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Glycerol and spent lye clarification - Illinois Institute of Technology

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sepaj?ated soap has been sTcimmed <strong>of</strong>f it is<br />

removed to the glycerine plant where it is to<br />

be treated before going to the evaporators.<br />

The alkali in the <strong>lye</strong> must be neutralized <strong>and</strong><br />

the organic impurities removed.<br />

The neutralization <strong>of</strong> the alkali is<br />

affected by the addition <strong>of</strong> hydrochloric or<br />

sulphuric acids. The use <strong>of</strong> the former is<br />

open to objection due to high cost. It has<br />

the advantage, however, <strong>of</strong> producing as a<br />

result <strong>of</strong> the chemical action, sodium chloride<br />

which after recovery can be used again in the<br />

soap kettle.<br />

Sulphuric acid is most generally used.<br />

Its use introduces sulphate into the <strong>lye</strong> which<br />

salt is recovered with the common salt from<br />

the evaporator. Sodium sulphate however is<br />

practically useless for graining soap, its<br />

graining qualities being but three fifths that<br />

<strong>of</strong> sodium chloride <strong>and</strong> the grain produced is<br />

s<strong>of</strong>t <strong>and</strong> <strong>of</strong>ten hard to separate from the <strong>lye</strong>.<br />

To remove the organic impurities some<br />

9

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