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W. Richard Bowen and Nidal Hilal 4

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Force<br />

1.2 THE ATOMIC FORCE MICROsCOPE 5<br />

Intermittent<br />

contact mode<br />

Contact mode<br />

Distance<br />

Repulsion<br />

Non-contact mode<br />

Attraction<br />

fIgure .3 Diagram illustrating the force regimes under which each of the three most<br />

common AFM imaging modes operate. Contact mode operation is in the repulsive force<br />

regime, where the probe is pressed against the sample surface, causing an upwards deflection<br />

of the cantilever. Non-contact mode interrogates the long-range forces experienced<br />

prior to actual contact with the surface. With intermittent contact, or tapping mode, the<br />

probe is oscillated close to the surface where it repeatedly comes into <strong>and</strong> out of contact<br />

with the surface.<br />

This ‘optical lever’ method to detect deflection of the cantilever is the<br />

method primarily in use currently [2, 3]. However, the original design<br />

for the AFM used an STM piggy-backed onto the upper side of the AFM<br />

as a deflection sensor [1]. Whilst this allowed extremely accurate determination<br />

of the deflection, it also could detect deflection only within a<br />

very small range, which is insufficient for most purposes. In addition,<br />

other methods have been trialled in the past for this purpose including<br />

the measurement of optical interferometry effects [4] as well as fabricating<br />

levers to be able to detect deflection through a piezoresistance-based<br />

mechanism [5–14].<br />

Scanners are available in different configurations, depending upon<br />

the particular AFM employed, or the purpose for which it is required.<br />

Tube scanners consist of a hollow tube made of piezoceramic material.<br />

Depending on how electrical current is applied, the tube may extend in<br />

the z-direction or be caused to flex in either the x- or y-direction to facilitate<br />

scanning. Alternatively scanners may consist of separate piezocrystals<br />

for each movement direction. Such a configuration removes certain<br />

non-linearity problems, which may occur in the simpler tube scanners.<br />

In many commercially available AFMs, especially in older models, the<br />

movement in the x- <strong>and</strong> y-directions may be achieved by the movement<br />

of the sample rather than by the movement of the probe.

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