VITAMIN A FORTIFIed PEANUT BUTTER - The Official Website of ...

VITAMIN A FORTIFIed PEANUT BUTTER - The Official Website of ... VITAMIN A FORTIFIed PEANUT BUTTER - The Official Website of ...

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used. From each production batch, one sample each was taken at the start, middle and end of filling. Premix used in this experiment was prepared using the Hobart planetary mixer of the industry collaborator. Results are shown in Table 2.9. Technology Transfer and Adoption To transfer the vitamin A fortification technology using a premix, a demonstration of the recommended process for vitamin A fortification of peanut butter was done during the standardization of the process at the collaborator's plant. The R&D Head, Production Head and two (2) production workers of the industry collaborator were trained on the proper method of adding and mixing the fortificant to peanut butter. A procedural guideline of the recommended process was likewise provided to the collaborator, a copy of which is shown in Appendix A. Preliminary Trials RESULTS Results of the dye test shown in Table 2.1 indicate that the dyed oil dispersed into the plain peanut butter after 5 min of mixing. Visual examination however, showed some of the dyed oil splattered at the sides of the mixer while some was noted at the bottom portion of the mixer. Scraping off of adhering product from the mixer and mixing of the peanut butter for another 5 min resulted in the full dispersion of the dyed oil into the plain peanut butter as indicated by the absence of reddish orange streaks in any part of the peanut butter mixture. The same observations were noted for the addition of dyed peanut butter to plain peanut butter. Considering the good dispersion of the dyed oil and of the dyed peanut butter in the plain peanut butter matrix, it was recommended that a total mixing time of 10 min be adapted for the mixing of the fortificant with plain peanut butter during the preparation of premix and of the premix during the preparation of the final fortified product. Manual mixing of the fortificant and premix with plain peanut butter was likewise recommended prior to mechanical mixing to facilitate their dispersion in the peanut butter matrix. Laboratory Trials at FDC Experiment 1: Validation of the adequacy of the 10 min mixing time established in the dye test Premix preparation. Results presented in Table 2.2 showed that peanut butter premix prepared in Trial 1 had an average vitamin A content of 263.70 µg RE/g peanut butter or a vitamin A recovery of 90.3%, indicating that approximately 10% of the vitamin A palmitate added was lost during processing. In terms of dispersion, it was found that the vitamin A added was uniformly distributed in the peanut butter premix as indicated by the low percentage variability of 2.78%. Premix prepared in Trial 2 likewise showed an acceptable vitamin A content of 273.61 µg RE/g peanut butter or a vitamin A recovery of 93.7%. 63

Table 2.1 Effect of mixing time on the dispersion of dyed oil and of dyed peanut butter in a peanut butter matrix after 5 and 10 min of mixing using a Hobart vertical mixer Model HCM 3 Observations Expt. Activity After 5 min mixing After additional 5 min mixing 1 2 Direct addition of dyed oil to plain peanut butter Direct addition of dyed peanut butter to plain peanut butter Presence of reddish orange streaks at the sides and bottom of mixer and occasional reddish streaks in the mixture; Bubble formations observed in the peanut butter mixture Presence of reddish orange streaks at the sides and bottom of mixer and occasional reddish streaks in the mixture; Bubble formations observed in the peanut butter mixture Absence of reddish orange streaks at the sides and bottom of the mixer and on the mixture; Bubble formations observed in the peanut butter mixture Absence of reddish orange streaks at the sides and bottom of the mixer and on the mixture; Bubble formation observed in the peanut butter mixture Table 2.2 Effect of 10 min mixing time on vitamin A recovery during laboratory preparation of premix at FDC Vitamin A Recovered Sampling Point Trial 1 Trial 2 (during filling) Vit. A Content (µg RE/g) % Recovery 1 Vit. A Content (µg RE/g) % Recovery 2 Start 271.97 93.10 --- N/A Middle 261.16 89.40 273.61 93.70 End 257.96 88.30 --- N/A Average 263.70 90.30 273.61 93.70 Std. Deviation 7.34 2.515 N/A N/A % Variability 2.78 2.78 N/A N/A 1 Expected level of vitamin A in the premix is 292 µg RE/g peanut butter. This was computed based on a fortificant with a vitamin A assay of 322,163.41 µg RE. 2 Expected level of vitamin A in the premix is 292 µg RE/g peanut butter. This was computed based on fortificant with a vitamin A assay of 117,735.51 µg RE. --- = No sample analyzed. 64

used. From each production batch, one sample each was taken at the start, middle and end <strong>of</strong> filling.<br />

Premix used in this experiment was prepared using the Hobart planetary mixer <strong>of</strong> the industry<br />

collaborator. Results are shown in Table 2.9.<br />

Technology Transfer and Adoption<br />

To transfer the vitamin A fortification technology using a premix, a demonstration <strong>of</strong> the<br />

recommended process for vitamin A fortification <strong>of</strong> peanut butter was done during the standardization <strong>of</strong><br />

the process at the collaborator's plant. <strong>The</strong> R&D Head, Production Head and two (2) production workers<br />

<strong>of</strong> the industry collaborator were trained on the proper method <strong>of</strong> adding and mixing the fortificant to<br />

peanut butter. A procedural guideline <strong>of</strong> the recommended process was likewise provided to the<br />

collaborator, a copy <strong>of</strong> which is shown in Appendix A.<br />

Preliminary Trials<br />

RESULTS<br />

Results <strong>of</strong> the dye test shown in Table 2.1 indicate that the dyed oil dispersed into the plain<br />

peanut butter after 5 min <strong>of</strong> mixing. Visual examination however, showed some <strong>of</strong> the dyed oil splattered<br />

at the sides <strong>of</strong> the mixer while some was noted at the bottom portion <strong>of</strong> the mixer. Scraping <strong>of</strong>f <strong>of</strong><br />

adhering product from the mixer and mixing <strong>of</strong> the peanut butter for another 5 min resulted in the full<br />

dispersion <strong>of</strong> the dyed oil into the plain peanut butter as indicated by the absence <strong>of</strong> reddish orange<br />

streaks in any part <strong>of</strong> the peanut butter mixture. <strong>The</strong> same observations were noted for the addition <strong>of</strong><br />

dyed peanut butter to plain peanut butter. Considering the good dispersion <strong>of</strong> the dyed oil and <strong>of</strong> the dyed<br />

peanut butter in the plain peanut butter matrix, it was recommended that a total mixing time <strong>of</strong> 10 min be<br />

adapted for the mixing <strong>of</strong> the fortificant with plain peanut butter during the preparation <strong>of</strong> premix and <strong>of</strong><br />

the premix during the preparation <strong>of</strong> the final fortified product. Manual mixing <strong>of</strong> the fortificant and<br />

premix with plain peanut butter was likewise recommended prior to mechanical mixing to facilitate their<br />

dispersion in the peanut butter matrix.<br />

Laboratory Trials at FDC<br />

Experiment 1: Validation <strong>of</strong> the adequacy <strong>of</strong> the 10 min mixing time established in the dye test<br />

Premix preparation. Results presented in Table 2.2 showed that peanut butter premix prepared in<br />

Trial 1 had an average vitamin A content <strong>of</strong> 263.70 µg RE/g peanut butter or a vitamin A recovery <strong>of</strong><br />

90.3%, indicating that approximately 10% <strong>of</strong> the vitamin A palmitate added was lost during processing.<br />

In terms <strong>of</strong> dispersion, it was found that the vitamin A added was uniformly distributed in the peanut<br />

butter premix as indicated by the low percentage variability <strong>of</strong> 2.78%. Premix prepared in Trial 2<br />

likewise showed an acceptable vitamin A content <strong>of</strong> 273.61 µg RE/g peanut butter or a vitamin A<br />

recovery <strong>of</strong> 93.7%.<br />

63

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