VITAMIN A FORTIFIed PEANUT BUTTER - The Official Website of ...
VITAMIN A FORTIFIed PEANUT BUTTER - The Official Website of ... VITAMIN A FORTIFIed PEANUT BUTTER - The Official Website of ...
Since the collaborator decided to use medium to dark roasted peanuts as starting raw material for its peanut butter, an increase in the level of the stabilizer from 0.8% to 1.5% and 2.0% was recommended. Increasing the level of the stabilizer is expected to improve the stability of the fortified product. Details of the study on the standardization of the process for a stabilized peanut butter to a small company is described in Chapter 5 of Monograph 6 entitled Peanut Spreads and Confections (PCRSP, 2006). Study 2. Validation of the Results of Vitamin A Recovery and Stabilizer Performance in Fortified Peanut Butter Prepared Using Parameters Established for the Vitamin A Fortification and Stabilization of Peanut Butter for a Small Company. Table 5a.8 shows the vitamin A content and vitamin A recoveries of fortified peanut butter prepared with the fortificant and stabilizer added after grinding step at 2 min mixing time. Table 5a.8 Vitamin A content and % vitamin A recovery of fortified stabilized peanut butter prepared with the fortificant and stabilizer added at 2 min mixing time (FDC, 2006f) Sampling Point (during filling) Vit. A added (µgRE/g) Vitamin A Content and % Vitamin A Recovery Trial 1 Trial 2 Trial3 Vit. A found (µgRE/g) Vit. A recovery (%) Vit. A added (µgRE/g Vit. A found (µgRE/g) Vit. A recovery (%) Vit. A added (µgRE/g Vit. A found (µgRE/g) Vit. A recovery (%) Start 4.56 4.27 93.66 4.51 7.19 156.66 4.51 7.21 159.90 Middle 4.56 4.71 103.29 4.51 7.22 160.12 4.51 4.54 100.73 End 4.56 4.72 103.56 4.51 7.24 160.54 4.51 7.54 167.22 Average 4.56 4.56 100.17 4.51 6.97 154.67 4.51 6.40 142.03 Std. deviation 0.00 0.26 5.63 0.00 0.48 10.76 0.00 1.34 29.79 % variability 0.00 5.63 5.63 0.00 6.96 6.96 0.00 20.98 20.98 Fortified peanut butter prepared in Trial 1 resulted in relatively good vitamin A recoveries and variability which were noted to be comparable with the 110.13% average vitamin A recovery and 0.61% variability (FDC, 2006e) and 90.03% average vitamin A recovery and 11.42% variability (FDC, 2006d), reported in previous studies. The vitamin A recoveries obtained were 93.66%, 103.29% and 103.56% or an average vitamin A recovery of 100.17% and a variability of 5.63%. The vitamin A added was noted to have uniformly dispersed in the fortified product as indicated by the
However, in Trial 3, the vitamin A added did not uniformly disperse in the fortified product as indicated by the high % variability of the vitamin A recoveries. In terms of stabilizer performance, visual examination of the fortified products prepared in Trials 2 and 3 after 16 days in storage at ambient conditions, showed signs of a very slight flowing product when the bottle was tilted which was not observed in Trial 1. The failure of the product to fully stabilize was attributed to insufficient conditioning likely brought about by the disturbance of the formation of crystals during the cooling and conditioning/tempering step. It should be noted that during the cooling step, the ice used melted easily causing the temperature of the ice-water bath to increase. The addition of more ice to the ice-water bath in order to maintain a 10 o C temperature may have disturbed the formation of crystals. According to Woodroof (1973), any procedure or temperature which disturbs the setting and allows a reset, seems to increase firmness and separation of oil on the surface. Technology Transfer and Adoption The technologies for sorting blanched peanuts and stabilization of peanut butter were readily adopted by the collaborator. However, adoption of the technology for vitamin A fortification of peanut butter was temporarily shelved in favor of the technology for stabilization of peanut butter. The latter was prioritized to enable the company to continue distribution of its peanut butter in the Visayas and Mindanao regions which was discontinued sometime in 2006 because of high product returns due to oil separation. Another reason for the delayed adoption of the technology is the on-going negotiation of the collaborator with a large company who is interested in subcontracting the production of the stabilized peanut butter. Other reasons cited for the delayed adoption of the fortification technology were the following: (a) The need to hire a technical personnel to oversee the addition/mixing of fortificant because the present manpower complement of the company do not have a technical background; (b) The need to purchase additional equipment and other processing equipment to enable the company to adopt the recommended process; (c) The need to improve the plant conditions to enable the company to meet GMP requirements; (d) The need to register the fortified peanut butter with BFAD before the product could be distributed in the market. Constraints in the Transfer of Technologies for Stabilization and Vitamin A Fortification of Peanut Butter Following were the constraints encountered during the transfer of technology to the industry collaborator: (a) Lack of equipment in the collaborator’s plant for measuring the required amount of fortificant. The available weighing scale of the collaborator is not suitable for measuring the small volume of fortificant (0.4790 g) needed to fortify a 6 kg production batch of peanut butter. Thus, during the standardization of the process at the collaborator's plant, the fortificant needed had to be weighed at FDC and brought to the processing plant. (b) Lack of facilities for cooling and conditioning/tempering of the fortified stabilized peanut butter. The collaborator did not have an ice-water bath for cooling and a cold storage area for conditioning/tempering the fortified stabilized product, thus, plastic basins filled with ice and water had to be used for immediate cooling of the product while conditioning/tempering of the fortified stabilized product had to be done in a household refrigerator. 132
- Page 82 and 83: CHAPTER 3 VITAMIN A FORTIFICATION O
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- Page 106 and 107: µgRE/g = µg/g ß-carotene x 0.3
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However, in Trial 3, the vitamin A added did not uniformly disperse in the fortified product as indicated<br />
by the high % variability <strong>of</strong> the vitamin A recoveries.<br />
In terms <strong>of</strong> stabilizer performance, visual examination <strong>of</strong> the fortified products prepared in Trials<br />
2 and 3 after 16 days in storage at ambient conditions, showed signs <strong>of</strong> a very slight flowing product<br />
when the bottle was tilted which was not observed in Trial 1. <strong>The</strong> failure <strong>of</strong> the product to fully stabilize<br />
was attributed to insufficient conditioning likely brought about by the disturbance <strong>of</strong> the formation <strong>of</strong><br />
crystals during the cooling and conditioning/tempering step. It should be noted that during the cooling<br />
step, the ice used melted easily causing the temperature <strong>of</strong> the ice-water bath to increase. <strong>The</strong> addition <strong>of</strong><br />
more ice to the ice-water bath in order to maintain a 10 o C temperature may have disturbed the formation<br />
<strong>of</strong> crystals. According to Woodro<strong>of</strong> (1973), any procedure or temperature which disturbs the setting and<br />
allows a reset, seems to increase firmness and separation <strong>of</strong> oil on the surface.<br />
Technology Transfer and Adoption<br />
<strong>The</strong> technologies for sorting blanched peanuts and stabilization <strong>of</strong> peanut butter were readily<br />
adopted by the collaborator. However, adoption <strong>of</strong> the technology for vitamin A fortification <strong>of</strong> peanut<br />
butter was temporarily shelved in favor <strong>of</strong> the technology for stabilization <strong>of</strong> peanut butter. <strong>The</strong> latter was<br />
prioritized to enable the company to continue distribution <strong>of</strong> its peanut butter in the Visayas and<br />
Mindanao regions which was discontinued sometime in 2006 because <strong>of</strong> high product returns due to oil<br />
separation. Another reason for the delayed adoption <strong>of</strong> the technology is the on-going negotiation <strong>of</strong> the<br />
collaborator with a large company who is interested in subcontracting the production <strong>of</strong> the stabilized<br />
peanut butter. Other reasons cited for the delayed adoption <strong>of</strong> the fortification technology were the<br />
following:<br />
(a) <strong>The</strong> need to hire a technical personnel to oversee the addition/mixing <strong>of</strong> fortificant because the present<br />
manpower complement <strong>of</strong> the company do not have a technical background;<br />
(b) <strong>The</strong> need to purchase additional equipment and other processing equipment to enable the company to<br />
adopt the recommended process;<br />
(c) <strong>The</strong> need to improve the plant conditions to enable the company to meet GMP requirements;<br />
(d) <strong>The</strong> need to register the fortified peanut butter with BFAD before the product could be distributed in<br />
the market.<br />
Constraints in the Transfer <strong>of</strong> Technologies for Stabilization and Vitamin A Fortification <strong>of</strong> Peanut<br />
Butter<br />
Following were the constraints encountered during the transfer <strong>of</strong> technology to the industry collaborator:<br />
(a) Lack <strong>of</strong> equipment in the collaborator’s plant for measuring the required amount <strong>of</strong> fortificant. <strong>The</strong><br />
available weighing scale <strong>of</strong> the collaborator is not suitable for measuring the small volume <strong>of</strong><br />
fortificant (0.4790 g) needed to fortify a 6 kg production batch <strong>of</strong> peanut butter. Thus, during the<br />
standardization <strong>of</strong> the process at the collaborator's plant, the fortificant needed had to be weighed at<br />
FDC and brought to the processing plant.<br />
(b) Lack <strong>of</strong> facilities for cooling and conditioning/tempering <strong>of</strong> the fortified stabilized peanut butter. <strong>The</strong><br />
collaborator did not have an ice-water bath for cooling and a cold storage area for<br />
conditioning/tempering the fortified stabilized product, thus, plastic basins filled with ice and water<br />
had to be used for immediate cooling <strong>of</strong> the product while conditioning/tempering <strong>of</strong> the fortified<br />
stabilized product had to be done in a household refrigerator.<br />
132