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Glycerol and spent lye clarification - Illinois Institute of Technology

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Contents.<br />

Part I.<br />

Introduction. ---^------^ -Page 1.<br />

Part II.<br />

Lye Clarification. -.«-.------ Page 4,<br />

Evolution <strong>of</strong> the process j Kind <strong>of</strong> <strong>lye</strong>s;<br />

Yield <strong>of</strong> glycerine; Alkalinity <strong>of</strong> <strong>lye</strong>s; Acids<br />

for neutralizing alkali in <strong>lye</strong>; Metallic salts.<br />

Procel|dure for <strong>clarification</strong>; Neutral-<br />

ization <strong>of</strong> alkali; Theatment with metallic<br />

salts; Filtration,<br />

Nitrogenous matters; Cotton-seed oil<br />

soap <strong>lye</strong>8; Fermented <strong>lye</strong>s.<br />

Part III.<br />

Detection <strong>and</strong> Estimation <strong>of</strong> <strong>Glycerol</strong> - Page 14,<br />

Detection by physical properties;<br />

Quantitative test; Clarification <strong>of</strong> crude<br />

glycerol; Theory <strong>of</strong> estimation <strong>of</strong> glycerol<br />

"by carbon-dioxide ; Method <strong>of</strong> proceedure;<br />

Discussion <strong>of</strong> method; Apparatus for evolution<br />

<strong>of</strong> carbon-dioxide.<br />

Ill

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