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TEST INSTRUCTIONS - Geotech Environmental Equipment

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NOTES: Reagents are light sensitive. Unused reagents should be stored in the<br />

shipping container, and in the refrigerator if possible, until needed.<br />

A reagent blank should be run with each set of samples and with each lot of<br />

reagents.<br />

The reacted blank will be stable if stored in the dark.<br />

To eliminate error caused by contamination, wash all glassware with 20%<br />

sulfuric acid.<br />

For greater accuracy, a minimum of three repetitions should be performed and<br />

the results averaged.<br />

Some samples may be digested completely in less than two hours. The<br />

concentration may be measured at 15 minute intervals while the vials are still<br />

hot until the reading remains unchanged. The vials should be cooled to room<br />

temperature before the final measurement is taken.<br />

COD–LR 4/4 Smart2 <strong>TEST</strong> PROCEDURES 03.05

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