST INSTRUCTIONS - Geotech Environmental Equipment

SHOW MORE
SHOW LESS

Create successful ePaper yourself

Turn your PDF publications into a flip-book with our unique Google optimized e-Paper software.

COD–STANDARD RANGE<br />

MERCURY FREE DIGESTION CODE 0073-SC<br />

MERCURY DIGESTION CODE 0076-SC<br />

QUANTITY CONTENTS CODE<br />

25 *COD Standard Range Mercury Free Tubes *0073-SC<br />

or 25 *COD Standard Range Mercury Tubes *0076-SC<br />

*WARNING: Reagents marked with an * are considered hazardous substances. To<br />

view or print a Material Safety Data Sheet (MSDS) for these reagents see MSDS CD<br />

or our web site. To obtain a printed copy, contact us by e-mail, phone or fax.<br />

COD Standard Range Mercury Free Tubes are not USEPA approved.<br />

COD Standard Range Mercury Tubes are USEPA approved.<br />

<strong>Equipment</strong> needed but not supplied:<br />

QUANTITY CONTENTS CODE<br />

1 COD Adapter 5-0087<br />

1 COD Reactor, 12 vial, 110V 5-0102<br />

or 1 COD Reactor, 12 vial, 230V 5-0102-EX2<br />

1 Measuring Pipet, 1.0 mL 2-2110<br />

1 Pipet Bulb 2-2164<br />

Chemical Oxygen Demand (COD) is a measure of the amount of organic<br />

matter in water which is susceptible to oxidation by chemical oxidants. COD<br />

can be empirically related to the Biological Oxygen Demand (BOD) and<br />

organic carbon content of a specific source of water. This correlation must be<br />

determined experimentally for each source of water.<br />

APPLICATION: Domestic and industrial wastes.<br />

RANGE: 0–1500 mg/L COD<br />

METHOD: Dichromate in the presence of silver salts, at high<br />

temperature in a closed system, oxidizes most organic<br />

compounds to 95-100% of the theoretical amount. This<br />

process is called digestion. As dichromate oxidizes the<br />

organic compounds, a green complex is formed. The<br />

concentration of the green complex is measured at 605 nm<br />

SAMPLE<br />

HANDLING &<br />

PRESERVATION:<br />

and is directly proportional to the COD of the sample.<br />

Collect samples in glass and test as soon as possible. If<br />

samples must be stored, preservation is accomplished by the<br />

addition of concentrated H2SO4 to adjust the pH below 2.<br />

Samples with suspended solids should be homogenized in a<br />

blender (100 mL for 30 seconds) and then stirred gently<br />

with a magnetic stirrer.<br />

Smart2 <strong>TEST</strong> PROCEDURES 03.05 COD–Standard Range 1/4

Hooray! Your file is uploaded and ready to be published.

Saved successfully!

Ooh no, something went wrong!