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PARAMETER LIST - Unilever

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CENTRAL LABORATORY UNILEVER SWITZERLAND<br />

<strong>PARAMETER</strong> <strong>LIST</strong><br />

valid from May 2011


01 NUTRITIONAL VALUE<br />

Parameter Principle<br />

Ash gravimetric<br />

Moisture (Drying Oven) gravimetric<br />

Moisture (Vacuum Oven) gravimetric<br />

Moisture (Karl Fischer) Karl-Fischer<br />

Nitrogen / Protein; total Kjeldahl<br />

Lipids gravimetric<br />

Fatty acids composition GC-FID<br />

Sugar composition HPLC-RI<br />

Fibres (AOAC method) gravimetric<br />

Salt potentiometric<br />

Sodium Flame photometer<br />

Potassium Flame photometer<br />

Ethanol enzymatic<br />

Carbohydrates, total calculated<br />

Energy Value calculated<br />

02 FAT CHARACTERISTIC<br />

Lipids gravimetric<br />

Fatty acids composition GC-FID<br />

Fatty acids incl. trans-fatty acids GC-FID<br />

Peroxide value<br />

Peroxide value (after extraction)<br />

titrimetric<br />

Free fatty acids<br />

Free fatty acids (after extraction)<br />

titrimetric<br />

Liability to rancidity Rancimat<br />

Lauric acid GC-FID<br />

03 CARBOHYDRATES<br />

Sugar composition (Fru; Glc; Lac; Mal; Sac) HPLC-RI<br />

Fructose enzymatic<br />

Glucose enzymatic<br />

Saccharose enzymatic<br />

Lactose enzymatic<br />

Starch<br />

07 VITAMINS<br />

HPLC-RI<br />

Central Laboratory <strong>Unilever</strong> Switzerland (CLUS) Parameter List • www.unilever.ch/clus<br />

* Analysis performed by subcontractor


04 OTHER CHEMICAL <strong>PARAMETER</strong>S<br />

Parameter Principle<br />

Acid, total (calc. as Acetic acid) potentiometric<br />

Acid, total (calc. as Citric acid) potentiometric<br />

Lactic acid titrimetric<br />

Monosodiumglutamat (MSG) enzymatic<br />

Ethanol enzymatic<br />

pH value potentiometric<br />

Water activity potentiometric<br />

Ash; HCl insoluble gravimetric<br />

Essential Oils distillation<br />

Sulfur dioxide distillation<br />

Creatinine HPLC-UV<br />

Benzoic- / Sorbic acid HPLC-UV<br />

Antioxidant HPLC-UV<br />

Vitamin C HPLC-UV<br />

05 OTHER PHYSICAL <strong>PARAMETER</strong>S<br />

Particle size (Sieve analysis) gravimetric<br />

Gross / Net Weight gravimetric<br />

Brix refractometric<br />

Optical Rotation polarographic<br />

Turbidity (Gelatine) optical<br />

Color optical<br />

Absorbance photometric<br />

Density of powders (Apparent; Compact; ISO) gravimetric<br />

Density of liquids density<br />

Viscosity – (Bostwick / Bloom) Bostwick / texture analysis<br />

Viscosity – (Bloom (Gelatine)) texture analysis<br />

06 PESTICIDES<br />

Pesticide<br />

Pesticide Screening GC-MS*<br />

Dieldrin GC-MS<br />

Antiparasitica<br />

1,4-Dichlorbenzene GC-MS<br />

Thymol, Naphtalene, Nitrobenzene and PDCB GC-MS


07 PROCESS INDUCED CONTAMINANTS<br />

Parameter Principle<br />

Acrylamide GC-MS<br />

3-MCPD GC-MS<br />

3-MCPD-Ester GC-MS<br />

Irradiation indicators PSL / calibr. PSL* / TL*<br />

N-Nitrosodimethylamine GC-MS<br />

Mineral oil (n-Alcane) GC-FID<br />

08 QUALITY INDICATORS<br />

Allylisothiocyanate GC-FID<br />

Butyric-, Phenylacetic- and Phenylpropionic acid GC-FID<br />

09 ALLERGENS<br />

Parameter Principle<br />

Egg ELISA<br />

Gluten ELISA<br />

Milk ELISA<br />

Peanut ELISA<br />

Hazelnut ELISA<br />

Almond ELISA<br />

Walnut ELISA<br />

Soya ELISA<br />

Mustard ELISA<br />

Sesame ELISA<br />

Celery PCR<br />

Lupine PCR<br />

Fish PCR*<br />

10 GENETICALLY MODIFIED ORGANISM (GMO)<br />

GMO Screening (35S-Promotor; NOS-Term.) PCR<br />

GMO Quantification ( When GMO Screening pos.) PCR<br />

Maize: BT-11, NK 603, Mon810, GA21<br />

Soja: RR<br />

Central Laboratory <strong>Unilever</strong> Switzerland (CLUS) Parameter List • www.unilever.ch/clus<br />

* Analysis performed by subcontractor


11 MICROBIOLOGY<br />

Parameter Principle<br />

Aerobic Total Plate Count Counting<br />

Anaerobic Total Plate Count Counting<br />

Bacillus cereus Counting<br />

Clostridium perfringens Counting<br />

E.coli Counting<br />

Enterobacteriaceae Counting<br />

Enterococci Counting<br />

Fat splitting bacteria Counting<br />

Lactobacilli (qualitative) Counting<br />

Lactobacilli (quantitative) Counting<br />

Listeria monocytogenes (qualitative) Counting<br />

Listeria monocytogenes (quantitative) Counting<br />

Pseudomonas aeruginosa Counting<br />

Salmonella PCR / Counting<br />

Spores of aerobic mesophiles Counting<br />

Spores of anaerobic mesophiles Counting<br />

Staphylococcus aureus Counting<br />

Sulphite red. Clostridia germs Counting<br />

Sulphite red. Clostridia spores Counting<br />

Yeast Counting<br />

Molds Counting<br />

Challenge Test Counting<br />

Commercial sterility Counting<br />

Storage Test Counting<br />

12 HYGIENE SURVEY<br />

Surface slides / swabs Counting<br />

Hand hygiene Counting


13 WATER QUALITY<br />

Parameter Principle<br />

pH value<br />

conductivity<br />

potentiometric<br />

p-/m-value titrimetric<br />

Water Hardness Hach Lange<br />

CSB Hach Lange<br />

TOC Hach Lange<br />

Ammonium Hach Lange<br />

Chloride Hach Lange<br />

Nitrat Hach Lange<br />

Nitrite Hach Lange<br />

Phosphor (total) Hach Lange<br />

Sulfate Hach Lange<br />

Central Laboratory <strong>Unilever</strong> Switzerland (CLUS) Parameter List • www.unilever.ch/clus<br />

* Analysis performed by subcontractor


GENERAL TERMS OF SALES AND CONDITIONS OF CONTRACT<br />

All services or analyses will be done exclusively due to the following general terms of sales and conditions<br />

of contracts – if not otherwise agreed.<br />

Prices<br />

The rates in the pricelist do not include the statutory value-added tax.<br />

Price reductions for sample series or long-term contracts will be arranged with the customer for special<br />

agreements. Express services will be charged by a surcharge of 50%. There will be an extra charge for special<br />

sample treatments.<br />

Prices are subject to change without notice – except for written short-term offers.<br />

Delivery dates<br />

Delivery dates for standard analyses are usually 8-10 working days, for express analyses 1-5 working days.<br />

The indication of delivery date is not guaranteed. The delivery date starts after receiving the sample and clarification<br />

of all relevant information.<br />

We shall not be liable to the customer for any delays in performance or any non-performance of its obligations<br />

as a result of causes beyond its control (which for the avoidance of doubts shall include, but not be<br />

limited to, acts of God, strike, lock-out, government order, non-availability of equipment or parts, power or<br />

other utilities failures etc.) and also if they affect our suppliers or subcontractors.<br />

Claim for damages due to noncompliance of a delivery date will be excluded in either case.<br />

Terms of payment<br />

Payment of all invoices is due strictly within 30 days of the invoice date.<br />

Methodology<br />

The customer can not demand any analyses instructions. Details of the uncertainty of measurement for the<br />

parameters will be provided on request.<br />

Liability<br />

For the results of analyses as well as eventually resulting damages, the liability will be expressly excluded<br />

(within the legal requirements), also those for auxiliary persons.<br />

A special risk (e.g. explosive, toxic, carcinogenic etc.) of materials send for analyses has to be labeled as<br />

well as written in the order-form. Otherwise the client will be responsible for damage to persons or property<br />

resulting thereof.<br />

Samples and archival storage<br />

Volume and kind of service are in accordance to the written request.<br />

The requester is responsible for the property and conditions of the delivered samples.<br />

Rest of non perishable samples will be stored for 3 months, perishable samples will be stored for 5 working<br />

days. Data of analyses will be retained for 5 years.<br />

Duty of confidentiality<br />

Results of analyses and information regarding product and customer will be treated as strictly confidential.<br />

Without the written permission of the customer, certificates of analyses will neither be sent by internet nor to<br />

third parties.<br />

Cancellation<br />

A cancellation of an analyses request has to be done in written form by the requestor. The requester will be<br />

charged according to current rates for the efforts and working time until the cancellation.<br />

Placing of sub-orders<br />

The contractor is authorised to perform services by third parties. If necessary due to QA-regulations or<br />

certification guidelines, the transfer to third parties will be carried out after consulting the client.<br />

Customer feedback<br />

Customer feedback will be registered and handled within our quality management system.<br />

Place of jurisdiction and applicable law<br />

The Swiss law will be exclusively adopted. Place of jurisdiction is exclusively the domicile of the contractor.


Central Laboratory <strong>Unilever</strong> Switzerland (CLUS)<br />

<strong>Unilever</strong> Schweiz GmbH<br />

Bahnhofstrasse 19<br />

CH-8240 Thayngen<br />

Switzerland<br />

Phone +41 (0)52 645 6509<br />

Fax +41 (0)52 645 6145<br />

clus.ulch@unilever.com<br />

www.unilever.ch/clus

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