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Glycerol and spent lye clarification - Illinois Institute of Technology

Glycerol and spent lye clarification - Illinois Institute of Technology

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catching any chlorine that may be present or water<br />

that has not condensed in the condenser (7).<br />

From the tube (8) the current passes through the<br />

sulphuric acid U tube (9) <strong>and</strong> then through the<br />

oalcitjin chloride U tube (10) where any moisture is<br />

collected. Prom the calcium chloride tube (8)<br />

the current passes through a second calcium<br />

chloride tube (11) <strong>and</strong> then to the Geissler (12)<br />

<strong>and</strong> small calcium chloride tube attached to the<br />

Geissler <strong>and</strong> through a calcitun chloride tube to<br />

the pump, the last drying tube being a safety<br />

device to keep moisture from entering the Geissler<br />

from the pump direction.<br />

The apparatus needs no further attention than<br />

to assure that a current <strong>of</strong> air is kept moving<br />

through the eyetein so as to eliminate any backing<br />

up <strong>of</strong> acid in bottles 3 <strong>and</strong> 4.<br />

27

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