TEST INSTRUCTIONS - Geotech Environmental Equipment

TEST INSTRUCTIONS - Geotech Environmental Equipment TEST INSTRUCTIONS - Geotech Environmental Equipment

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PROCEDURE 1. Press and hold ON button until colorimeter turns on. 2. Press ENTER to start. 3. Press ENTER to select Testing Menu. 4. Select ALL TESTS (or another sequence containing 47 H Per-HR) from TESTING MENU. 5. Scroll to and select 47 H Per-HR from menu. 6. Use the pipet (0342) to add 5 drops of the sample water to a tube (0290). 7. Dilute to the 10 mL line with distilled or hydrogen peroxide-free water. 8. Insert the tube into chamber, close lid and select SCAN BLANK. 9. Remove the tube from colorimeter and add 4 drops of *Hydrogen Peroxide Reagent #1 (6452). Cap and mix. 10. Add one *Hydrogen Peroxide LR Tablet (6454). Crush tablet with Tablet Crusher (0175). Cap and mix for 30 seconds. Solution will turn pink if hydrogen peroxide is present. Wait 5 minutes for full color development. 11. At the end of 5 minute waiting period, mix, insert tube into chamber, close lid and select SCAN SAMPLE. Record result. 12. Press OFF button to turn the meter off or press EXIT button to exit to a previous menu or make another menu selection. NOTES: For best possible results, a blank should be determined to account for any contribution to the test result by the reagent system. To determine the reagent blank, follow the above test procedure to scan a distilled or deionized water blank. Then follow the above procedure to perform the test on a distilled or deionized water sample. This test result is the reagent blank. Subtract the reagent blank from all subsequent test results of unknown samples. It is necessary to determine the reagent blank only when a new lot number of reagents are obtained. For the most accurate results, the sample and reagents should be at 25 ±4°C. Hydrogen Peroxide–HR 2/2 Smart2 TEST PROCEDURES 2.04

HYDROGEN PEROXIDE–SHOCK DPD Method CODE 4045 QUANTITY CONTENTS CODE 30 mL *Hydrogen Peroxide Reagent #1 *6452-G 100 *Hydrogen Peroxide LR Tablets *6454-J 1 Tablet Crusher 0175 1 Pipet, glass 0342 *WARNING: Reagents marked with an * are considered hazardous substances. To view or print a Material Safety Data Sheet (MSDS) for these reagents see MSDS CD or our web site. To obtain a printed copy, contact us by e-mail, phone or fax. Large quantities of hydrogen peroxide shock are added to a swimming pool to “shock” it. Shocking breaks down waste products and re-establishes a positive level of sanitizer. While many types of shock can be used with chlorine or bromine pools, only hydrogen peroxide shock can be used to shock biguanide pools. APPLICATION: Swimming pools RANGE: 0–225 ppm Hydrogen Peroxide Shock METHOD: Hydrogen peroxide reacts with an excess of potassium iodide through the action of a catalyst and buffer to release an equivalent amount of iodine. The iodine in turn reacts with diethyl-p-phenylenediamine (DPD) to produce a pink-red SAMPLE HANDLING & PRESERVATION: color in proportion to the iodine released. Hydrogen peroxide is not stable in aqueous solutions. Exposure to sunlight and agitation will accelerate the reduction of hydrogen peroxide in dilute solutions. For best results start analysis immediately after sampling. INTERFERENCES: The likelihood of other oxidizing compounds interfering with this method is eliminated by the presence of hydrogen peroxide. Manganese may interfere and should be removed before analysis Smart2 TEST PROCEDURES 2.04 Hydrogen Peroxide–Shock 1/2

HYDROGEN PEROXIDE–SHOCK<br />

DPD Method CODE 4045<br />

QUANTITY CONTENTS CODE<br />

30 mL *Hydrogen Peroxide Reagent #1 *6452-G<br />

100 *Hydrogen Peroxide LR Tablets *6454-J<br />

1 Tablet Crusher 0175<br />

1 Pipet, glass 0342<br />

*WARNING: Reagents marked with an * are considered hazardous substances. To<br />

view or print a Material Safety Data Sheet (MSDS) for these reagents see MSDS CD<br />

or our web site. To obtain a printed copy, contact us by e-mail, phone or fax.<br />

Large quantities of hydrogen peroxide shock are added to a swimming pool to<br />

“shock” it. Shocking breaks down waste products and re-establishes a positive<br />

level of sanitizer. While many types of shock can be used with chlorine or<br />

bromine pools, only hydrogen peroxide shock can be used to shock biguanide<br />

pools.<br />

APPLICATION: Swimming pools<br />

RANGE: 0–225 ppm Hydrogen Peroxide Shock<br />

METHOD: Hydrogen peroxide reacts with an excess of potassium iodide<br />

through the action of a catalyst and buffer to release an<br />

equivalent amount of iodine. The iodine in turn reacts with<br />

diethyl-p-phenylenediamine (DPD) to produce a pink-red<br />

SAMPLE<br />

HANDLING &<br />

PRESERVATION:<br />

color in proportion to the iodine released.<br />

Hydrogen peroxide is not stable in aqueous solutions.<br />

Exposure to sunlight and agitation will accelerate the<br />

reduction of hydrogen peroxide in dilute solutions. For best<br />

results start analysis immediately after sampling.<br />

INTERFERENCES: The likelihood of other oxidizing compounds interfering<br />

with this method is eliminated by the presence of hydrogen<br />

peroxide. Manganese may interfere and should be removed<br />

before analysis<br />

Smart2 <strong>TEST</strong> PROCEDURES 2.04 Hydrogen Peroxide–Shock 1/2

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