Continuous Flow Synthesis - Selected Examples from ... - ThalesNano
Continuous Flow Synthesis - Selected Examples from ... - ThalesNano
Continuous Flow Synthesis - Selected Examples from ... - ThalesNano
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Case Study: 2-Methylbenzimidazole Formation<br />
Conversion [%]<br />
Kinetic Study<br />
100<br />
T [°C]<br />
80<br />
60<br />
40<br />
20<br />
0<br />
0 5 10 15 20 25 30 35 40 45 50 55 60<br />
Time [min]<br />
60 °C<br />
100 °C<br />
130 °C<br />
160 °C<br />
200 °C<br />
>99 % conv.<br />
after<br />
25 9 weeks<br />
60 5 days<br />
100 5 h<br />
130 (2 bar) 30 min<br />
160 (4 bar) 10 min<br />
200 (9 bar) 3 min<br />
270 (29 bar) “1 s”
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