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180 Abbreviations Ligands (cont.) 2,3-O-isopropylidene-2,3-hydroxy-1,4bis(diphenylphosphino)butane Diop norbornadiene (bicyclo[2.2.1]hepta-2,5-diene) nbd ç 5 -pentamethylcyclopentadienyl Cp* Radicals acetyl Ac aryl Ar benzotriazol-1-yl Bt benzoyl Bz benzyl Bn benzyloxycarbonyl Cbz benzyloxymethyl BOM 9-borabicyclo[3.3.1]nonyl 9-BBN tert-butoxycarbonyl Boc butyl Bu sec-butyl s-Bu tert-butyl t-Bu tert-butyldimethylsilyl TBDMS tert-butyldiphenylsilyl TBDPS cyclohexyl Cy 3,4-dimethoxybenzyl DMB ethyl Et ferrocenyl Fc 9-fluorenylmethoxycarbonyl Fmoc isobutyl iBu mesityl Mes mesyl Ms 4-methoxybenzyl PMB (2-methoxyethoxy)methyl MEM methoxymethyl MOM methyl Me 4-nitrobenzyl PNB phenyl Ph phthaloyl Phth phthalimido NPhth propyl Pr isopropyl iPr tetrahydropyranyl THP tolyl Tol tosyl Ts triethylsilyl TES triflyl, trifluoromethanesulfonyl Tf triisopropylsilyl TIPS trimethylsilyl TMS 2-(trimethylsilyl)ethoxymethyl SEM trityl [triphenylmethyl] Tr
Abbreviations 181 General absolute abs anhydrous anhyd aqueous aq boiling point bp catalyst no abbreviation catalytic cat. chemical shift ä circular dichroism CD column chromatographyno abbreviation concentrated concd configuration (in tables) Config coupling constant J dayd density d decomposed dec degrees Celsius 8C diastereomeric ratio dr dilute dil electron-donating group EDG electron-withdrawing group EWG electrophile E + enantiomeric excess ee enantiomeric ratio er equation eq equivalent(s) equiv flash-vacuum pyrolysis FVP gas chromatographyGC gas chromatography-mass spectrometry GC/MS gas–liquid chromatographyGLC gram g highest occupied molecular orbital HOMO high-performance liquid chromatographyHPLC hour(s) h infrared IR in situ in situ in vacuo in vacuo lethal dosage, e.g. to 50% of animals tested LD 50 liquid liq liter L lowest unoccupied molecular orbital LUMO mass spectrometryMS medium-pressure liquid chromatographyMPLC melting point mp milliliter mL millimole(s) mmol millimoles per liter mM minute(s) min mole(s) mol nuclear magnetic resonance NMR nucleophile Nu – optical purityop phase-transfer catalysis PTC proton NMR 1H NMR
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Science of Synthesis Houben-Weyl Me
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8 Science of Synthesis Category 1:
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Volume 1: Compounds withTransition
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Table of Contents Volume 2 13 Volum
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Table of Contents 15 Volume 4: Comp
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Table of Contents 17 4.4.27 Product
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2001 Georg Thieme Verlag Rüdigerst
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1.1 Product Class 1: Organometallic
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1.1 Product Class 1: Organometallic
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1.1.1 Nickel Complexes of 1,3-Diene
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1.1.1 Nickel Complexes of 1,3-Diene
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1.1.2 Nickel-Allyl Complexes 37 tra
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1.1.2 Nickel-Allyl Complexes 39 Bis
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1.1.2 Nickel-Allyl Complexes 41 App
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1.1.2 Nickel-Allyl Complexes 43 NiC
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1.1.2 Nickel-Allyl Complexes 45 Sch
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1.1.2 Nickel-Allyl Complexes 47 Sch
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1.1.3 Nickel-Alkyne Complexes 49 Ca
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1.1.3 Nickel-Alkyne Complexes 51 (2
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1.1.3 Nickel-Alkyne Complexes 53 Sc
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1.1.3 Nickel-Alkyne Complexes 55 at
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1.1.3 Nickel-Alkyne Complexes 57 Sc
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1.1.3 Nickel-Alkyne Complexes 59 en
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1.1.3 Nickel-Alkyne Complexes 61 of
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1.1.4 Nickel-Alkene Complexes 63 Bi
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1.1.4 Nickel-Alkene Complexes 65 Sc
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1.1.4 Nickel-Alkene Complexes 67 1.
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1.1.4 Nickel-Alkene Complexes 69 Sc
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1.1.4 Nickel-Alkene Complexes 71 [5
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1.1.4 Nickel-Alkene Complexes 75 4-
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References 79 References [1] Chetcu
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References 81 [98] Tsuda, T.; Mizun
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86 Biographical Sketches Rinaldo Po
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88 2.6.4.2.2 Variation 2: Two-Elect
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90 2.6 Product Class 6: Organometal
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92 Science of Synthesis 2.6 Complex
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100 Science of Synthesis 2.6 Comple
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Page 145 and 146: 4.4.27 Product Subclass 27: Æ-Halo
Page 147 and 148: 4.4.27 Æ-Haloalkylsilanes 147 Sche
Page 149 and 150: 4.4.27 Æ-Haloalkylsilanes 149 dros
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Page 159 and 160: References 159 References [1] Haman
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Page 166 and 167: 166 Biographical Sketches Alan Spiv
Page 168 and 169: 168 5.1.22 Product Subclass 22: Ary
Page 170 and 171: 170 Science of Synthesis 5.1 German
Page 176 and 177: 176 References [43] Eaborn, C.; Var
Page 178 and 179: 178 Abbreviations Chemical (cont.)
Page 182: 182 Abbreviations General (cont.) q
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