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TEST INSTRUCTIONS - Geotech Environmental Equipment

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NITRATE<br />

ZINC REDUCTION CODE 3689-SC<br />

QUANTITY CONTENTS CODE<br />

50 *Nitrate Spectrophotometric Grade Tablets *3881A-H<br />

1 Tablet Crusher 0175<br />

*WARNING: Reagents marked with a * are considered to be potential health<br />

hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents see<br />

MSDS CD or www.lamotte.com. To obtain a printed copy, contact LaMotte by email,<br />

phone or fax.<br />

Nitrogen is essential for plant growth, but excessive amounts in water supplies<br />

can result in nutrient pollution. Nitrates, in conjunction with phosphate,<br />

stimulate the growth of algae creating water quality problems. Nitrogen<br />

compounds may enter water as nitrates or be converted to nitrates from<br />

agricultural fertilizers, sewage, industrial and packing house wastes, drainage<br />

from livestock feeding areas and manure. Nitrates in large amounts in drinking<br />

water can cause “blue baby syndrome” (methemoglobenemia) in infants in less<br />

than 6 months of age and other health problems. US Public Health Service<br />

Drinking Water Standards state that 44 ppm nitrate should not be exceeded.<br />

To the sanitary and industrial engineer, concentrations of less than 4 ppm are<br />

acceptable.<br />

APPLICATION: Drinking, surface, and saline waters; domestic and industrial<br />

waters.<br />

RANGE: 0.0–60.0 ppm Nitrate<br />

METHOD: Zinc is used to reduce nitrate to nitrite. The nitrite that was<br />

originally present, plus the reduced nitrate, reacts with<br />

chromotropic acid to form a red color in proportion to the<br />

SAMPLE<br />

HANDLING &<br />

PRESERVATION:<br />

amount of nitrite in the sample.<br />

Analysis should be made as soon as possible. If analysis<br />

cannotbemadewithin24hours,thesampleshouldbe<br />

refrigerated at 4C. When samples must be stored for more<br />

than 24 hours, add 2 mL of concentrated sulfuric acid per<br />

liter of sample. For best results, the analysis for nitrate should<br />

be determined at temperatures between 20Cand25C.<br />

INTERFERENCES: Nitrite interferes at all concentrations. Strong oxidizing and<br />

reducing substances interfere. Low results might be obtained<br />

for samples that contain high concentrations of copper and<br />

iron.<br />

Smart2 <strong>TEST</strong> PROCEDURES 1.07 Nitrate-TesTab 1/2

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