Continuous Flow Synthesis - Selected Examples from ... - ThalesNano
Continuous Flow Synthesis - Selected Examples from ... - ThalesNano
Continuous Flow Synthesis - Selected Examples from ... - ThalesNano
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<strong>Continuous</strong> <strong>Flow</strong> Newman-Kwart Rearrangement<br />
Kinetic Analysis (HPLC)<br />
HPLC Conversion (%)<br />
100<br />
80<br />
60<br />
40<br />
20<br />
0<br />
NMP<br />
DME<br />
NMP<br />
100 150 200 250 300<br />
Temperature (°C)<br />
DME<br />
flow processing<br />
100-330 °C, 60-80 bar<br />
1 mL min-1 flow rate<br />
4 mL coil<br />
residence time 4 min
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