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VITAMIN A FORTIFIed PEANUT BUTTER - The Official Website of ...

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the collaborator at Vitachem Industries (44 Zamboanga St., Quezon City). According to the collaborator,<br />

the vitamin A fortificant was opened in January 2006 and stored thereafter at refrigerated conditions<br />

(10 o C). <strong>The</strong> vitamin A fortificant was described in the Product Data Sheet supplied by the collaborator as<br />

a greenish-yellow to golden-yellow, oily liquid which may crystallize on storage. It consists <strong>of</strong> pure<br />

vitamin A palmitate in peanut oil, and contains dl-α-tocopherol as an antioxidant (DSM Nutritional<br />

Products, No date). <strong>The</strong> vitamin A fortificant was assayed for vitamin A content prior to every use to<br />

determine its actual potency at the time <strong>of</strong> use.<br />

Weighing <strong>of</strong> ingredients<br />

[roasted peanuts, sugar, salt, oleo flakes (Oleo Fats, Inc., 2000), and vegetable oil]<br />

Transfer <strong>of</strong> each ingredient to a fabricated tumbler mixer<br />

Mixing <strong>of</strong> all ingredients in a fabricated tumbler mixer<br />

Manual transfer <strong>of</strong> the combined ingredients to an Almedah Emulsifier<br />

1 st grinding <strong>of</strong> the combined ingredients in an Almedah Emulsifier<br />

Repeat <strong>of</strong> above steps until four volumes <strong>of</strong> ~38.81 kg peanut butter have been prepared<br />

Manual transfer <strong>of</strong> four volumes <strong>of</strong> ~38.81 kg peanut butter to a stainless steel vessel<br />

Manual mixing <strong>of</strong> four volumes <strong>of</strong> ~38.81 kg peanut butter in a stainless steel vessel<br />

2 nd grinding <strong>of</strong> four volumes <strong>of</strong> ~38.81 kg peanut butter in a colloid mill for 15 minutes<br />

Cooling <strong>of</strong> peanut butter to 60 o C in a cooling tank equipped with a mechanical mixer<br />

Mixing <strong>of</strong> cooled peanut butter in a filler tank equipped with a mechanical mixer<br />

Fig. 5b.1 Schematic diagram <strong>of</strong> the process flow for the preparation <strong>of</strong> peanut butter matrix for<br />

receiving the vitamin A fortificant<br />

Method <strong>of</strong> Sampling and Analysis<br />

One sample each <strong>of</strong> fortified peanut butter was collected at the start, middle and end <strong>of</strong> the filling<br />

operations in plastic bottles, for vitamin A analysis. A 10 g sample <strong>of</strong> the vitamin A fortificant was taken<br />

from the 5 Kg capacity aluminum can and transferred to a 100 mL capacity aluminum can, for vitamin A<br />

assay. <strong>The</strong> vitamin A content <strong>of</strong> the fortified product and vitamin A fortificant were analyzed at the FDC<br />

Chemistry Laboratory using AOAC (1995) <strong>Official</strong> Method <strong>of</strong> Analysis # 974-29.<br />

147

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