TEST INSTRUCTIONS - Geotech Environmental Equipment

TEST INSTRUCTIONS - Geotech Environmental Equipment TEST INSTRUCTIONS - Geotech Environmental Equipment

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PROCEDURE 1. Press and hold ON button until colorimeter turns on. 2. Press ENTER to start. 3. Press ENTER to select TESTING MENU. 4. Select ALL TESTS (or another sequence containing 20 CHLOR DIOX) from TESTING MENU. 5. Scroll to and select 20 CHLOR DIOX from menu. 6. Rinse a clean tube (0290) with sample water. Fill to 10 mL line with sample. 7. Insert tube into chamber, close lid and select SCAN BLANK. 8. Remove tube from colorimeter. Pour out all but a sufficient amount of sample water to cover tablet. Add 5 drops of Glycine Solution (6811). 9. Add one *Chlorine DPD #1 Instrument Grade Tablet (6903). Crush tablet with tablet crusher. Cap and shake until tablet dissolves. Fill to 10 mL line with sample water. Solution will turn pink if chlorine dioxide is present. Wait 15 seconds, but no longer than 30 seconds. Mix. 10. Insert tube into chamber, close lid and select SCAN SAMPLE. 11. Press OFF button to turn colorimeter off or press EXIT button to exit to a previous menu or make another menu selection. Chlorine Dioxide 2/2 Smart2 TEST PROCEDURES 2.04

CHROMIUM DIPHENYLCARBOHYDRAZIDE METHOD CODE 3697-SC QUANTITY CONTENTS CODE 50 *Chromium Spectrophotometric Grade Tablets *3889A-H 1 Tablet Crusher 0175 *WARNING: Reagents marked with a * are considered to be potential health hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents see MSDS CD or www.lamotte.com. To obtain a printed copy, contact LaMotte by email, phone or fax. Chromium is one of a class of heavy metals found in the bottom mud of polluted bodies of water. It is considered to be a toxic chemical. Chromium will become concentrated in some shellfish, endangering the health of the human or animal that consumes them. Chromium may be present in water containing waste from industries such as metal plating. If more than 0.5 ppm chromium is present, it is evidence of contamination from untreated or incompletely treated industrial waste. APPLICATION: Drinking, surface, and saline waters; domestic and industrial wastewaters. RANGE: 0.00–1.00 ppm Chromium METHOD: Hexavalent chromium reacts with 1,5 diphenylcarbohydrazide under acidic conditions to form a red-purple color in proportion to the amount of chromium SAMPLE HANDLING & PRESERVATION: present. Analysis for chromium should be made as quickly as possible. Storage in plastic or glass containers may result in low results. INTERFERENCES: High concentrations of mercurous and mercuric ions may impart a blue color to the chromium determination. Iron and vanadium in concentrations above 1 ppm may result in a yellow color. Smart2 TEST PROCEDURES 1.07 Chromium-TesTab 1/2

PROCEDURE<br />

1. Press and hold ON button until colorimeter turns on.<br />

2. Press ENTER to start.<br />

3. Press ENTER to select <strong>TEST</strong>ING MENU.<br />

4. Select ALL <strong>TEST</strong>S (or another sequence containing 20 CHLOR DIOX)<br />

from <strong>TEST</strong>ING MENU.<br />

5. Scroll to and select 20 CHLOR DIOX from menu.<br />

6. Rinse a clean tube (0290) with sample water. Fill to 10 mL line with<br />

sample.<br />

7. Insert tube into chamber, close lid and select SCAN BLANK.<br />

8. Remove tube from colorimeter. Pour out all but a sufficient amount of<br />

sample water to cover tablet. Add 5 drops of Glycine Solution (6811).<br />

9. Add one *Chlorine DPD #1 Instrument Grade Tablet (6903). Crush<br />

tablet with tablet crusher. Cap and shake until tablet dissolves. Fill to 10<br />

mL line with sample water. Solution will turn pink if chlorine dioxide is<br />

present. Wait 15 seconds, but no longer than 30 seconds. Mix.<br />

10. Insert tube into chamber, close lid and select SCAN SAMPLE.<br />

11. Press OFF button to turn colorimeter off or press EXIT button to exit to a<br />

previous menu or make another menu selection.<br />

Chlorine Dioxide 2/2 Smart2 <strong>TEST</strong> PROCEDURES 2.04

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